Home / Publications / N-Thiophosphorylthiourea containing an aza-18-crown-6 fragment. The crystal structure of bis[N-(N’-diisopropoxythiophosphorylamidothiocarbonyl)-aza-18-crown-6]nickel(II)

N-Thiophosphorylthiourea containing an aza-18-crown-6 fragment. The crystal structure of bis[N-(N’-diisopropoxythiophosphorylamidothiocarbonyl)-aza-18-crown-6]nickel(II)

Felix Dmitrievich Sokolov 1
Felix Dmitrievich Sokolov
, 
Nail Galievich Zabirov 1
Nail Galievich Zabirov
,  , 
Dmitry Borisovich Krivolapov 2
Dmitry Borisovich Krivolapov
, 
Igor Anatol'evich Litvinov 2
Igor Anatol'evich Litvinov
10.1070/MC2003v013n02ABEH001733
Published 2003-04-28
Communication , Volume 13, Issue 2, 72-73
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Sokolov F. D. et al. N-Thiophosphorylthiourea containing an aza-18-crown-6 fragment. The crystal structure of bis[N-(N’-diisopropoxythiophosphorylamidothiocarbonyl)-aza-18-crown-6]nickel(II) // Mendeleev Communications. 2003. Vol. 13. No. 2. pp. 72-73.
GOST all authors (up to 50) Copy
Sokolov F. D., Zabirov N. G., Brusko V. V., Krivolapov D. B., Litvinov I. A. N-Thiophosphorylthiourea containing an aza-18-crown-6 fragment. The crystal structure of bis[N-(N’-diisopropoxythiophosphorylamidothiocarbonyl)-aza-18-crown-6]nickel(II) // Mendeleev Communications. 2003. Vol. 13. No. 2. pp. 72-73.
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TY - JOUR
DO - 10.1070/MC2003v013n02ABEH001733
UR - https://mendcomm.colab.ws/publications/10.1070/MC2003v013n02ABEH001733
TI - N-Thiophosphorylthiourea containing an aza-18-crown-6 fragment. The crystal structure of bis[N-(N’-diisopropoxythiophosphorylamidothiocarbonyl)-aza-18-crown-6]nickel(II)
T2 - Mendeleev Communications
AU - Sokolov, Felix Dmitrievich
AU - Zabirov, Nail Galievich
AU - Brusko, Vasiliy Valer'evich
AU - Krivolapov, Dmitry Borisovich
AU - Litvinov, Igor Anatol'evich
PY - 2003
DA - 2003/04/28
PB - Mendeleev Communications
SP - 72-73
IS - 2
VL - 13
ER -
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@article{2003_Sokolov,
author = {Felix Dmitrievich Sokolov and Nail Galievich Zabirov and Vasiliy Valer'evich Brusko and Dmitry Borisovich Krivolapov and Igor Anatol'evich Litvinov},
title = {N-Thiophosphorylthiourea containing an aza-18-crown-6 fragment. The crystal structure of bis[N-(N’-diisopropoxythiophosphorylamidothiocarbonyl)-aza-18-crown-6]nickel(II)},
journal = {Mendeleev Communications},
year = {2003},
volume = {13},
publisher = {Mendeleev Communications},
month = {Apr},
url = {https://mendcomm.colab.ws/publications/10.1070/MC2003v013n02ABEH001733},
number = {2},
pages = {72--73},
doi = {10.1070/MC2003v013n02ABEH001733}
}
MLA
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Sokolov, Felix Dmitrievich, et al. “N-Thiophosphorylthiourea containing an aza-18-crown-6 fragment. The crystal structure of bis[N-(N’-diisopropoxythiophosphorylamidothiocarbonyl)-aza-18-crown-6]nickel(II).” Mendeleev Communications, vol. 13, no. 2, Apr. 2003, pp. 72-73. https://mendcomm.colab.ws/publications/10.1070/MC2003v013n02ABEH001733.

Abstract

N-(N’-Diisopropoxythiophosphorylamidothiocarbonyl)aza-18-crown-6 (HL) was obtained by the reaction of aza-18-crown-6 with diisopropoxythiophosphorylisothiocyanate, and its chelate with NiII was characterised using IR, 1H and 31P NMR spectroscopy and single-crystal X-ray diffraction.

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