Home / Publications / Crystal structure of C60Cl6 prepared by a reaction of C60 with POCl3

Crystal structure of C60Cl6 prepared by a reaction of C60 with POCl3

Natalia Borisovna Shustova 1
Natalia Borisovna Shustova
, 
Dmitry Yu Chernyshev 2
Dmitry Yu Chernyshev
, 
10.1070/MC2006v016n04ABEH002307
Published 2006-09-01
Communication , Volume 16, Issue 4, 209-210
13
Share
Cite this
GOST
 | 
Cite this
GOST Copy
Shustova N. B., Chernyshev D. Yu., Troyanov S. I. Crystal structure of C60Cl6 prepared by a reaction of C60 with POCl3 // Mendeleev Communications. 2006. Vol. 16. No. 4. pp. 209-210.
GOST all authors (up to 50) Copy
Shustova N. B., Chernyshev D. Yu., Troyanov S. I. Crystal structure of C60Cl6 prepared by a reaction of C60 with POCl3 // Mendeleev Communications. 2006. Vol. 16. No. 4. pp. 209-210.
RIS
 | 
Cite this
RIS Copy
TY - JOUR
DO - 10.1070/MC2006v016n04ABEH002307
UR - https://mendcomm.colab.ws/publications/10.1070/MC2006v016n04ABEH002307
TI - Crystal structure of C60Cl6 prepared by a reaction of C60 with POCl3
T2 - Mendeleev Communications
AU - Shustova, Natalia Borisovna
AU - Chernyshev, Dmitry Yu
AU - Troyanov, Sergey Igorevich
PY - 2006
DA - 2006/09/01
PB - Mendeleev Communications
SP - 209-210
IS - 4
VL - 16
ER -
BibTex
 | 
Cite this
BibTex (up to 50 authors) Copy
@article{2006_Shustova,
author = {Natalia Borisovna Shustova and Dmitry Yu Chernyshev and Sergey Igorevich Troyanov},
title = {Crystal structure of C60Cl6 prepared by a reaction of C60 with POCl3},
journal = {Mendeleev Communications},
year = {2006},
volume = {16},
publisher = {Mendeleev Communications},
month = {Sep},
url = {https://mendcomm.colab.ws/publications/10.1070/MC2006v016n04ABEH002307},
number = {4},
pages = {209--210},
doi = {10.1070/MC2006v016n04ABEH002307}
}
MLA
Cite this
MLA Copy
Shustova, Natalia Borisovna, et al. “Crystal structure of C60Cl6 prepared by a reaction of C60 with POCl3.” Mendeleev Communications, vol. 16, no. 4, Sep. 2006, pp. 209-210. https://mendcomm.colab.ws/publications/10.1070/MC2006v016n04ABEH002307.

Abstract

C60Cl6 was prepared using POCl3 as a chlorinating agent; crystal structure determination revealed that the C60Cl6 molecules are packed in slightly corrugated layers, which are arranged in the ABAC sequence.

References

1.
Preparation and crystallographic characterization of C60Cl24.
Shustova N.B., Popov A.A., Sidorov L.N., Turnbull A.P., Kemnitz E., Troyanov S.I.
Chemical Communications, 2005
2.
Preparation and Structural Characterization of Two Kinetically Stable Chlorofullerenes, C60Cl28 and C60Cl30
Troyanov S.I., Shustova N.B., Popov A.A., Sidorov L.N., Kemnitz E.
Angewandte Chemie - International Edition, 2005
3.
Synthesis and structure of the highly chlorinated [60]fullerene C60Cl30 with a drum-shaped carbon cage.
Troshin P.A., Lyubovskaya R.N., Ioffe I.N., Shustova N.B., Kemnitz E., Troyanov S.I.
Angewandte Chemie - International Edition, 2005
4.
Preparation and 13C NMR spectroscopic characterisation of C60Cl6
Birkett P.R., Avent A.G., Darwish A.D., Kroto H.W., Taylor R., Walton D.R.
Journal of the Chemical Society Chemical Communications, 1993
5.
Identity of Transients Formed from Chlorinated Fullerenes in Organic Solvents:  A Pulse Radiolysis Study
Priyadarsini K.I., Mohan H., Birkett P.R., Mittal J.P.
The Journal of Physical Chemistry, 1996
6.
The structure of C60Ph5Cl and C60Ph5H, formed via electrophilic aromatic substitution
Avent A.G., Birkett P.R., Crane J.D., Darwish A.D., Langley G.J., Kroto H.W., Taylor R., Walton D.R.
Journal of the Chemical Society Chemical Communications, 1994
7.
A hexaallyl[60]fullerene, C60(CH2CHCH2)6
Abdul-Sada A.K., Avent A.G., Birkett P.R., Kroto H.W., Taylor R., Walton D.R.
Journal of the Chemical Society Perkin Transactions 1, 1998
8.
Arylation of [60]fullerene via electrophilic aromaticsubstitution involving the electrophile C60Cl6:frontside nucleophilic substitution of fullerenes
Birkett P.R., Avent A.G., Darwish A.D., Hahn I., Kroto H.W., Langley G.J., O’Loughlin J., Taylor R., Walton D.R.
Journal of the Chemical Society Perkin Transactions 2, 1997
9.
The influence of phenylated by-products on the MALDI analysis of chlorinated fullerenes
Vasil’ev Y.V., Streletskiy A.V., Kuvychko I.V., Boltalina O.V., Birkett P.R., Campbell E.E., Korobov M.V., Drewello T.
International Journal of Mass Spectrometry, 2003
10.
Seven-minute synthesis of pure C(s)-C60Cl6 from [60]fullerene and iodine monochloride: first IR, Raman, and mass spectra of 99 mol % C60Cl6.
Kuvychko I.V., Streletskii A.V., Popov A.A., Kotsiris S.G., Drewello T., Strauss S.H., Boltalina O.V.
Chemistry - A European Journal, 2005
11.
Some New Aspects of Chlorination of Fullerenes
Troshin P.A., Popkov O., Lyubovskaya R.N.
Fullerenes Nanotubes and Carbon Nanostructures, 2003
12.
Solid C60: a new form of carbon
Krätschmer W., Lamb L.D., Fostiropoulos K., Huffman D.R.
Nature, 1990
13.
The gas-phase on-line production of phosphoryl halides, POX3 and their identification by infrared spectroscopy
Allaf A.W.
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 1998
14.
10.1070/MC2006v016n04ABEH002307_bib14
Troshin
Izv. Akad. Nauk, Ser. Khim., 2004