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Synthesis and Properties of 2,3-Dimethoxy-1,4,2,3-dioxadiazinane and Dialkoxydiazene Oxides

Vladimir Fedorovich Rudchenko 1
Vladimir Fedorovich Rudchenko
, 
Sergei Mikhailovich Ignatov 1
Sergei Mikhailovich Ignatov
, 
Ivan Ivanovich Chervin 1
Ivan Ivanovich Chervin
, 
Abil E Aliev 1
Abil E Aliev
, 
Remir Grigorevich Kostyanovsky 1
Remir Grigorevich Kostyanovsky
10.1070/MC1992v002n02ABEH000125
Published 1992-06-30
Communication , Volume 2, Issue 2, 50-51
4
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Rudchenko V. F. et al. Synthesis and Properties of 2,3-Dimethoxy-1,4,2,3-dioxadiazinane and Dialkoxydiazene Oxides // Mendeleev Communications. 1992. Vol. 2. No. 2. pp. 50-51.
GOST all authors (up to 50) Copy
Rudchenko V. F., Ignatov S. M., Chervin I. I., Aliev A. E., Kostyanovsky R. G. Synthesis and Properties of 2,3-Dimethoxy-1,4,2,3-dioxadiazinane and Dialkoxydiazene Oxides // Mendeleev Communications. 1992. Vol. 2. No. 2. pp. 50-51.
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TY - JOUR
DO - 10.1070/MC1992v002n02ABEH000125
UR - https://mendcomm.colab.ws/publications/10.1070/MC1992v002n02ABEH000125
TI - Synthesis and Properties of 2,3-Dimethoxy-1,4,2,3-dioxadiazinane and Dialkoxydiazene Oxides
T2 - Mendeleev Communications
AU - Rudchenko, Vladimir Fedorovich
AU - Ignatov, Sergei Mikhailovich
AU - Chervin, Ivan Ivanovich
AU - Aliev, Abil E
AU - Kostyanovsky, Remir Grigorevich
PY - 1992
DA - 1992/06/30
PB - Mendeleev Communications
SP - 50-51
IS - 2
VL - 2
ER -
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@article{1992_Rudchenko,
author = {Vladimir Fedorovich Rudchenko and Sergei Mikhailovich Ignatov and Ivan Ivanovich Chervin and Abil E Aliev and Remir Grigorevich Kostyanovsky},
title = {Synthesis and Properties of 2,3-Dimethoxy-1,4,2,3-dioxadiazinane and Dialkoxydiazene Oxides},
journal = {Mendeleev Communications},
year = {1992},
volume = {2},
publisher = {Mendeleev Communications},
month = {Jun},
url = {https://mendcomm.colab.ws/publications/10.1070/MC1992v002n02ABEH000125},
number = {2},
pages = {50--51},
doi = {10.1070/MC1992v002n02ABEH000125}
}
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Rudchenko, Vladimir Fedorovich, et al. “Synthesis and Properties of 2,3-Dimethoxy-1,4,2,3-dioxadiazinane and Dialkoxydiazene Oxides.” Mendeleev Communications, vol. 2, no. 2, Jun. 1992, pp. 50-51. https://mendcomm.colab.ws/publications/10.1070/MC1992v002n02ABEH000125.

Abstract

The oxidation of 1,2-bis(methoxyaminooxy)ethane 1 with PbO2 results in the formation of 2,3-dimetboxy-1,4,2,3-dioxadiazinane 2 as a mixture of trans- and cis-isomers (55:45), the regio- and stereo-specific reaction of which with p-nitrobenzoic acid gives (E)-dialkoxydiazene oxide 3 and methyl p-nitrobenzoate.

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