Home / Articles / Kinetic resolution of 1-methyl- and 1-phenyl-3-amino-1,2-dicarba-closo-dodecaboranes via acylation with chiral acyl chlorides

Kinetic resolution of 1-methyl- and 1-phenyl-3-amino-1,2-dicarba-closo-dodecaboranes via acylation with chiral acyl chlorides

Galina L'vovna Levit 1
Galina L'vovna Levit
, 
Victor Pavlovich Krasnov 1
Victor Pavlovich Krasnov
, 
Alexander Mikhailovich Demin 1
Alexander Mikhailovich Demin
, 
Mikhail Isaakovich Kodess 1
Mikhail Isaakovich Kodess
, 
Liliya Shirmukhametovna Sadretdinova 1
Liliya Shirmukhametovna Sadretdinova
, 
Tatyana Victorovna Matveeva 1
Tatyana Victorovna Matveeva
, 
Valentina Antonovna Ol'shevskaya 2
Valentina Antonovna Ol'shevskaya
, 
Valery Nikolaevich Kalinin 2
Valery Nikolaevich Kalinin
, 
Oleg Nikolaevich Chupakhin 1
Oleg Nikolaevich Chupakhin
, 
10.1070/MC2004v014n06ABEH002047
Published 17 December 2004 , received 27 September 2004
Communication , Volume 14, Issue 6, 293-295
14
Share
Cite this
GOST
 | 
Cite this
GOST
Copy cite
Levit G. L. et al. Kinetic resolution of 1-methyl- and 1-phenyl-3-amino-1,2-dicarba-closo-dodecaboranes via acylation with chiral acyl chlorides // Mendeleev Communications. 2004. Vol. 14. No. 6. pp. 293-295.
GOST all authors (up to 50)
Copy cite
Levit G. L., Krasnov V. P., Demin A. M., Kodess M. I., Sadretdinova L. S., Matveeva T. V., Ol'shevskaya V. A., Kalinin V. N., Chupakhin O. N., Charushin V. N. Kinetic resolution of 1-methyl- and 1-phenyl-3-amino-1,2-dicarba-closo-dodecaboranes via acylation with chiral acyl chlorides // Mendeleev Communications. 2004. Vol. 14. No. 6. pp. 293-295.
RIS
 | 
Cite this
RIS
Copy cite
TY - JOUR
DO - 10.1070/MC2004v014n06ABEH002047
UR - https://mendcomm.colab.ws/publications/10.1070/MC2004v014n06ABEH002047
TI - Kinetic resolution of 1-methyl- and 1-phenyl-3-amino-1,2-dicarba-closo-dodecaboranes via acylation with chiral acyl chlorides
T2 - Mendeleev Communications
AU - Levit, Galina L'vovna
AU - Krasnov, Victor Pavlovich
AU - Demin, Alexander Mikhailovich
AU - Kodess, Mikhail Isaakovich
AU - Sadretdinova, Liliya Shirmukhametovna
AU - Matveeva, Tatyana Victorovna
AU - Ol'shevskaya, Valentina Antonovna
AU - Kalinin, Valery Nikolaevich
AU - Chupakhin, Oleg Nikolaevich
AU - Charushin, Valery Nikolaevich
PY - 2004
DA - 2004/12/17
PB - Mendeleev Communications
SP - 293-295
IS - 6
VL - 14
ER -
BibTex
 | 
Cite this
BibTex (up to 50 authors)
Copy cite
@article{2004_Levit,
author = {Galina L'vovna Levit and Victor Pavlovich Krasnov and Alexander Mikhailovich Demin and Mikhail Isaakovich Kodess and Liliya Shirmukhametovna Sadretdinova and Tatyana Victorovna Matveeva and Valentina Antonovna Ol'shevskaya and Valery Nikolaevich Kalinin and Oleg Nikolaevich Chupakhin and Valery Nikolaevich Charushin},
title = {Kinetic resolution of 1-methyl- and 1-phenyl-3-amino-1,2-dicarba-closo-dodecaboranes via acylation with chiral acyl chlorides},
journal = {Mendeleev Communications},
year = {2004},
volume = {14},
publisher = {Mendeleev Communications},
month = {Dec},
url = {https://mendcomm.colab.ws/publications/10.1070/MC2004v014n06ABEH002047},
number = {6},
pages = {293--295},
doi = {10.1070/MC2004v014n06ABEH002047}
}
MLA
Cite this
MLA
Copy cite
Levit, Galina L'vovna, et al. “Kinetic resolution of 1-methyl- and 1-phenyl-3-amino-1,2-dicarba-closo-dodecaboranes via acylation with chiral acyl chlorides.” Mendeleev Communications, vol. 14, no. 6, Dec. 2004, pp. 293-295. https://mendcomm.colab.ws/publications/10.1070/MC2004v014n06ABEH002047.
Views / Visits / Downloads
37 / 37 / 57

Abstract

A study of the kinetic resolution of racemic 1-substituted 3-amino-1,2-dicarba-closo-dodecaboranes by chiral acyl chlorides has shown that N-tosyl-(S)-prolyl and N-phthaloyl-(S)-alaninyl chlorides are more efficient resolving agents than (S)-naproxen chloride.

References

3.
The Chemistry of Neutron Capture Therapy
Soloway A.H., Tjarks W., Barnum B.A., Rong F., Barth R.F., Codogni I.M., Wilson J.G.
Chemical Reviews, 1998
4.
Enantiomers of 3-amino-1-methyl-1,2-dicarba-closo-dodecaborane
Krasnov V.P., Levit G.L., Charushin V.N., Grishakov A.N., Kodess M.I., Kalinin V.N., Ol'shevskaya V.A., Chupakhin O.N.
Tetrahedron Asymmetry, 2002
5.
Palladium and Rhodium Complexes with Planar-Chiral Carborane Ligands
Brunner H., Apfelbacher A., Zabel M.
European Journal of Inorganic Chemistry, 2001
6.
Kinetic resolution of (±)-2,3-dihydro-3-methyl-4H-1,4-benzoxazines with (S)-naproxen
Charushin V.N., Krasnov V.P., Levit G.L., Korolyova M.A., Kodess M.I., Chupakhin O.N., Kim M.H., Lee H.S., Park Y.J., Kim K.
Tetrahedron Asymmetry, 1999
7.
Krasnov V.P., Levit G.L., Andreeva I.N., Grishakov A.N., Charushin V.N., Chupakhin O.N.
Mendeleev Communications, 2002
8.
Kinetic resolution of (±)-2,3-dihydro-3-methyl-4H-1,4-benzoxazine, (±)-2-methyl-1,2,3,4-tetrahydroquinoline and (±)-2-methylindoline using N-tosyl-(S)-prolyl chloride
Krasnov V.P., Levit G.L., Bukrina I.M., Andreeva I.N., Sadretdinova L.S., Korolyova M.A., Kodess M.I., Charushin V.N., Chupakhin O.N.
Tetrahedron Asymmetry, 2003
9.
N-Phthaloyl-(S)-alanyl chloride as a chiral resolving agent for the kinetic resolution of heterocyclic amines
Krasnov V.P., Levit G.L., Kodess M.I., Charushin V.N., Chupakhin O.N.
Tetrahedron Asymmetry, 2004
10.
Potemkin V.A., Krasnov V.P., Levit G.L., Bartashevich E.V., Andreeva I.N., Kuzminsky M.B., Anikin N.A., Charushin V.N., Chupakhin O.N.
Mendeleev Communications, 2004
11.
10.1070/MC2004v014n06ABEH002047_bib11
Krasnov
Izv. Akad. Nauk, Ser. Khim., 2004