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3,7-Diazabicyclo[3.3.0]octane-2,6-diones: synthesis, NMR spectra and structures

Remir Grigorevich Kostyanovsky 1
Remir Grigorevich Kostyanovsky
, 
Yuri Il'ich Èl'natanov 1
Yuri Il'ich Èl'natanov
, 
Oleg Nikolaevich Krutius 1
Oleg Nikolaevich Krutius
, 
Konstantin Alexandrovich Lyssenko 2
Konstantin Alexandrovich Lyssenko
, 
Yurii Andreevich Strelenko 3
Yurii Andreevich Strelenko
10.1070/MC1999v009n02ABEH001042
Published 1999-04-01
Communication , Volume 9, Issue 2, 70-73
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Kostyanovsky R. G. et al. 3,7-Diazabicyclo[3.3.0]octane-2,6-diones: synthesis, NMR spectra and structures // Mendeleev Communications. 1999. Vol. 9. No. 2. pp. 70-73.
GOST all authors (up to 50) Copy
Kostyanovsky R. G., Èl'natanov Y. I., Krutius O. N., Lyssenko K. A., Strelenko Y. A. 3,7-Diazabicyclo[3.3.0]octane-2,6-diones: synthesis, NMR spectra and structures // Mendeleev Communications. 1999. Vol. 9. No. 2. pp. 70-73.
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TY - JOUR
DO - 10.1070/MC1999v009n02ABEH001042
UR - https://mendcomm.colab.ws/publications/10.1070/MC1999v009n02ABEH001042
TI - 3,7-Diazabicyclo[3.3.0]octane-2,6-diones: synthesis, NMR spectra and structures
T2 - Mendeleev Communications
AU - Kostyanovsky, Remir Grigorevich
AU - Èl'natanov, Yuri Il'ich
AU - Krutius, Oleg Nikolaevich
AU - Lyssenko, Konstantin Alexandrovich
AU - Strelenko, Yurii Andreevich
PY - 1999
DA - 1999/04/01
PB - Mendeleev Communications
SP - 70-73
IS - 2
VL - 9
ER -
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@article{1999_Kostyanovsky,
author = {Remir Grigorevich Kostyanovsky and Yuri Il'ich Èl'natanov and Oleg Nikolaevich Krutius and Konstantin Alexandrovich Lyssenko and Yurii Andreevich Strelenko},
title = {3,7-Diazabicyclo[3.3.0]octane-2,6-diones: synthesis, NMR spectra and structures},
journal = {Mendeleev Communications},
year = {1999},
volume = {9},
publisher = {Mendeleev Communications},
month = {Apr},
url = {https://mendcomm.colab.ws/publications/10.1070/MC1999v009n02ABEH001042},
number = {2},
pages = {70--73},
doi = {10.1070/MC1999v009n02ABEH001042}
}
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Kostyanovsky, Remir Grigorevich, et al. “3,7-Diazabicyclo[3.3.0]octane-2,6-diones: synthesis, NMR spectra and structures.” Mendeleev Communications, vol. 9, no. 2, Apr. 1999, pp. 70-73. https://mendcomm.colab.ws/publications/10.1070/MC1999v009n02ABEH001042.

Abstract

Parent 3,7-diazabicyclo[3.3.0]octane-2,6-dione 5, the corresponding 1,5-dicarboxylic acid 4 and esters 3 have been synthesized for the first time; NMR spectra of the compounds were analysed, and the structures of 3b and 5 were studied by X-ray crystallography; hydrogen bonding generates self-assembly in the form of heterochiral infinite diagonal zigzag tape in the crystal of 5, while in the crystal structure of 3b the H-bonded layers consist of homochiral spirals and heterochiral chains.

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