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3,7-Diazabicyclo[3.3.1]nonane-2,6-diones: building of homo- and heterochiral crystals

Remir Grigorevich Kostyanovsky 1
Remir Grigorevich Kostyanovsky
, 
Konstantin Alexandrovich Lyssenko 2
Konstantin Alexandrovich Lyssenko
, 
Yuri Il'ich Èl'natanov 1
Yuri Il'ich Èl'natanov
, 
Oleg Nikolaevich Krutius 1
Oleg Nikolaevich Krutius
, 
Irina Aleksandrovna Bronzova 1
Irina Aleksandrovna Bronzova
, 
Yurii Andreevich Strelenko 3
Yurii Andreevich Strelenko
, 
Vasily Remirovich Kostyanovsky 1
Vasily Remirovich Kostyanovsky
10.1070/MC1999v009n03ABEH001058
Published 27 May 1999 , received 22 October 1998
Communication , Volume 9, Issue 3, 106-108
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Kostyanovsky R. G. et al. 3,7-Diazabicyclo[3.3.1]nonane-2,6-diones: building of homo- and heterochiral crystals // Mendeleev Communications. 1999. Vol. 9. No. 3. pp. 106-108.
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Kostyanovsky R. G., Lyssenko K. A., Èl'natanov Y. I., Krutius O. N., Bronzova I. A., Strelenko Y. A., Kostyanovsky V. R. 3,7-Diazabicyclo[3.3.1]nonane-2,6-diones: building of homo- and heterochiral crystals // Mendeleev Communications. 1999. Vol. 9. No. 3. pp. 106-108.
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TY - JOUR
DO - 10.1070/MC1999v009n03ABEH001058
UR - https://mendcomm.colab.ws/publications/10.1070/MC1999v009n03ABEH001058
TI - 3,7-Diazabicyclo[3.3.1]nonane-2,6-diones: building of homo- and heterochiral crystals
T2 - Mendeleev Communications
AU - Kostyanovsky, Remir Grigorevich
AU - Lyssenko, Konstantin Alexandrovich
AU - Èl'natanov, Yuri Il'ich
AU - Krutius, Oleg Nikolaevich
AU - Bronzova, Irina Aleksandrovna
AU - Strelenko, Yurii Andreevich
AU - Kostyanovsky, Vasily Remirovich
PY - 1999
DA - 1999/05/27
PB - Mendeleev Communications
SP - 106-108
IS - 3
VL - 9
ER -
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@article{1999_Kostyanovsky,
author = {Remir Grigorevich Kostyanovsky and Konstantin Alexandrovich Lyssenko and Yuri Il'ich Èl'natanov and Oleg Nikolaevich Krutius and Irina Aleksandrovna Bronzova and Yurii Andreevich Strelenko and Vasily Remirovich Kostyanovsky},
title = {3,7-Diazabicyclo[3.3.1]nonane-2,6-diones: building of homo- and heterochiral crystals},
journal = {Mendeleev Communications},
year = {1999},
volume = {9},
publisher = {Mendeleev Communications},
month = {May},
url = {https://mendcomm.colab.ws/publications/10.1070/MC1999v009n03ABEH001058},
number = {3},
pages = {106--108},
doi = {10.1070/MC1999v009n03ABEH001058}
}
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Kostyanovsky, Remir Grigorevich, et al. “3,7-Diazabicyclo[3.3.1]nonane-2,6-diones: building of homo- and heterochiral crystals.” Mendeleev Communications, vol. 9, no. 3, May. 1999, pp. 106-108. https://mendcomm.colab.ws/publications/10.1070/MC1999v009n03ABEH001058.
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Abstract

A strategy in the synthesis of 1,5- or 3,7-unsubstituted derivatives of the title dilactams has been developed, and the parent 3,7-diazabicyclo[3.3.1]nonane-2,6-dione 4 was synthesised; the hydrogen bonding generated self-assembly as a heterochiral infinite diagonal zigzag tape was found in the crystal of 2 (space group P21/c) whereas a homochiral helical architecture was observed in 4 (space group P212121).

References

1.
Kostyanovsky R.G., Lyssenko K.A., Kadorkina G.K., Lebedev O.V., Kravchenko A.N., Chervin I.I., Kostyanovsky V.R.
Mendeleev Communications, 1998
2.
Kostyanovsky R.G., El’natanov Y.I., Krutius O.N., Lyssenko K.A., Strelenko Y.A.
Mendeleev Communications, 1999
3.
Axially chiral dilactams. Synthesis, racemization barriers and crystal structures
Tichý M., Ridvan L., Holý P., Závada J., Cı́sařová I., Podlaha J.
Tetrahedron Asymmetry, 1998
4.
New reactions of 1,3,5- trialkyl-hexahydro-1,3,5-triazines
Darnbrough G., Knowles P., O'Connor S.P., Tierney F.J.
Tetrahedron, 1986
5.
10.1070/MC1999v009n03ABEH001058_bib5
Kostyanovsky
Izv. Akad. Nauk, Ser. Khim., 1996
6.
10.1070/MC1999v009n03ABEH001058_bib6
Kostyanovsky
Izv. Akad. Nauk, Ser. Khim., 1994
7.
Chirality directed self-assembly. Resolution of 2,5-diazabicyclo[2.2.2]octane-3,6-dione and crystal structures of its racemic and (−) enantiomeric forms
Brienne M., Gabard J., Leclercq M., Lehn J., Cesario M., Pascard C., Chevé M., Dutruc-Rosset G.
Tetrahedron Letters, 1994
11.
Conformational dependence and mechanisms for long-range hydrogen-hydrogen coupling constants over four bonds
Barfield M., Dean A.M., Fallick C.J., Spear R.J., Sternhell S., Westerman P.W.
Journal of the American Chemical Society, 1975
12.
10.1070/MC1999v009n03ABEH001058_bib12
Nasakin
Khim. Geterotsikl. Soedin., 1996