Abstract
The complexes (PriO)2P(S)NHC(S)R (R=NEt2, NHPh), [(PriO)2P(S)NHC(S)]2-1,10-diaza-18-crown-6 have been obtained by the metathesis reaction of potassium salts of corresponding thiophosphorylated thioureas with (PPh3)2CuNO3; the crystal structure of (Ph3P)2Cu[Et2NC(S)NP(S)(OPri)2] has been confirmed by X-ray crystallography.
References
1.
Tarkhanova I.G., Smirnov V.V., Rostovshchikova T.N.
Kinetics and Catalysis,
2001
2.
Pellei M., Pettinari C., Santini C., Skelton B.W., Somers N., White A.H.
Journal of the Chemical Society Dalton Transactions,
2000
3.
Haiduc I., Cea-Olivares R., Toscano R.A., Silvestru C.
Polyhedron,
1995
4.
Novosad J., Necas M., Marek J., Veltsistas P., Papadimitriou C., Haiduc I., Watanabe M., Woollins J.D.
Inorganica Chimica Acta,
1999
5.
Silvestru A., Rotar A., Drake J.E., Hursthouse M.B., Light M.E., Farcas S.I., Rösler R., Silvestru C.
Canadian Journal of Chemistry,
2001
6.
Birdsall D.J., Green J., Ly T.Q., Novosad J., Necas M., Slawin A.M., Woollins J.D., Zak Z.
European Journal of Inorganic Chemistry,
1999
7.
Yang R., Wang D., Liu Y., Jin D.
Polyhedron,
2001
8.
Shin H.-., Hampden-Smith M.J., Duesler E.N., Kodas T.T.
Polyhedron,
1991
9.
10.1070/MC2003v013n04ABEH001717_bib9
Brusko
Zh. Obshch. Khim.,
2000
10.
Grim S.O., Yankowsky A.W.
Journal of Organic Chemistry,
1977
11.
Ohrenberg C., Liable-Sands L.M., Rheingold A.L., Riordan C.G.
Inorganic Chemistry,
2001
12.
Altomare A., Cascarano G., Giacovazzo C., Viterbo D.
Acta Crystallographica Section A Foundations of Crystallography,
1991
13.
10.1070/MC2003v013n04ABEH001717_bib13
Straver
1994
14.
10.1070/MC2003v013n04ABEH001717_bib14
Spec
Acta Crystallogr., Sect. A,
1990