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Electrochemistry of Pd-based nanoparticles prepared via thermal decomposition of palladium acetylacetonate

Igor Nikolaevich Leontyev 1
Igor Nikolaevich Leontyev
, 
Alexandra Borisovna Kuriganova 2
Alexandra Borisovna Kuriganova
, 
Alexandra A Gubanova 2
Alexandra A Gubanova
, 
Alexey N Yatsenko 2
Alexey N Yatsenko
, 
Mikhail Vladimirovich Gorshenkov 3
Mikhail Vladimirovich Gorshenkov
, 
Vera Pavlovna Kashparova 1
Vera Pavlovna Kashparova
, 
Nikolay Georgievich Leont'ev 4
Nikolay Georgievich Leont'ev
, 
Nina Vladimirovna Smirnova 2
Nina Vladimirovna Smirnova
1 Department of Physics, Southern Federal University, 344090 Rostov-on-Don, Russian Federation
2 Department of Technology, Platov South Russian State Polytechnic University (NPI), 346428 Novocherkassk, Russian Federation
3 National University of Science and Technology ‘MISIS’, 119049 Moscow, Russian Federation
4 Azov-Black Sea Engineering Institute of Don State Agrarian University, 347740 Zernograd, Russian Federation
10.71267/mencom.7975
Published 4 June 2026 , received 24 November 2025
Communication , Volume 36, Issue 4, 478-480
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Leontyev I. N. et al. Electrochemistry of Pd-based nanoparticles prepared via thermal decomposition of palladium acetylacetonate // Mendeleev Communications. 2026. Vol. 36. No. 4. pp. 478-480.
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Leontyev I. N., Kuriganova A. B., Gubanova A. A., Yatsenko A. N., Gorshenkov M. V., Kashparova V. P., Leont'ev N. G., Smirnova N. V. Electrochemistry of Pd-based nanoparticles prepared via thermal decomposition of palladium acetylacetonate // Mendeleev Communications. 2026. Vol. 36. No. 4. pp. 478-480.
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TY - JOUR
DO - 10.71267/mencom.7975
UR - https://mendcomm.colab.ws/publications/10.71267/mencom.7975
TI - Electrochemistry of Pd-based nanoparticles prepared via thermal decomposition of palladium acetylacetonate
T2 - Mendeleev Communications
AU - Leontyev, Igor Nikolaevich
AU - Kuriganova, Alexandra Borisovna
AU - Gubanova, Alexandra A
AU - Yatsenko, Alexey N
AU - Gorshenkov, Mikhail Vladimirovich
AU - Kashparova, Vera Pavlovna
AU - Leont'ev, Nikolay Georgievich
AU - Smirnova, Nina Vladimirovna
PY - 2026
DA - 2026/06/04
PB - Mendeleev Communications
SP - 478-480
IS - 4
VL - 36
ER -
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@article{2026_Leontyev,
author = {Igor Nikolaevich Leontyev and Alexandra Borisovna Kuriganova and Alexandra A Gubanova and Alexey N Yatsenko and Mikhail Vladimirovich Gorshenkov and Vera Pavlovna Kashparova and Nikolay Georgievich Leont'ev and Nina Vladimirovna Smirnova},
title = {Electrochemistry of Pd-based nanoparticles prepared via thermal decomposition of palladium acetylacetonate},
journal = {Mendeleev Communications},
year = {2026},
volume = {36},
publisher = {Mendeleev Communications},
month = {Jun},
url = {https://mendcomm.colab.ws/publications/10.71267/mencom.7975},
number = {4},
pages = {478--480},
doi = {10.71267/mencom.7975}
}
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Leontyev, Igor Nikolaevich, et al. “Electrochemistry of Pd-based nanoparticles prepared via thermal decomposition of palladium acetylacetonate.” Mendeleev Communications, vol. 36, no. 4, Jun. 2026, pp. 478-480. https://mendcomm.colab.ws/publications/10.71267/mencom.7975.
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Keywords

electrocatalysis
palladium acetylacetonate
palladium oxide
Pd nanoparticles
thermal decomposition

Abstract

Using thermal decomposition of palladium acetylacetonate in a nonisothermal mode, we synthesized two models of carbon-supported Pd-based nanoparticles with similar Pd lattice parameters and varying sizes and the presence or absence of a PdO phase in the electrocatalyst. These model systems were examined in the electrocatalytic processes of CO stripping, ethanol and formic acid electrooxidation reactions, and electrochemical reduction of hydrogen peroxide.

Funders

Russian Science Foundation
25-19-00280

References

1.
Chernysheva D.V., Klushin V.A., Alekseenko A.A., Moguchikh E.A., Kolesnikov E.A., Gorshenkov M.V., Kaichev V.V., Fesenko L.N., Smirnova N.V.
Mendeleev Communications, 2024