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Cyclopropanation of Unsaturated Compounds with Diazomethane Generated in situ: A New Efficient and Practical Route to Cyclopropane Derivatives

Oleg Matveevich Nefedov 1
Oleg Matveevich Nefedov
,  , 
Andrei B Kostitsyn 1
Andrei B Kostitsyn
,  , 
Vladimir Anatol'evich Dokitchev 3
Vladimir Anatol'evich Dokitchev
10.1070/MC1992v002n01ABEH000099
Published 1992-03-31
Communication , Volume 2, Issue 1, 13-15
29
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Nefedov O. M. et al. Cyclopropanation of Unsaturated Compounds with Diazomethane Generated in situ: A New Efficient and Practical Route to Cyclopropane Derivatives // Mendeleev Communications. 1992. Vol. 2. No. 1. pp. 13-15.
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Nefedov O. M., Tomilov Y. V., Kostitsyn A. B., Dzhemilev U. M., Dokitchev V. A. Cyclopropanation of Unsaturated Compounds with Diazomethane Generated in situ: A New Efficient and Practical Route to Cyclopropane Derivatives // Mendeleev Communications. 1992. Vol. 2. No. 1. pp. 13-15.
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TY - JOUR
DO - 10.1070/MC1992v002n01ABEH000099
UR - https://mendcomm.colab.ws/publications/10.1070/MC1992v002n01ABEH000099
TI - Cyclopropanation of Unsaturated Compounds with Diazomethane Generated in situ: A New Efficient and Practical Route to Cyclopropane Derivatives
T2 - Mendeleev Communications
AU - Nefedov, Oleg Matveevich
AU - Tomilov, Yury Vasil'evich
AU - Kostitsyn, Andrei B
AU - Dzhemilev, Usein Memetovich
AU - Dokitchev, Vladimir Anatol'evich
PY - 1992
DA - 1992/03/31
PB - Mendeleev Communications
SP - 13-15
IS - 1
VL - 2
ER -
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@article{1992_Nefedov,
author = {Oleg Matveevich Nefedov and Yury Vasil'evich Tomilov and Andrei B Kostitsyn and Usein Memetovich Dzhemilev and Vladimir Anatol'evich Dokitchev},
title = {Cyclopropanation of Unsaturated Compounds with Diazomethane Generated in situ: A New Efficient and Practical Route to Cyclopropane Derivatives},
journal = {Mendeleev Communications},
year = {1992},
volume = {2},
publisher = {Mendeleev Communications},
month = {Mar},
url = {https://mendcomm.colab.ws/publications/10.1070/MC1992v002n01ABEH000099},
number = {1},
pages = {13--15},
doi = {10.1070/MC1992v002n01ABEH000099}
}
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Nefedov, Oleg Matveevich, et al. “Cyclopropanation of Unsaturated Compounds with Diazomethane Generated in situ: A New Efficient and Practical Route to Cyclopropane Derivatives.” Mendeleev Communications, vol. 2, no. 1, Mar. 1992, pp. 13-15. https://mendcomm.colab.ws/publications/10.1070/MC1992v002n01ABEH000099.
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Abstract

The synthesis of the title compounds is easily achieved by the Pd-catalysed cyclopropanation of unsaturated compounds with diazomethane generated in situ from N-methyl-N-nitrosourea–KOH in CH2Cl2–Et2O.

References

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10.1070/MC1992v002n01ABEH000099_bib1
Maas
Top. Curr. Chem., 1987
2.
10.1070/MC1992v002n01ABEH000099_bib2_1
Tomilov
Izv. Akad. Nauk SSSR, Ser. Khim., 1984
3.
10.1070/MC1992v002n01ABEH000099_bib2_2
Dzhemilev
Izv. Akad. Nauk SSSR, Ser. Khim., 1989
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10.1070/MC1992v002n01ABEH000099_bib3
Regitz
Diazo Compounds. Properties and Synthesis, 1986