Home / Publications / Synthesis of 3,4-Dihydro-1,2-diazete 1,2-Dioxides based on 1,2-Bishydroxylamines and 1,2-Nitroso Oxime

Synthesis of 3,4-Dihydro-1,2-diazete 1,2-Dioxides based on 1,2-Bishydroxylamines and 1,2-Nitroso Oxime

Dmitrii Gennad'evich Mazhukin 1
Dmitrii Gennad'evich Mazhukin
, 
Leonid Borisovich Volodarsky 1
Leonid Borisovich Volodarsky
, 
Lidiya Adol'fovna Tikhonova 1
Lidiya Adol'fovna Tikhonova
, 
Aleksei Ya Tikhonov 1
Aleksei Ya Tikhonov
10.1070/MC1992v002n01ABEH000111
Published 1992-03-31
Communication , Volume 2, Issue 1, 29-30
6
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Mazhukin D. G. et al. Synthesis of 3,4-Dihydro-1,2-diazete 1,2-Dioxides based on 1,2-Bishydroxylamines and 1,2-Nitroso Oxime // Mendeleev Communications. 1992. Vol. 2. No. 1. pp. 29-30.
GOST all authors (up to 50) Copy
Mazhukin D. G., Volodarsky L. B., Tikhonova L. A., Tikhonov A. Ya. Synthesis of 3,4-Dihydro-1,2-diazete 1,2-Dioxides based on 1,2-Bishydroxylamines and 1,2-Nitroso Oxime // Mendeleev Communications. 1992. Vol. 2. No. 1. pp. 29-30.
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TY - JOUR
DO - 10.1070/MC1992v002n01ABEH000111
UR - https://mendcomm.colab.ws/publications/10.1070/MC1992v002n01ABEH000111
TI - Synthesis of 3,4-Dihydro-1,2-diazete 1,2-Dioxides based on 1,2-Bishydroxylamines and 1,2-Nitroso Oxime
T2 - Mendeleev Communications
AU - Mazhukin, Dmitrii Gennad'evich
AU - Volodarsky, Leonid Borisovich
AU - Tikhonova, Lidiya Adol'fovna
AU - Tikhonov, Aleksei Ya
PY - 1992
DA - 1992/03/31
PB - Mendeleev Communications
SP - 29-30
IS - 1
VL - 2
ER -
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@article{1992_Mazhukin,
author = {Dmitrii Gennad'evich Mazhukin and Leonid Borisovich Volodarsky and Lidiya Adol'fovna Tikhonova and Aleksei Ya Tikhonov},
title = {Synthesis of 3,4-Dihydro-1,2-diazete 1,2-Dioxides based on 1,2-Bishydroxylamines and 1,2-Nitroso Oxime},
journal = {Mendeleev Communications},
year = {1992},
volume = {2},
publisher = {Mendeleev Communications},
month = {Mar},
url = {https://mendcomm.colab.ws/publications/10.1070/MC1992v002n01ABEH000111},
number = {1},
pages = {29--30},
doi = {10.1070/MC1992v002n01ABEH000111}
}
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Mazhukin, Dmitrii Gennad'evich, et al. “Synthesis of 3,4-Dihydro-1,2-diazete 1,2-Dioxides based on 1,2-Bishydroxylamines and 1,2-Nitroso Oxime.” Mendeleev Communications, vol. 2, no. 1, Mar. 1992, pp. 29-30. https://mendcomm.colab.ws/publications/10.1070/MC1992v002n01ABEH000111.

Abstract

Oxidation of 1,2-bishydroxylamines having one or two hydroxylamino groups at a secondary carbon atom(s), by sodium hypobromite, leads to 3,4-dihydro-1,2-diazete 1,2-dioxides; treatment of 1,2-nitroso oxime with nitric acid or N2O4 gives 3,4-dihydro-3-nitro-1,2-diazete 1,2-dioxide.

References

1.
3,3,4,4-Tetramethyl-1,2-diazetine 1,2-dioxide, a useful low-energy triplet quencher
Ullman E.F., Singh P.
Journal of the American Chemical Society, 1972
2.
Decomposition of meso- and dl-3,4-diethyl-3,4-dimethyldiazetine (a 1,2-diaza-1-cyclobutene)
White D.K., Greene F.D.
Journal of the American Chemical Society, 1978
3.
10.1070/MC1992v002n01ABEH000111_bib3
Volodarskii
Khim. Geterotsikl. Soedin., 1975
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10.1070/MC1992v002n01ABEH000111_bib4
Shustov
Izv. Akad. Nauk SSSR, Ser. Khim., 1982
5.
J. H. Boyer, in The chemistry of the nitro and nitroso groups. Part 1, ed. H. Feuer, Interscience, New York, London, 1969, p. 255.