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Synthesis and crystal structure of the tetraalkylammonium salts of 1,2,3,4-tetramercapto-1,2,3,4-tetrathioxotetraphosphetane based on white phosphorus

Elena Kazimirovna Badeeva 1
Elena Kazimirovna Badeeva
, 
Dmitry Borisovich Krivolapov 1
Dmitry Borisovich Krivolapov
, 
Aidar Timergalievich Gubaidullin 1
Aidar Timergalievich Gubaidullin
, 
Igor Anatol'evich Litvinov 1
Igor Anatol'evich Litvinov
, 
Elvira Salikhovna Batyeva 1
Elvira Salikhovna Batyeva
, 
10.1070/MC2005v015n01ABEH001996
Published 2005-02-09
Communication , Volume 15, Issue 1, 22-23
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Badeeva E. K. et al. Synthesis and crystal structure of the tetraalkylammonium salts of 1,2,3,4-tetramercapto-1,2,3,4-tetrathioxotetraphosphetane based on white phosphorus // Mendeleev Communications. 2005. Vol. 15. No. 1. pp. 22-23.
GOST all authors (up to 50) Copy
Badeeva E. K., Krivolapov D. B., Gubaidullin A. T., Litvinov I. A., Batyeva E. S., Sinyashin O. G. Synthesis and crystal structure of the tetraalkylammonium salts of 1,2,3,4-tetramercapto-1,2,3,4-tetrathioxotetraphosphetane based on white phosphorus // Mendeleev Communications. 2005. Vol. 15. No. 1. pp. 22-23.
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TY - JOUR
DO - 10.1070/MC2005v015n01ABEH001996
UR - https://mendcomm.colab.ws/publications/10.1070/MC2005v015n01ABEH001996
TI - Synthesis and crystal structure of the tetraalkylammonium salts of 1,2,3,4-tetramercapto-1,2,3,4-tetrathioxotetraphosphetane based on white phosphorus
T2 - Mendeleev Communications
AU - Badeeva, Elena Kazimirovna
AU - Krivolapov, Dmitry Borisovich
AU - Gubaidullin, Aidar Timergalievich
AU - Litvinov, Igor Anatol'evich
AU - Batyeva, Elvira Salikhovna
AU - Sinyashin, Oleg Gerol'dovich
PY - 2005
DA - 2005/02/09
PB - Mendeleev Communications
SP - 22-23
IS - 1
VL - 15
ER -
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@article{2005_Badeeva,
author = {Elena Kazimirovna Badeeva and Dmitry Borisovich Krivolapov and Aidar Timergalievich Gubaidullin and Igor Anatol'evich Litvinov and Elvira Salikhovna Batyeva and Oleg Gerol'dovich Sinyashin},
title = {Synthesis and crystal structure of the tetraalkylammonium salts of 1,2,3,4-tetramercapto-1,2,3,4-tetrathioxotetraphosphetane based on white phosphorus},
journal = {Mendeleev Communications},
year = {2005},
volume = {15},
publisher = {Mendeleev Communications},
month = {Feb},
url = {https://mendcomm.colab.ws/publications/10.1070/MC2005v015n01ABEH001996},
number = {1},
pages = {22--23},
doi = {10.1070/MC2005v015n01ABEH001996}
}
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Badeeva, Elena Kazimirovna, et al. “Synthesis and crystal structure of the tetraalkylammonium salts of 1,2,3,4-tetramercapto-1,2,3,4-tetrathioxotetraphosphetane based on white phosphorus.” Mendeleev Communications, vol. 15, no. 1, Feb. 2005, pp. 22-23. https://mendcomm.colab.ws/publications/10.1070/MC2005v015n01ABEH001996.

Abstract

The reaction of P4 with sulfur, 3-methylbutane-1-thiol and alkylamines yields tetraalkylammonium salts of tetraphosphetane previously unknown; the crystal structure of the tetrakis(triethylammonium) salt of 1,2,3,4-tetramercapto-1,2,3,4-tetrathioxotetraphosphetane is determined by X-ray diffraction analysis.

References

2.
10.1070/MC2005v015n01ABEH001996_bib1_2
Voronkov
Reaktsii sery s organicheskimi soedineniyami (Reactions of Sulfur with Organic Compounds), 1979
3.
10.1070/MC2005v015n01ABEH001996_bib2
Batyeva
XVII Mendeleev Congress on General and Applied Chemistry, 2003
4.
Tables of bond lengths determined by X-ray and neutron diffraction. Part 1. Bond lengths in organic compounds
Allen F.H., Kennard O., Watson D.G., Brammer L., Orpen A.G., Taylor R.
Journal of the Chemical Society Perkin Transactions 2, 1987
5.
Beilsteins Handbuch der Org. Chemie, Vierte Auflage, 1958, Bd. I, no. 2, S. 1647.
6.
E-map improvement in direct procedures
Altomare A., Cascarano G., Giacovazzo C., Viterbo D.
Acta Crystallographica Section A Foundations of Crystallography, 1991
7.
10.1070/MC2005v015n01ABEH001996_bib6
Sheldrick
SHELXL97 – A Computer Program for Crystal Structure Determination, 1997
8.
WinGXsuite for small-molecule single-crystal crystallography
Farrugia L.J.
Journal of Applied Crystallography, 1999
9.
10.1070/MC2005v015n01ABEH001996_bib8
Straver
1994
10.
10.1070/MC2005v015n01ABEH001996_bib9
Spek
Acta Crystallogr., Sect. A., 1990