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Synthesis and Structure of (22R,24R)-6β-Acetoxy-24-methyl-5α-cholestane-3β,5α,22,24-tetrol

Raisa Pavlovna Litvinovskaya 1
Raisa Pavlovna Litvinovskaya
, 
Aleksander Vyacheslavovich Baranovskii 1
Aleksander Vyacheslavovich Baranovskii
, 
Vladimir Aleksandrovich Khripach 1
Vladimir Aleksandrovich Khripach
, 
Yurii E Ovchinnikov 2
Yurii E Ovchinnikov
, 
Yuri Timofeevich Struchkov 2
Yuri Timofeevich Struchkov
10.1070/MC1994v004n03ABEH000361
Published 1994-06-30
Communication , Volume 4, Issue 3, 89-90
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Litvinovskaya R. P. et al. Synthesis and Structure of (22R,24R)-6β-Acetoxy-24-methyl-5α-cholestane-3β,5α,22,24-tetrol // Mendeleev Communications. 1994. Vol. 4. No. 3. pp. 89-90.
GOST all authors (up to 50) Copy
Litvinovskaya R. P., Baranovskii A. V., Khripach V. A., Ovchinnikov Y. E., Struchkov Y. T. Synthesis and Structure of (22R,24R)-6β-Acetoxy-24-methyl-5α-cholestane-3β,5α,22,24-tetrol // Mendeleev Communications. 1994. Vol. 4. No. 3. pp. 89-90.
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TY - JOUR
DO - 10.1070/MC1994v004n03ABEH000361
UR - https://mendcomm.colab.ws/publications/10.1070/MC1994v004n03ABEH000361
TI - Synthesis and Structure of (22R,24R)-6β-Acetoxy-24-methyl-5α-cholestane-3β,5α,22,24-tetrol
T2 - Mendeleev Communications
AU - Litvinovskaya, Raisa Pavlovna
AU - Baranovskii, Aleksander Vyacheslavovich
AU - Khripach, Vladimir Aleksandrovich
AU - Ovchinnikov, Yurii E
AU - Struchkov, Yuri Timofeevich
PY - 1994
DA - 1994/06/30
PB - Mendeleev Communications
SP - 89-90
IS - 3
VL - 4
ER -
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@article{1994_Litvinovskaya,
author = {Raisa Pavlovna Litvinovskaya and Aleksander Vyacheslavovich Baranovskii and Vladimir Aleksandrovich Khripach and Yurii E Ovchinnikov and Yuri Timofeevich Struchkov},
title = {Synthesis and Structure of (22R,24R)-6β-Acetoxy-24-methyl-5α-cholestane-3β,5α,22,24-tetrol},
journal = {Mendeleev Communications},
year = {1994},
volume = {4},
publisher = {Mendeleev Communications},
month = {Jun},
url = {https://mendcomm.colab.ws/publications/10.1070/MC1994v004n03ABEH000361},
number = {3},
pages = {89--90},
doi = {10.1070/MC1994v004n03ABEH000361}
}
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Litvinovskaya, Raisa Pavlovna, et al. “Synthesis and Structure of (22R,24R)-6β-Acetoxy-24-methyl-5α-cholestane-3β,5α,22,24-tetrol.” Mendeleev Communications, vol. 4, no. 3, Jun. 1994, pp. 89-90. https://mendcomm.colab.ws/publications/10.1070/MC1994v004n03ABEH000361.

Abstract

The title compound 1 has been synthesized for the first time from 20-isoxazolinylsteroid 2 via 5α,6α-epoxide 3 whose stereochemistry has been firmly established by an X-ray crystallographic analysis.

References

2.
10.1070/MC1994v004n03ABEH000361_bib2_1
Khripach
Dokl. Akad. Nauk SSSR, 1991
3.
10.1070/MC1994v004n03ABEH000361_bib2_2
Khripach
Khim. Prir. Soedin., 1992
4.
Khripach V.V., Litvinovskaya R.P., Baranovskii A.V.
Mendeleev Communications, 1992