Home / Publications / Crystal engineering strategies in alkane-bis(ammonium) 2,5-diaza-3,6-dioxobicyclo[2.2.2]octane-1,4-dicarboxylates

Crystal engineering strategies in alkane-bis(ammonium) 2,5-diaza-3,6-dioxobicyclo[2.2.2]octane-1,4-dicarboxylates

Denis Alekseevich Lenev 1
Denis Alekseevich Lenev
, 
Konstantin Alexandrovich Lyssenko 2
Konstantin Alexandrovich Lyssenko
, 
Remir Grigorevich Kostyanovsky 1
Remir Grigorevich Kostyanovsky
10.1070/MC2004v014n06ABEH002071
Published 2004-12-17
Communication , Volume 14, Issue 6, 312-314
6
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Lenev D. A., Lyssenko K. A., Kostyanovsky R. G. Crystal engineering strategies in alkane-bis(ammonium) 2,5-diaza-3,6-dioxobicyclo[2.2.2]octane-1,4-dicarboxylates // Mendeleev Communications. 2004. Vol. 14. No. 6. pp. 312-314.
GOST all authors (up to 50) Copy
Lenev D. A., Lyssenko K. A., Kostyanovsky R. G. Crystal engineering strategies in alkane-bis(ammonium) 2,5-diaza-3,6-dioxobicyclo[2.2.2]octane-1,4-dicarboxylates // Mendeleev Communications. 2004. Vol. 14. No. 6. pp. 312-314.
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TY - JOUR
DO - 10.1070/MC2004v014n06ABEH002071
UR - https://mendcomm.colab.ws/publications/10.1070/MC2004v014n06ABEH002071
TI - Crystal engineering strategies in alkane-bis(ammonium) 2,5-diaza-3,6-dioxobicyclo[2.2.2]octane-1,4-dicarboxylates
T2 - Mendeleev Communications
AU - Lenev, Denis Alekseevich
AU - Lyssenko, Konstantin Alexandrovich
AU - Kostyanovsky, Remir Grigorevich
PY - 2004
DA - 2004/12/17
PB - Mendeleev Communications
SP - 312-314
IS - 6
VL - 14
ER -
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@article{2004_Lenev,
author = {Denis Alekseevich Lenev and Konstantin Alexandrovich Lyssenko and Remir Grigorevich Kostyanovsky},
title = {Crystal engineering strategies in alkane-bis(ammonium) 2,5-diaza-3,6-dioxobicyclo[2.2.2]octane-1,4-dicarboxylates},
journal = {Mendeleev Communications},
year = {2004},
volume = {14},
publisher = {Mendeleev Communications},
month = {Dec},
url = {https://mendcomm.colab.ws/publications/10.1070/MC2004v014n06ABEH002071},
number = {6},
pages = {312--314},
doi = {10.1070/MC2004v014n06ABEH002071}
}
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Lenev, Denis Alekseevich, et al. “Crystal engineering strategies in alkane-bis(ammonium) 2,5-diaza-3,6-dioxobicyclo[2.2.2]octane-1,4-dicarboxylates.” Mendeleev Communications, vol. 14, no. 6, Dec. 2004, pp. 312-314. https://mendcomm.colab.ws/publications/10.1070/MC2004v014n06ABEH002071.

Abstract

The crystal structures of (+)-3, (±)-4 and P-(–)-5 were studied; the competitive H-bonding of carboxylic groups in (+)-3 and (±)-4 leads to disruption of crystal structure elements, used previously in crystal engineering of chiral bis(lactams); the new structure elements may be described as 1D homochiral R22(10) tapes; the diastereomeric resolution in P-(–)-5 is rationalised using an analogy between the H-bonded structure of the salt and 2,5-diaza-3,6-dioxobicyclo[2.2.2]octane-1,4-dicarboxylic acid dihydrate.

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