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Synthesis and Molecular Structure of 1,5-Dimethyl-3,7-di-tert-butyl-3,7-diazabicyclo[3.3.1]nonan-9-one

Konstantin Albertovich Potekhin 1
Konstantin Albertovich Potekhin
, 
Olga Ivanovna Levina 1
Olga Ivanovna Levina
, 
Yuri Timofeevich Struchkov 2
Yuri Timofeevich Struchkov
, 
Anna Mikhailovna Svetlanova 1
Anna Mikhailovna Svetlanova
, 
Roza S Idrisova 1
Roza S Idrisova
, 
Vladimir Alexandrovich Palyulin 1
Vladimir Alexandrovich Palyulin
, 
Nikolai Serafimovich Zefirov 1
Nikolai Serafimovich Zefirov
10.1070/MC1991v001n03ABEH000053
Published 1991-09-30
Communication , Volume 1, Issue 3, 87-88
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Potekhin K. A. et al. Synthesis and Molecular Structure of 1,5-Dimethyl-3,7-di-tert-butyl-3,7-diazabicyclo[3.3.1]nonan-9-one // Mendeleev Communications. 1991. Vol. 1. No. 3. pp. 87-88.
GOST all authors (up to 50) Copy
Potekhin K. A., Levina O. I., Struchkov Y. T., Svetlanova A. M., Idrisova R. S., Palyulin V. A., Zefirov N. S. Synthesis and Molecular Structure of 1,5-Dimethyl-3,7-di-tert-butyl-3,7-diazabicyclo[3.3.1]nonan-9-one // Mendeleev Communications. 1991. Vol. 1. No. 3. pp. 87-88.
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TY - JOUR
DO - 10.1070/MC1991v001n03ABEH000053
UR - https://mendcomm.colab.ws/publications/10.1070/MC1991v001n03ABEH000053
TI - Synthesis and Molecular Structure of 1,5-Dimethyl-3,7-di-tert-butyl-3,7-diazabicyclo[3.3.1]nonan-9-one
T2 - Mendeleev Communications
AU - Potekhin, Konstantin Albertovich
AU - Levina, Olga Ivanovna
AU - Struchkov, Yuri Timofeevich
AU - Svetlanova, Anna Mikhailovna
AU - Idrisova, Roza S
AU - Palyulin, Vladimir Alexandrovich
AU - Zefirov, Nikolai Serafimovich
PY - 1991
DA - 1991/09/30
PB - Mendeleev Communications
SP - 87-88
IS - 3
VL - 1
ER -
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@article{1991_Potekhin,
author = {Konstantin Albertovich Potekhin and Olga Ivanovna Levina and Yuri Timofeevich Struchkov and Anna Mikhailovna Svetlanova and Roza S Idrisova and Vladimir Alexandrovich Palyulin and Nikolai Serafimovich Zefirov},
title = {Synthesis and Molecular Structure of 1,5-Dimethyl-3,7-di-tert-butyl-3,7-diazabicyclo[3.3.1]nonan-9-one},
journal = {Mendeleev Communications},
year = {1991},
volume = {1},
publisher = {Mendeleev Communications},
month = {Sep},
url = {https://mendcomm.colab.ws/publications/10.1070/MC1991v001n03ABEH000053},
number = {3},
pages = {87--88},
doi = {10.1070/MC1991v001n03ABEH000053}
}
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Potekhin, Konstantin Albertovich, et al. “Synthesis and Molecular Structure of 1,5-Dimethyl-3,7-di-tert-butyl-3,7-diazabicyclo[3.3.1]nonan-9-one.” Mendeleev Communications, vol. 1, no. 3, Sep. 1991, pp. 87-88. https://mendcomm.colab.ws/publications/10.1070/MC1991v001n03ABEH000053.

Abstract

X-Ray analysis of 1,5-dimethyl-3,7-di-tert-butyl-3,7-diazabicyclo[3.3.1]nonan-9-one 5 has established that its molecules adopt a chair–boat conformation; compound 5 has been synthesized in one step using a Mannich condensation.

References

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Cryst. Struct. Commun., 1982
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Cryst. Struct. Commun., 1982
4.
Structure of 3-benzyl-7-methyl-3,7-diazabicyclo[3.3.1]nonan-9-one, C15H20N2O
Smith-Verdier P., Florencio F., García-Blanco S.
Acta Crystallographica Section C Crystal Structure Communications, 1983
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Conformational control in the 3,7-diazbicyclo[3.3.1]nonane system
McCabe P.H., Milne N.J., Sim G.A.
Journal of the Chemical Society Chemical Communications, 1985
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10.1070/MC1991v001n03ABEH000053_bib6
Levina
Dokl. Akad. Nauk SSSR, 1985