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Functionalization of the Aliphatic Chain in 4-Nitro-N,N-diethylaniline: Direct Tri-fluoroacetylation of the β-Carbon Atom

Nikolai Vladilenovich Moskalev ¹

Nikolai Vladilenovich Moskalev

Vladimir D Ogorodnikov ²

Vladimir D Ogorodnikov

¹ Department of Chemistry, Tomsk Polytechnical University, Tomsk, Russian Federation

² Institute of Petroleum Chemistry, Siberian Branch of the Russian Academy of Sciences, Tomsk, Russian Federation

10.1070/MC1995v005n05ABEH000523

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Published 1995-10-30

Communication , Volume 5, Issue 5, 197-198

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Moskalev N. V., Ogorodnikov V. D. Functionalization of the Aliphatic Chain in 4-Nitro-N,N-diethylaniline: Direct Tri-fluoroacetylation of the β-Carbon Atom // Mendeleev Communications. 1995. Vol. 5. No. 5. pp. 197-198.

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TY - JOUR

DO - 10.1070/MC1995v005n05ABEH000523

UR - https://mendcomm.colab.ws/publications/10.1070/MC1995v005n05ABEH000523

TI - Functionalization of the Aliphatic Chain in 4-Nitro-N,N-diethylaniline: Direct Tri-fluoroacetylation of the β-Carbon Atom

T2 - Mendeleev Communications

AU - Moskalev, Nikolai Vladilenovich

AU - Ogorodnikov, Vladimir D

PY - 1995

DA - 1995/10/30

PB - Mendeleev Communications

SP - 197-198

IS - 5

VL - 5

ER -

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@article{1995_Moskalev,

author = {Nikolai Vladilenovich Moskalev and Vladimir D Ogorodnikov},

title = {Functionalization of the Aliphatic Chain in 4-Nitro-N,N-diethylaniline: Direct Tri-fluoroacetylation of the β-Carbon Atom},

journal = {Mendeleev Communications},

year = {1995},

volume = {5},

publisher = {Mendeleev Communications},

month = {Oct},

url = {https://mendcomm.colab.ws/publications/10.1070/MC1995v005n05ABEH000523},

number = {5},

pages = {197--198},

doi = {10.1070/MC1995v005n05ABEH000523}

}

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Moskalev, Nikolai Vladilenovich, and Vladimir D Ogorodnikov. “Functionalization of the Aliphatic Chain in 4-Nitro-N,N-diethylaniline: Direct Tri-fluoroacetylation of the β-Carbon Atom.” Mendeleev Communications, vol. 5, no. 5, Oct. 1995, pp. 197-198. https://mendcomm.colab.ws/publications/10.1070/MC1995v005n05ABEH000523.

Abstract

Treatment of 4-nitro-N,N-diethylaniline 1 with trifluoroacetic anhydride 2 at 120°C unexpectedly gives trans-1,1,1-trifluoro-4-[N-ethyl-N-(4-nitrophenylamino)]but-3-en-2-one 3 in good yield.