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3,7-Dimethyl-3,7-diazabicyclo[3.3.1]nonane-2,6-dione-1,5-dicarboxylic acid derivatives: synthesis, structure and resolution

Remir Grigorevich Kostyanovsky 1
Remir Grigorevich Kostyanovsky
, 
Konstantin Alexandrovich Lyssenko 2
Konstantin Alexandrovich Lyssenko
, 
Denis Alekseevich Lenev 3
Denis Alekseevich Lenev
, 
Yuri Il'ich Èl'natanov 1
Yuri Il'ich Èl'natanov
, 
Oleg Nikolaevich Krutius 1
Oleg Nikolaevich Krutius
, 
Irina Aleksandrovna Bronzova 1
Irina Aleksandrovna Bronzova
10.1070/MC1999v009n04ABEH001067
Published 1999-07-09
Communication , Volume 9, Issue 4, 151-154
4
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Kostyanovsky R. G. et al. 3,7-Dimethyl-3,7-diazabicyclo[3.3.1]nonane-2,6-dione-1,5-dicarboxylic acid derivatives: synthesis, structure and resolution // Mendeleev Communications. 1999. Vol. 9. No. 4. pp. 151-154.
GOST all authors (up to 50) Copy
Kostyanovsky R. G., Lyssenko K. A., Lenev D. A., Èl'natanov Y. I., Krutius O. N., Bronzova I. A. 3,7-Dimethyl-3,7-diazabicyclo[3.3.1]nonane-2,6-dione-1,5-dicarboxylic acid derivatives: synthesis, structure and resolution // Mendeleev Communications. 1999. Vol. 9. No. 4. pp. 151-154.
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TY - JOUR
DO - 10.1070/MC1999v009n04ABEH001067
UR - https://mendcomm.colab.ws/publications/10.1070/MC1999v009n04ABEH001067
TI - 3,7-Dimethyl-3,7-diazabicyclo[3.3.1]nonane-2,6-dione-1,5-dicarboxylic acid derivatives: synthesis, structure and resolution
T2 - Mendeleev Communications
AU - Kostyanovsky, Remir Grigorevich
AU - Lyssenko, Konstantin Alexandrovich
AU - Lenev, Denis Alekseevich
AU - Èl'natanov, Yuri Il'ich
AU - Krutius, Oleg Nikolaevich
AU - Bronzova, Irina Aleksandrovna
PY - 1999
DA - 1999/07/09
PB - Mendeleev Communications
SP - 151-154
IS - 4
VL - 9
ER -
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@article{1999_Kostyanovsky,
author = {Remir Grigorevich Kostyanovsky and Konstantin Alexandrovich Lyssenko and Denis Alekseevich Lenev and Yuri Il'ich Èl'natanov and Oleg Nikolaevich Krutius and Irina Aleksandrovna Bronzova},
title = {3,7-Dimethyl-3,7-diazabicyclo[3.3.1]nonane-2,6-dione-1,5-dicarboxylic acid derivatives: synthesis, structure and resolution},
journal = {Mendeleev Communications},
year = {1999},
volume = {9},
publisher = {Mendeleev Communications},
month = {Jul},
url = {https://mendcomm.colab.ws/publications/10.1070/MC1999v009n04ABEH001067},
number = {4},
pages = {151--154},
doi = {10.1070/MC1999v009n04ABEH001067}
}
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Kostyanovsky, Remir Grigorevich, et al. “3,7-Dimethyl-3,7-diazabicyclo[3.3.1]nonane-2,6-dione-1,5-dicarboxylic acid derivatives: synthesis, structure and resolution.” Mendeleev Communications, vol. 9, no. 4, Jul. 1999, pp. 151-154. https://mendcomm.colab.ws/publications/10.1070/MC1999v009n04ABEH001067.

Abstract

Diamide monohydrate 6 was found to form a conglomerate (space group P21), and it was spontaneously resolved by crystallization; esters 1 and 2 were optically enriched by classical methods; the above compounds were structurally characterised by NMR spectroscopy and X-ray analysis.

References

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Kostyanovsky R.G., Lyssenko K.A., El’natanov Y.I., Krutius O.N., Bronzova I.A., Strelenko Y.A., Kostyanovsky V.R.
Mendeleev Communications, 1999
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Mendeleev Communications, 1998
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Kostyanovsky R.G., El’natanov Y.I., Krutius O.N., Lyssenko K.A., Strelenko Y.A.
Mendeleev Communications, 1999
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