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Reaction of 2-acetyl-5-methyl-2H-1,2,3-diazaphosphole with butane-2,3-diol

Narkis Gabbasovna Khusainova 1
Narkis Gabbasovna Khusainova
,  , 
Nail Mustafovich Azancheev 2
Nail Mustafovich Azancheev
, 
Igor Anatol'evich Litvinov 2
Igor Anatol'evich Litvinov
, 
Dmitry Borisovich Krivolapov 2
Dmitry Borisovich Krivolapov
, 
Rafael Askhatovich Cherkasov 1
Rafael Askhatovich Cherkasov
10.1070/MC2004v014n05ABEH001926
Published 2004-09-29
Communication , Volume 14, Issue 5, 212-214
11
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Khusainova N. G. et al. Reaction of 2-acetyl-5-methyl-2H-1,2,3-diazaphosphole with butane-2,3-diol // Mendeleev Communications. 2004. Vol. 14. No. 5. pp. 212-214.
GOST all authors (up to 50) Copy
Khusainova N. G., Mostovaya O. A., Azancheev N. M., Litvinov I. A., Krivolapov D. B., Cherkasov R. A. Reaction of 2-acetyl-5-methyl-2H-1,2,3-diazaphosphole with butane-2,3-diol // Mendeleev Communications. 2004. Vol. 14. No. 5. pp. 212-214.
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TY - JOUR
DO - 10.1070/MC2004v014n05ABEH001926
UR - https://mendcomm.colab.ws/publications/10.1070/MC2004v014n05ABEH001926
TI - Reaction of 2-acetyl-5-methyl-2H-1,2,3-diazaphosphole with butane-2,3-diol
T2 - Mendeleev Communications
AU - Khusainova, Narkis Gabbasovna
AU - Mostovaya, Olga Aleksandrovna
AU - Azancheev, Nail Mustafovich
AU - Litvinov, Igor Anatol'evich
AU - Krivolapov, Dmitry Borisovich
AU - Cherkasov, Rafael Askhatovich
PY - 2004
DA - 2004/09/29
PB - Mendeleev Communications
SP - 212-214
IS - 5
VL - 14
ER -
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@article{2004_Khusainova,
author = {Narkis Gabbasovna Khusainova and Olga Aleksandrovna Mostovaya and Nail Mustafovich Azancheev and Igor Anatol'evich Litvinov and Dmitry Borisovich Krivolapov and Rafael Askhatovich Cherkasov},
title = {Reaction of 2-acetyl-5-methyl-2H-1,2,3-diazaphosphole with butane-2,3-diol},
journal = {Mendeleev Communications},
year = {2004},
volume = {14},
publisher = {Mendeleev Communications},
month = {Sep},
url = {https://mendcomm.colab.ws/publications/10.1070/MC2004v014n05ABEH001926},
number = {5},
pages = {212--214},
doi = {10.1070/MC2004v014n05ABEH001926}
}
MLA
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Khusainova, Narkis Gabbasovna, et al. “Reaction of 2-acetyl-5-methyl-2H-1,2,3-diazaphosphole with butane-2,3-diol.” Mendeleev Communications, vol. 14, no. 5, Sep. 2004, pp. 212-214. https://mendcomm.colab.ws/publications/10.1070/MC2004v014n05ABEH001926.

Abstract

The reaction of 2-acetyl-5-methyl-2H-1,2,3-diazaphosphole with (rac)-butane-2,3-diol at temperatures below 0 °C leads to the formation of a hydrospirophosphorane containing both a diazaphospholene and a dioxaphospholane ring system and a β-hydroxyalkoxy-1,2,3-diazaphospholene. On heating, these products form a hydrospirotetraoxaphosphorane, its tautomeric monocyclic β-hydroxyalkylphosphite and N-acetyl-N’-isopropylidene-hydrazine.

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