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Crystallization behavior of fluorozirconate glasses as monitored by 35Cl NMR

Andrei Andreevich Gippius 1, 2
Andrei Andreevich Gippius
, 
Aleksei Vladimirovich Tkachev 1
Aleksei Vladimirovich Tkachev
, 
Eleonora Aleksandrovna Kravchenko 3
Eleonora Aleksandrovna Kravchenko
, 
Leonid Aleksandrovich Vaimugin 3
Leonid Aleksandrovich Vaimugin
, 
Liudmila Victorovna Moiseeva 4
Liudmila Victorovna Moiseeva
, 
1 P.N. Lebedev Physical Institute, Russian Academy of Sciences, Moscow, Russian Federation
2 Department of Physics, M.V. Lomonosov Moscow State University, Moscow, Russian Federation
4 Prokhorov General Physics Institute, Russian Academy of Sciences, Moscow, Russian Federation
10.1016/j.mencom.2024.10.042
Published 2024-10-22
Communication , Volume 34, Issue 6, 902-904
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Gippius A. A. et al. Crystallization behavior of fluorozirconate glasses as monitored by 35Cl NMR // Mendeleev Communications. 2024. Vol. 34. No. 6. pp. 902-904.
GOST all authors (up to 50) Copy
Gippius A. A., Tkachev A. V., Kravchenko E. A., Vaimugin L. A., Moiseeva L. V., Brekhovskikh M. N. Crystallization behavior of fluorozirconate glasses as monitored by 35Cl NMR // Mendeleev Communications. 2024. Vol. 34. No. 6. pp. 902-904.
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TY - JOUR
DO - 10.1016/j.mencom.2024.10.042
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2024.10.042
TI - Crystallization behavior of fluorozirconate glasses as monitored by 35Cl NMR
T2 - Mendeleev Communications
AU - Gippius, Andrei Andreevich
AU - Tkachev, Aleksei Vladimirovich
AU - Kravchenko, Eleonora Aleksandrovna
AU - Vaimugin, Leonid Aleksandrovich
AU - Moiseeva, Liudmila Victorovna
AU - Brekhovskikh, Maria Nikolaevna
PY - 2024
DA - 2024/10/22
PB - Mendeleev Communications
SP - 902-904
IS - 6
VL - 34
ER -
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@article{2024_Gippius,
author = {Andrei Andreevich Gippius and Aleksei Vladimirovich Tkachev and Eleonora Aleksandrovna Kravchenko and Leonid Aleksandrovich Vaimugin and Liudmila Victorovna Moiseeva and Maria Nikolaevna Brekhovskikh},
title = {Crystallization behavior of fluorozirconate glasses as monitored by 35Cl NMR},
journal = {Mendeleev Communications},
year = {2024},
volume = {34},
publisher = {Mendeleev Communications},
month = {Oct},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2024.10.042},
number = {6},
pages = {902--904},
doi = {10.1016/j.mencom.2024.10.042}
}
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Gippius, Andrei Andreevich, et al. “Crystallization behavior of fluorozirconate glasses as monitored by 35Cl NMR.” Mendeleev Communications, vol. 34, no. 6, Oct. 2024, pp. 902-904. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2024.10.042.

Keywords

35Cl NMR spectroscopy
composition modification
crystallization
fluorozirconate glass
glass ceramics
magnetic centers.

Abstract

The 35Cl nuclear magnetic resonance (NMR) spectroscopy was first used to study the crystallization of erbium-doped fluorochlorozirconate glass in the ZrF4-BaF2-BaCl2-LaF3-AlF3-NaF system. It has been shown that crystallization results in the increasing homogeneity of electronic structure on chlorine atoms and a narrowing of the NMR line. The glass being crystallized, erbium cations are displaced into the fluoride phase.

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