Home / Publications / Spontaneous resolution in the imidazolidin-2-one series

Spontaneous resolution in the imidazolidin-2-one series

Angelina Nikolaevna Kravchenko 1
Angelina Nikolaevna Kravchenko
, 
Gulnara Konstantinovna Kadorkina 2
Gulnara Konstantinovna Kadorkina
, 
Andrey Sergeevich Sigachev 1
Andrey Sergeevich Sigachev
, 
Elena Yulianovna Maksareva 1
Elena Yulianovna Maksareva
, 
Konstantin Alexandrovich Lyssenko 3
Konstantin Alexandrovich Lyssenko
, 
Pavel Alekseevich Belyakov 1
Pavel Alekseevich Belyakov
, 
Oleg Vasilevich Lebedev 1
Oleg Vasilevich Lebedev
, 
Oleg Nikolaevich Kharybin 4
Oleg Nikolaevich Kharybin
, 
Nina Nikolaevna Makhova 1
Nina Nikolaevna Makhova
, 
Remir Grigorevich Kostyanovsky 2
Remir Grigorevich Kostyanovsky
10.1070/MC2003v013n03ABEH001736
Published 2003-07-11
Communication , Volume 13, Issue 3, 114-116
15
Share
Cite this
GOST
 | 
Cite this
GOST Copy
Kravchenko A. N. et al. Spontaneous resolution in the imidazolidin-2-one series // Mendeleev Communications. 2003. Vol. 13. No. 3. pp. 114-116.
GOST all authors (up to 50) Copy
Kravchenko A. N., Kadorkina G. K., Sigachev A. S., Maksareva E. Y., Lyssenko K. A., Belyakov P. A., Lebedev O. V., Kharybin O. N., Makhova N. N., Kostyanovsky R. G. Spontaneous resolution in the imidazolidin-2-one series // Mendeleev Communications. 2003. Vol. 13. No. 3. pp. 114-116.
RIS
 | 
Cite this
RIS Copy
TY - JOUR
DO - 10.1070/MC2003v013n03ABEH001736
UR - https://mendcomm.colab.ws/publications/10.1070/MC2003v013n03ABEH001736
TI - Spontaneous resolution in the imidazolidin-2-one series
T2 - Mendeleev Communications
AU - Kravchenko, Angelina Nikolaevna
AU - Kadorkina, Gulnara Konstantinovna
AU - Sigachev, Andrey Sergeevich
AU - Maksareva, Elena Yulianovna
AU - Lyssenko, Konstantin Alexandrovich
AU - Belyakov, Pavel Alekseevich
AU - Lebedev, Oleg Vasilevich
AU - Kharybin, Oleg Nikolaevich
AU - Makhova, Nina Nikolaevna
AU - Kostyanovsky, Remir Grigorevich
PY - 2003
DA - 2003/07/11
PB - Mendeleev Communications
SP - 114-116
IS - 3
VL - 13
ER -
BibTex
 | 
Cite this
BibTex (up to 50 authors) Copy
@article{2003_Kravchenko,
author = {Angelina Nikolaevna Kravchenko and Gulnara Konstantinovna Kadorkina and Andrey Sergeevich Sigachev and Elena Yulianovna Maksareva and Konstantin Alexandrovich Lyssenko and Pavel Alekseevich Belyakov and Oleg Vasilevich Lebedev and Oleg Nikolaevich Kharybin and Nina Nikolaevna Makhova and Remir Grigorevich Kostyanovsky},
title = {Spontaneous resolution in the imidazolidin-2-one series},
journal = {Mendeleev Communications},
year = {2003},
volume = {13},
publisher = {Mendeleev Communications},
month = {Jul},
url = {https://mendcomm.colab.ws/publications/10.1070/MC2003v013n03ABEH001736},
number = {3},
pages = {114--116},
doi = {10.1070/MC2003v013n03ABEH001736}
}
MLA
Cite this
MLA Copy
Kravchenko, Angelina Nikolaevna, et al. “Spontaneous resolution in the imidazolidin-2-one series.” Mendeleev Communications, vol. 13, no. 3, Jul. 2003, pp. 114-116. https://mendcomm.colab.ws/publications/10.1070/MC2003v013n03ABEH001736.

Abstract

For the first time, spontaneous resolution of trans-dihydroxyimidazolidin-2-one 1a was performed and racemisation of (–)-1a was studied; regiospecific reaction of 1a–c with aminoguanidine resulted in derivatives 2a–c; compound 2b was also shown to undergo spontaneous resolution, and the absolute configuration (4R,5R) of (–)-2b crystals was established by X-ray diffraction analysis.

References

2.
Einwirkung von Glyoxal auf Harnstoff; neue Bildungsweisen des Hydantoins
Pauly H., Sauter H.
Berichte der deutschen chemischen Gesellschaft (A and B Series), 1930
3.
Formation and Identification of cis- and trans-Dihydroxyimidazolidinones from Ureas and Glyoxal
Vail S.L., Barker R.H., Mennitt P.G.
Journal of Organic Chemistry, 1965
4.
10.1070/MC2003v013n03ABEH001736_bib2_3
Zaagg
1965
5.
Synthese und Eigenschaften füngliedriger cyclischer Harnstoffe
Petersen H.
European Journal of Organic Chemistry, 1969
8.
Kravchenko A.N., Lebedev O.V., Maksareva E.Y.
Mendeleev Communications, 2000
9.
Chegaev K.Y., Kravchenko A.N., Lebedev O.V., Strelenko Y.A.
Mendeleev Communications, 2001
10.
Gazieva G.A., Lyssenko K.A., Gaziev R.G., Kravchenko A.N., Lebedev O.V., Zhulin V.M.
Mendeleev Communications, 2001
11.
Gazieva G.A., Kravchenko A.N., Lebedev O.V., Lyssenko K.A., Dekaprilevich M.O., Men'shov V.M., Strelenko Y.A., Makhova N.N.
Mendeleev Communications, 2001
12.
Crystal Structure of d-Desthiobiotin.
OKABE N., SASAKI Y.
Chemical and Pharmaceutical Bulletin, 2011
13.
Molecular Encapsulation
Hof F., Craig S.L., Nuckolls C., Rebek Jr. J.
Angewandte Chemie - International Edition, 2002
14.
Social Isomers in Encapsulation Complexes
Shivanyuk A., Rebek J.
Journal of the American Chemical Society, 2002
15.
Kostyanovsky R.G., Lyssenko K.A., Kadorkina G.K., Lebedev O.V., Kravchenko A.N., Chervin I.I., Kostyanovsky V.R.
Mendeleev Communications, 1998
16.
Kostyanovsky R.G., Lyssenko K.A., Kravchenko A.N., Lebedev O.V., Kadorkina G.K., Kostyanovsky V.R.
Mendeleev Communications, 2001
17.
Kostyanovsky R.G., Kadorkina G.K., Lyssenko K.A., Torbeev V.Y., Kravchenko A.N., Lebedev O.V., Grintselev-Knyazev G.V., Kostyanovsky V.R.
Mendeleev Communications, 2002
19.
10.1070/MC2003v013n03ABEH001736_bib6
Aekella
Acta Crystallogr., 1974