Home / Publications / First representatives of macrocyclic poly(diazene oxide furazans): 3,4:7,8:11,12:15,16-tetrafurazano-1,2,5,6,9,10,13,14-octaazacyclohexadeca-1,3,5,7,9,11,13,15-octaene 1,9- and 1,10-dioxides; 1,5,9,13-tetraoxide and its crystal structure

First representatives of macrocyclic poly(diazene oxide furazans): 3,4:7,8:11,12:15,16-tetrafurazano-1,2,5,6,9,10,13,14-octaazacyclohexadeca-1,3,5,7,9,11,13,15-octaene 1,9- and 1,10-dioxides; 1,5,9,13-tetraoxide and its crystal structure

Vladimir A Eman 1
Vladimir A Eman
, 
Mikhail S Sukhanov 1
Mikhail S Sukhanov
, 
Oleg Vasilevich Lebedev 1
Oleg Vasilevich Lebedev
, 
Lyudmila Valentinovna Batog 1
Lyudmila Valentinovna Batog
, 
Lidia Sergeevna Konstantinova 1
Lidia Sergeevna Konstantinova
, 
Vladimir Yuryevich Rozhkov 1
Vladimir Yuryevich Rozhkov
, 
Marina Olegovna Dekaprilevich 1
Marina Olegovna Dekaprilevich
, 
Yuri Timofeevich Struchkov 2
Yuri Timofeevich Struchkov
, 
Lenor Ivanovich Khmel'nitskii 1
Lenor Ivanovich Khmel'nitskii
10.1070/MC1997v007n01ABEH000672
Published 1997-02-28
Communication , Volume 7, Issue 1, 5-7
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Eman V. A. et al. First representatives of macrocyclic poly(diazene oxide furazans): 3,4:7,8:11,12:15,16-tetrafurazano-1,2,5,6,9,10,13,14-octaazacyclohexadeca-1,3,5,7,9,11,13,15-octaene 1,9- and 1,10-dioxides; 1,5,9,13-tetraoxide and its crystal structure // Mendeleev Communications. 1997. Vol. 7. No. 1. pp. 5-7.
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Eman V. A., Sukhanov M. S., Lebedev O. V., Batog L. V., Konstantinova L. S., Rozhkov V. Y., Dekaprilevich M. O., Struchkov Y. T., Khmel'nitskii L. I. First representatives of macrocyclic poly(diazene oxide furazans): 3,4:7,8:11,12:15,16-tetrafurazano-1,2,5,6,9,10,13,14-octaazacyclohexadeca-1,3,5,7,9,11,13,15-octaene 1,9- and 1,10-dioxides; 1,5,9,13-tetraoxide and its crystal structure // Mendeleev Communications. 1997. Vol. 7. No. 1. pp. 5-7.
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TY - JOUR
DO - 10.1070/MC1997v007n01ABEH000672
UR - https://mendcomm.colab.ws/publications/10.1070/MC1997v007n01ABEH000672
TI - First representatives of macrocyclic poly(diazene oxide furazans): 3,4:7,8:11,12:15,16-tetrafurazano-1,2,5,6,9,10,13,14-octaazacyclohexadeca-1,3,5,7,9,11,13,15-octaene 1,9- and 1,10-dioxides; 1,5,9,13-tetraoxide and its crystal structure
T2 - Mendeleev Communications
AU - Eman, Vladimir A
AU - Sukhanov, Mikhail S
AU - Lebedev, Oleg Vasilevich
AU - Batog, Lyudmila Valentinovna
AU - Konstantinova, Lidia Sergeevna
AU - Rozhkov, Vladimir Yuryevich
AU - Dekaprilevich, Marina Olegovna
AU - Struchkov, Yuri Timofeevich
AU - Khmel'nitskii, Lenor Ivanovich
PY - 1997
DA - 1997/02/28
PB - Mendeleev Communications
SP - 5-7
IS - 1
VL - 7
ER -
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@article{1997_Eman,
author = {Vladimir A Eman and Mikhail S Sukhanov and Oleg Vasilevich Lebedev and Lyudmila Valentinovna Batog and Lidia Sergeevna Konstantinova and Vladimir Yuryevich Rozhkov and Marina Olegovna Dekaprilevich and Yuri Timofeevich Struchkov and Lenor Ivanovich Khmel'nitskii},
title = {First representatives of macrocyclic poly(diazene oxide furazans): 3,4:7,8:11,12:15,16-tetrafurazano-1,2,5,6,9,10,13,14-octaazacyclohexadeca-1,3,5,7,9,11,13,15-octaene 1,9- and 1,10-dioxides; 1,5,9,13-tetraoxide and its crystal structure},
journal = {Mendeleev Communications},
year = {1997},
volume = {7},
publisher = {Mendeleev Communications},
month = {Feb},
url = {https://mendcomm.colab.ws/publications/10.1070/MC1997v007n01ABEH000672},
number = {1},
pages = {5--7},
doi = {10.1070/MC1997v007n01ABEH000672}
}
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Eman, Vladimir A., et al. “First representatives of macrocyclic poly(diazene oxide furazans): 3,4:7,8:11,12:15,16-tetrafurazano-1,2,5,6,9,10,13,14-octaazacyclohexadeca-1,3,5,7,9,11,13,15-octaene 1,9- and 1,10-dioxides; 1,5,9,13-tetraoxide and its crystal structure.” Mendeleev Communications, vol. 7, no. 1, Feb. 1997, pp. 5-7. https://mendcomm.colab.ws/publications/10.1070/MC1997v007n01ABEH000672.

Abstract

Macrocyclic poly(diazene oxide furazans) have been synthesised for the first time: the tetraoxide was prepared by the oxidation of diazene fragments in the tetradiazenofurazan macrocycle, and the dioxides were synthesised by the intramolecular and intermolecular oxidative cyclisation of structures already containing diazene oxide fragments. The structure of the tetraoxide derivative has been established by X-ray diffraction analysis.

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