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Synthesis and properties of benzo[b]thiopheno[2,3-d]-1,3,2λ5-diazaphosphinane-2-thione derivatives

Dmitry Borisovich Nilov 1
Dmitry Borisovich Nilov
, 
Vladimir Grigor'evich Granik 2
Vladimir Grigor'evich Granik
1 Centre for Medicinal Chemistry. Sergo Ordzhonikidze All-Russian Research Chemical-Pharmaceutical Institute, Moscow, Russian Federation
10.1070/MC2003v013n02ABEH001705
Published 2003-04-28
Communication , Volume 13, Issue 2, 78-79
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Nilov D. B., Granik V. G. Synthesis and properties of benzo[b]thiopheno[2,3-d]-1,3,2λ5-diazaphosphinane-2-thione derivatives // Mendeleev Communications. 2003. Vol. 13. No. 2. pp. 78-79.
GOST all authors (up to 50) Copy
Nilov D. B., Granik V. G. Synthesis and properties of benzo[b]thiopheno[2,3-d]-1,3,2λ5-diazaphosphinane-2-thione derivatives // Mendeleev Communications. 2003. Vol. 13. No. 2. pp. 78-79.
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TY - JOUR
DO - 10.1070/MC2003v013n02ABEH001705
UR - https://mendcomm.colab.ws/publications/10.1070/MC2003v013n02ABEH001705
TI - Synthesis and properties of benzo[b]thiopheno[2,3-d]-1,3,2λ5-diazaphosphinane-2-thione derivatives
T2 - Mendeleev Communications
AU - Nilov, Dmitry Borisovich
AU - Granik, Vladimir Grigor'evich
PY - 2003
DA - 2003/04/28
PB - Mendeleev Communications
SP - 78-79
IS - 2
VL - 13
ER -
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@article{2003_Nilov,
author = {Dmitry Borisovich Nilov and Vladimir Grigor'evich Granik},
title = {Synthesis and properties of benzo[b]thiopheno[2,3-d]-1,3,2λ5-diazaphosphinane-2-thione derivatives},
journal = {Mendeleev Communications},
year = {2003},
volume = {13},
publisher = {Mendeleev Communications},
month = {Apr},
url = {https://mendcomm.colab.ws/publications/10.1070/MC2003v013n02ABEH001705},
number = {2},
pages = {78--79},
doi = {10.1070/MC2003v013n02ABEH001705}
}
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Nilov, Dmitry Borisovich, and Vladimir Grigor'evich Granik. “Synthesis and properties of benzo[b]thiopheno[2,3-d]-1,3,2λ5-diazaphosphinane-2-thione derivatives.” Mendeleev Communications, vol. 13, no. 2, Apr. 2003, pp. 78-79. https://mendcomm.colab.ws/publications/10.1070/MC2003v013n02ABEH001705.

Abstract

The treatment of 2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylic acid amide with phosphorus pentasulfide in the presence of pyridine yielded 4,5,6,7-tetrahydrobenzo[b]thiopheno[2,3-d]-1,3,2λ5-diazaphosphinane-2-thione; the alkylation of its sodium salts was studied.

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