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Cyclopropanation of Unsaturated Compounds with Diazomethane Generated in situ: A New Efficient and Practical Route to Cyclopropane Derivatives

Oleg Matveevich Nefedov 1
Oleg Matveevich Nefedov
,  , 
Andrei B Kostitsyn 1
Andrei B Kostitsyn
,  , 
Vladimir Anatol'evich Dokitchev 3
Vladimir Anatol'evich Dokitchev
10.1070/MC1992v002n01ABEH000099
Published 1992-03-31
Communication , Volume 2, Issue 1, 13-15
27
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Nefedov O. M. et al. Cyclopropanation of Unsaturated Compounds with Diazomethane Generated in situ: A New Efficient and Practical Route to Cyclopropane Derivatives // Mendeleev Communications. 1992. Vol. 2. No. 1. pp. 13-15.
GOST all authors (up to 50) Copy
Nefedov O. M., Tomilov Y. V., Kostitsyn A. B., Dzhemilev U. M., Dokitchev V. A. Cyclopropanation of Unsaturated Compounds with Diazomethane Generated in situ: A New Efficient and Practical Route to Cyclopropane Derivatives // Mendeleev Communications. 1992. Vol. 2. No. 1. pp. 13-15.
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TY - JOUR
DO - 10.1070/MC1992v002n01ABEH000099
UR - https://mendcomm.colab.ws/publications/10.1070/MC1992v002n01ABEH000099
TI - Cyclopropanation of Unsaturated Compounds with Diazomethane Generated in situ: A New Efficient and Practical Route to Cyclopropane Derivatives
T2 - Mendeleev Communications
AU - Nefedov, Oleg Matveevich
AU - Tomilov, Yury Vasil'evich
AU - Kostitsyn, Andrei B
AU - Dzhemilev, Usein Memetovich
AU - Dokitchev, Vladimir Anatol'evich
PY - 1992
DA - 1992/03/31
PB - Mendeleev Communications
SP - 13-15
IS - 1
VL - 2
ER -
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@article{1992_Nefedov,
author = {Oleg Matveevich Nefedov and Yury Vasil'evich Tomilov and Andrei B Kostitsyn and Usein Memetovich Dzhemilev and Vladimir Anatol'evich Dokitchev},
title = {Cyclopropanation of Unsaturated Compounds with Diazomethane Generated in situ: A New Efficient and Practical Route to Cyclopropane Derivatives},
journal = {Mendeleev Communications},
year = {1992},
volume = {2},
publisher = {Mendeleev Communications},
month = {Mar},
url = {https://mendcomm.colab.ws/publications/10.1070/MC1992v002n01ABEH000099},
number = {1},
pages = {13--15},
doi = {10.1070/MC1992v002n01ABEH000099}
}
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Nefedov, Oleg Matveevich, et al. “Cyclopropanation of Unsaturated Compounds with Diazomethane Generated in situ: A New Efficient and Practical Route to Cyclopropane Derivatives.” Mendeleev Communications, vol. 2, no. 1, Mar. 1992, pp. 13-15. https://mendcomm.colab.ws/publications/10.1070/MC1992v002n01ABEH000099.

Abstract

The synthesis of the title compounds is easily achieved by the Pd-catalysed cyclopropanation of unsaturated compounds with diazomethane generated in situ from N-methyl-N-nitrosourea–KOH in CH2Cl2–Et2O.

References

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10.1070/MC1992v002n01ABEH000099_bib1
Maas
Top. Curr. Chem., 1987
2.
10.1070/MC1992v002n01ABEH000099_bib2_1
Tomilov
Izv. Akad. Nauk SSSR, Ser. Khim., 1984
3.
10.1070/MC1992v002n01ABEH000099_bib2_2
Dzhemilev
Izv. Akad. Nauk SSSR, Ser. Khim., 1989
4.
10.1070/MC1992v002n01ABEH000099_bib3
Regitz
Diazo Compounds. Properties and Synthesis, 1986