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Unsymmetrical porphyrazines with annulated 1,2,5-thia(seleno)diazole and 3,6-diamyloxybenzene rings: synthesis, characterization and X-ray crystal structure of H2{XN2}{3,6-(OAm)2Bz}3Pz (X = S, Se)

Evgeny Valentinovich Kudrik 1
Evgeny Valentinovich Kudrik
, 
Elvira M Bauer 2
Elvira M Bauer
, 
Claudio Ercolani 2
Claudio Ercolani
, 
Angiola Chiesi-Villa 2
Angiola Chiesi-Villa
, 
Corrado Rizzoli 3
Corrado Rizzoli
, 
Anna Alexandrovna Gaberkorn 1
Anna Alexandrovna Gaberkorn
, 
10.1070/MC2001v011n02ABEH001372
Published 2001-04-24
Communication , Volume 11, Issue 2, 45-47
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Kudrik E. V. et al. Unsymmetrical porphyrazines with annulated 1,2,5-thia(seleno)diazole and 3,6-diamyloxybenzene rings: synthesis, characterization and X-ray crystal structure of H2{XN2}{3,6-(OAm)2Bz}3Pz (X = S, Se) // Mendeleev Communications. 2001. Vol. 11. No. 2. pp. 45-47.
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Kudrik E. V., Bauer E. M., Ercolani C., Chiesi-Villa A., Rizzoli C., Gaberkorn A. A., Stuzhin P. A. Unsymmetrical porphyrazines with annulated 1,2,5-thia(seleno)diazole and 3,6-diamyloxybenzene rings: synthesis, characterization and X-ray crystal structure of H2{XN2}{3,6-(OAm)2Bz}3Pz (X = S, Se) // Mendeleev Communications. 2001. Vol. 11. No. 2. pp. 45-47.
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TY - JOUR
DO - 10.1070/MC2001v011n02ABEH001372
UR - https://mendcomm.colab.ws/publications/10.1070/MC2001v011n02ABEH001372
TI - Unsymmetrical porphyrazines with annulated 1,2,5-thia(seleno)diazole and 3,6-diamyloxybenzene rings: synthesis, characterization and X-ray crystal structure of H2{XN2}{3,6-(OAm)2Bz}3Pz (X = S, Se)
T2 - Mendeleev Communications
AU - Kudrik, Evgeny Valentinovich
AU - Bauer, Elvira M
AU - Ercolani, Claudio
AU - Chiesi-Villa, Angiola
AU - Rizzoli, Corrado
AU - Gaberkorn, Anna Alexandrovna
AU - Stuzhin, Pavel Anatolievich
PY - 2001
DA - 2001/04/24
PB - Mendeleev Communications
SP - 45-47
IS - 2
VL - 11
ER -
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@article{2001_Kudrik,
author = {Evgeny Valentinovich Kudrik and Elvira M Bauer and Claudio Ercolani and Angiola Chiesi-Villa and Corrado Rizzoli and Anna Alexandrovna Gaberkorn and Pavel Anatolievich Stuzhin},
title = {Unsymmetrical porphyrazines with annulated 1,2,5-thia(seleno)diazole and 3,6-diamyloxybenzene rings: synthesis, characterization and X-ray crystal structure of H2{XN2}{3,6-(OAm)2Bz}3Pz (X = S, Se)},
journal = {Mendeleev Communications},
year = {2001},
volume = {11},
publisher = {Mendeleev Communications},
month = {Apr},
url = {https://mendcomm.colab.ws/publications/10.1070/MC2001v011n02ABEH001372},
number = {2},
pages = {45--47},
doi = {10.1070/MC2001v011n02ABEH001372}
}
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Kudrik, Evgeny Valentinovich, et al. “Unsymmetrical porphyrazines with annulated 1,2,5-thia(seleno)diazole and 3,6-diamyloxybenzene rings: synthesis, characterization and X-ray crystal structure of H2{XN2}{3,6-(OAm)2Bz}3Pz (X = S, Se).” Mendeleev Communications, vol. 11, no. 2, Apr. 2001, pp. 45-47. https://mendcomm.colab.ws/publications/10.1070/MC2001v011n02ABEH001372.

Abstract

Cyclotetramerization of a mixture of 3,4-dicyano-1,2,5-thiadiazole or 3,4-dicyano-1,2,5-selenodiazole with 3,6-diamyloxyphthalodinitrile gives new unsymmetrical porphyrazines with annulated 1,2,5-thia(seleno)diazole and 3,6-diamyloxybenzene rings; the structures of the 1:3 products H2{XN2}{3,6-(OAm)2Bz}3Pz (X = S, Se) has been elucidated by single-crystal X-ray diffraction.

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