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Synthesis of [1,2,5]Oxadiazolo[3,4-e][1,2,3,4]tetrazine 4,6-Di-N-oxide

Aleksandr Mikhailovich Churakov 1
Aleksandr Mikhailovich Churakov
, 
Sema Leibovich Ioffe 1
Sema Leibovich Ioffe
, 
Vladimir Alexandrovich Tartakovsky 1
Vladimir Alexandrovich Tartakovsky
10.1070/MC1995v005n06ABEH000539
Published 1995-12-31
Communication , Volume 5, Issue 6, 227-228
70
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Churakov A. M., Ioffe S. L., Tartakovsky V. A. Synthesis of [1,2,5]Oxadiazolo[3,4-e][1,2,3,4]tetrazine 4,6-Di-N-oxide // Mendeleev Communications. 1995. Vol. 5. No. 6. pp. 227-228.
GOST all authors (up to 50) Copy
Churakov A. M., Ioffe S. L., Tartakovsky V. A. Synthesis of [1,2,5]Oxadiazolo[3,4-e][1,2,3,4]tetrazine 4,6-Di-N-oxide // Mendeleev Communications. 1995. Vol. 5. No. 6. pp. 227-228.
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TY - JOUR
DO - 10.1070/MC1995v005n06ABEH000539
UR - https://mendcomm.colab.ws/publications/10.1070/MC1995v005n06ABEH000539
TI - Synthesis of [1,2,5]Oxadiazolo[3,4-e][1,2,3,4]tetrazine 4,6-Di-N-oxide
T2 - Mendeleev Communications
AU - Churakov, Aleksandr Mikhailovich
AU - Ioffe, Sema Leibovich
AU - Tartakovsky, Vladimir Alexandrovich
PY - 1995
DA - 1995/12/31
PB - Mendeleev Communications
SP - 227-228
IS - 6
VL - 5
ER -
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@article{1995_Churakov,
author = {Aleksandr Mikhailovich Churakov and Sema Leibovich Ioffe and Vladimir Alexandrovich Tartakovsky},
title = {Synthesis of [1,2,5]Oxadiazolo[3,4-e][1,2,3,4]tetrazine 4,6-Di-N-oxide},
journal = {Mendeleev Communications},
year = {1995},
volume = {5},
publisher = {Mendeleev Communications},
month = {Dec},
url = {https://mendcomm.colab.ws/publications/10.1070/MC1995v005n06ABEH000539},
number = {6},
pages = {227--228},
doi = {10.1070/MC1995v005n06ABEH000539}
}
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Churakov, Aleksandr Mikhailovich, et al. “Synthesis of [1,2,5]Oxadiazolo[3,4-e][1,2,3,4]tetrazine 4,6-Di-N-oxide.” Mendeleev Communications, vol. 5, no. 6, Dec. 1995, pp. 227-228. https://mendcomm.colab.ws/publications/10.1070/MC1995v005n06ABEH000539.

Abstract

Treatment of 3-amino-4-(tert-butyl)azoxyfurazan with NO2BF4 in MeCN gives [1,2,5]oxadiazolo[3,4-e][1,2,3,4]tetrazine 4,6-di-N-oxide 2; 15N labelling experiments allowed the spectra of 2 to be fully assigned and provided support for the proposed structure. Diazonium oxide cation is proposed as the intermediate in ring closure.

References

1.
Churakov A.M., Ioffe S.L., Tartakovskii V.A.
Mendeleev Communications, 1991
2.
Churakov A.M., Semenov S.E., loffe S.L., Strelenko Y.A., Tartakovskii V.A.
Mendeleev Communications, 1995
3.
Lead tetraacetate oxidation of 1- and 2-amino-5-phenyl[1,2,3]triazolo[4,5-d][1,2,3]triazoles; synthesis of a fused 1,2,3,4-tetrazine
Kaihoh T., Itoh T., Yamaguchi K., Ohsawa A.
Journal of the Chemical Society Perkin Transactions 1, 1991
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Rezchikova K.I., Churakov A.M., Shlyapochnikov V.A., Tartakovskii V.A.
Mendeleev Communications, 1995
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10.1070/MC1995v005n06ABEH000539_bib5
Solodyuk
Zh. Org. Khim., 1981