Synthesis of ferrierite-type zeolite by microwave method using ethylenediamine as an organic structure-directing agent

Makova, Anna S; Kustov, Aleksandr Leonidovich; Davshan, Nikolay Alekseevich; Mishin, Igor Vladimirovich; Kalmykov, Konstantin Borisovich; Shesterkina, Anastasiya Alekseevna; Kustov, Leonid Modestovich

doi:10.1016/j.mencom.2023.06.028

Home / Publications / Synthesis of ferrierite-type zeolite by microwave method using ethylenediamine as an organic structure-directing agent

Synthesis of ferrierite-type zeolite by microwave method using ethylenediamine as an organic structure-directing agent

Anna S Makova ^{1, 2}

Anna S Makova

,

Aleksandr Leonidovich Kustov ^{1, 2, 3}

Aleksandr Leonidovich Kustov

,

Nikolay Alekseevich Davshan ¹

Nikolay Alekseevich Davshan

0009-0004-2120-6953

,

Igor Vladimirovich Mishin ¹

Igor Vladimirovich Mishin

,

Konstantin Borisovich Kalmykov ³

Konstantin Borisovich Kalmykov

,

Anastasiya Alekseevna Shesterkina ^{1, 2, 3}

Anastasiya Alekseevna Shesterkina

0000-0002-9961-7515

,

Leonid Modestovich Kustov ^{1, 2, 3}

Leonid Modestovich Kustov

0000-0003-2312-3583

¹ N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russian Federation

² National University of Science and Technology 'MISIS', Moscow, Russian Federation

³ Department of Chemistry, M.V. Lomonosov Moscow State University, Moscow, Russian Federation

10.1016/j.mencom.2023.06.028

Copy DOI

Published 2023-06-13

Communication , Volume 33, Issue 4, 528-530

View PDF

Graphical abstract

5

Share

Cite this

GOST

|

Cite this

GOST Copy

Makova A. S. et al. Synthesis of ferrierite-type zeolite by microwave method using ethylenediamine as an organic structure-directing agent // Mendeleev Communications. 2023. Vol. 33. No. 4. pp. 528-530.

GOST all authors (up to 50) Copy

Makova A. S., Kustov A. L., Davshan N. A., Mishin I. V., Kalmykov K. B., Shesterkina A. A., Kustov L. M. Synthesis of ferrierite-type zeolite by microwave method using ethylenediamine as an organic structure-directing agent // Mendeleev Communications. 2023. Vol. 33. No. 4. pp. 528-530.

RIS

|

Cite this

RIS Copy

TY - JOUR

DO - 10.1016/j.mencom.2023.06.028

UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2023.06.028

TI - Synthesis of ferrierite-type zeolite by microwave method using ethylenediamine as an organic structure-directing agent

T2 - Mendeleev Communications

AU - Makova, Anna S

AU - Kustov, Aleksandr Leonidovich

AU - Davshan, Nikolay Alekseevich

AU - Mishin, Igor Vladimirovich

AU - Kalmykov, Konstantin Borisovich

AU - Shesterkina, Anastasiya Alekseevna

AU - Kustov, Leonid Modestovich

PY - 2023

DA - 2023/06/13

PB - Mendeleev Communications

SP - 528-530

IS - 4

VL - 33

ER -

BibTex

|

Cite this

BibTex (up to 50 authors) Copy

@article{2023_Makova,

author = {Anna S Makova and Aleksandr Leonidovich Kustov and Nikolay Alekseevich Davshan and Igor Vladimirovich Mishin and Konstantin Borisovich Kalmykov and Anastasiya Alekseevna Shesterkina and Leonid Modestovich Kustov},

title = {Synthesis of ferrierite-type zeolite by microwave method using ethylenediamine as an organic structure-directing agent},

journal = {Mendeleev Communications},

year = {2023},

volume = {33},

publisher = {Mendeleev Communications},

month = {Jun},

url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2023.06.028},

number = {4},

pages = {528--530},

doi = {10.1016/j.mencom.2023.06.028}

}

MLA

Cite this

MLA Copy

Makova, Anna S., et al. “Synthesis of ferrierite-type zeolite by microwave method using ethylenediamine as an organic structure-directing agent.” Mendeleev Communications, vol. 33, no. 4, Jun. 2023, pp. 528-530. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2023.06.028.

Keywords

ethylenediamine.

FER

ferrierite

microwave synthesis

organic structure-directing agents

zeolites

Abstract

A new method for the synthesis of ferrierite-type zeolite has been developed using microwave irradiation in the presence of structure-directing agents (templates). The physicochemical characteristics of the synthesized zeolites were investigated by X-ray diffraction analysis, low-temperature nitrogen adsorption-desorption and SEM-EDX. When comparing the synthesis products, it was found that microwave irradiation significantly reduces the crystallization time of the synthesized zeolites compared to traditional hydrothermal treatment

References

.

10.1016/j.mencom.2021.07.030

IR spectroscopic investigation of internal silanol groups in different zeolites with pentasil structure

Kustov L.M., Kustov A.L.

Mendeleev Communications, 2021

.

10.1016/S0920-5861(98)00050-9

Surface area and pore texture of catalysts

Leofanti G., Padovan M., Tozzola G., Venturelli B.

Catalysis Today, 1998

.

10.1021/jp973028e

Multinuclear MQMAS NMR Study of NH₄/Na-Ferrierites

Sarv P., Wichterlová B., Čejka J.

Journal of Physical Chemistry B, 1998

.

10.3390/molecules25163722

Advances in the Synthesis of Ferrierite Zeolite

Xu H., Zhu J., Zhu L., Zhou E., Shen C.

Molecules, 2020

.

10.1021/jacs.1c04081

Exfoliated Ferrierite-Related Unilamellar Nanosheets in Solution and Their Use for Preparation of Mixed Zeolite Hierarchical Structures

Roth W.J., Sasaki T., Wolski K., Ebina Y., Tang D., Michiue Y., Sakai N., Ma R., Cretu O., Kikkawa J., Kimoto K., Kalahurska K., Gil B., Mazur M., Zapotoczny S., et. al.

Journal of the American Chemical Society, 2021

.

10.1039/c1jm11786f

Organotemplate-free synthesis of high-silica ferrierite zeolite induced by CDO-structure zeolite building units

Zhang H., Guo Q., Ren L., Yang C., Zhu L., Meng X., Li C., Xiao F.

Journal of Materials Chemistry A, 2011

.

$A Synchrotron X-ray Diffraction, Neutron Diffraction, 29Si MAS-NMR, and Computational Study of the Siliceous Form of Zeolite Ferrierite$

10.1021/ja00105a027

A Synchrotron X-ray Diffraction, Neutron Diffraction, 29Si MAS-NMR, and Computational Study of the Siliceous Form of Zeolite Ferrierite

Morris R.E., Weigel S.J., Henson N.J., Bull L.M., Janicke M.T., Chmelka B.F., Cheetham A.K.

Journal of the American Chemical Society, 1994

.

10.1023/a:1019099006237

Epoxidation of styrene with TBHP/O2 over ferrierite (FER) type molecular sieves

Anand R., Shevade S.S., Ahedi R.K., Mirajkar S.P., Rao B.S.

Catalysis Letters, 1999

.

10.1016/j.jcat.2009.02.017

Template-controlled acidity and catalytic activity of ferrierite crystals

Pinar A.B., Márquez-Álvarez C., Grande-Casas M., Pérez-Pariente J.

Journal of Catalysis, 2009

.

10.1016/j.micromeso.2014.07.057

In situ and post-synthesis control of physicochemical properties of FER-type crystals

Chen X., Todorova T., Vimont A., Ruaux V., Qin Z., Gilson J., Valtchev V.

Microporous and Mesoporous Materials, 2014

.

10.1016/j.micromeso.2015.10.040

Reduced coke formation during the gas phase oxidative dehydration of glycerol over ferrierite zeolites synthesized in fluoride medium

dos Santos M.B., Andrade H.M., Mascarenhas A.J.

Microporous and Mesoporous Materials, 2016

.

10.1016/j.apcata.2017.07.013

Propylene conversion in Ferrierite: Effect of mesoporous formation

Pereira M.M., Vieira A., Pereira E.B., Santos L.R., Lam Y.L.

Applied Catalysis A: General, 2017

.

10.1016/j.apcatb.2018.10.060

Catalytic application of ferrierite nanocrystals in vapour-phase dehydration of methanol to dimethyl ether

Catizzone E., Daele S.V., Bianco M., Di Michele A., Aloise A., Migliori M., Valtchev V., Giordano G.

Applied Catalysis B: Environmental, 2019

.

10.1016/j.micromeso.2018.12.036

Rapid synthesis of ferrierite zeolite through microwave assisted organic template free route

Wei P., Zhu X., Wang Y., Chu W., Xie S., Yang Z., Liu X., Li X., Xu L.

Microporous and Mesoporous Materials, 2019

.

10.1016/j.micromeso.2011.05.004

Tailoring of Fe-ferrierite for N2O decomposition: On the decisive role of framework Al distribution for catalytic activity of Fe species in Fe-ferrierite

Sobalik Z., Novakova J., Dedecek J., Sathu N.K., Tabor E., Sazama P., Stastny P., Wichterlova B.

Microporous and Mesoporous Materials, 2011

.

10.1016/j.ces.2019.08.005

Ferrierite zeolite passivation and its catalytic application in toluene disproportionation

Mesa S., Arboleda J., Echavarría A., López-Suárez F.E.

Chemical Engineering Science, 2019

.

$Synthesis of ferrierite zeolite with pyrrolidine as structure directing agent: A combined X-ray diffraction and computational study$

10.1016/j.micromeso.2009.09.012

Synthesis of ferrierite zeolite with pyrrolidine as structure directing agent: A combined X-ray diffraction and computational study

Pinar A.B., Wright P.A., Gómez-Hortigüela L., Pérez-Pariente J.

Microporous and Mesoporous Materials, 2010

.

10.1016/j.micromeso.2010.03.016

Layering of ferrierite sheets by using large co-structure directing agents: Zeolite synthesis using 1-benzyl-1-methylpyrrolidinium and tetraethylammonium

García R., Gómez-Hortigüela L., Blasco T., Pérez-Pariente J.

Microporous and Mesoporous Materials, 2010

.

10.1016/j.jcat.2009.04.022

Desilication of ferrierite zeolite for porosity generation and improved effectiveness in polyethylene pyrolysis

Bonilla A., Baudouin D., Pérez-Ramírez J.

Journal of Catalysis, 2009

.

10.1016/j.jcat.2006.06.010

Isothermal oscillation during N2O decomposition over Fe- and Fe/Pt-ferrierite: Effect of NO addition

KAUCKY D., JISA K., VONDROVA A., NOVAKOVA J., SOBALIK Z.

Journal of Catalysis, 2006

.

10.1016/j.micromeso.2007.01.046

Synthesis of large crystals of all-silica zeolite ferrierite

Rakoczy R.A., Traa Y., Kortunov P., Vasenkov S., Kärger J., Weitkamp J.

Microporous and Mesoporous Materials, 2007

.

10.1016/j.micromeso.2007.02.004

Comparison of butene skeletal isomerization selectivity over a pair of commercial H-ferrierites

Onyestyák G.

Microporous and Mesoporous Materials, 2007

.

10.1016/j.micromeso.2021.111262

Microwave synthesis of zeolites and their related applications

Zeng X., Hu X., Song H., Xia G., Shen Z., Yu R., Moskovits M.

Microporous and Mesoporous Materials, 2021

.

10.1016/j.mencom.2021.03.028

Increasing the yield of aromatic hydrocarbons in aromatization of n-butane over Ga/H-ZSM-5 zeolite using a palladium membrane

Bogdan V.I., Koklin A.E., Mishanin I.I., Bogdan T.V., Mashchenko N.V., Kustov L.M.

Mendeleev Communications, 2021

.

10.1016/j.mencom.2021.09.040

Gas-phase oxidative carbonylation of methane to acetic acid over zeolites

Golubev K.B., Yashina O.V., Ezhova N.N., Kolesnichenko N.N.

Mendeleev Communications, 2021

.

10.1016/j.ijhydene.2022.07.212

Dimethyl ether (DME) synthesis from CO2 and H2 through ethanol-assisted methanol synthesis and methanol dehydration

Kriprasertkul W., Witoon T., Kim-Lohsoontorn P.

International Journal of Hydrogen Energy, 2022

.

10.1016/j.apcata.2022.118676

Engineering pore structure and acidity of ferrierite zeolites by organic structure directing agents for n-butene isomerization

Liu X., Liao Z., Wang H., Fu J., Zheng J., Zhang N., Chen B.

Applied Catalysis A: General, 2022

.

10.57634/RCR5064

Recent developments of Fe-based metal-organic frameworks and their composites in photocatalytic applications: fundamentals, synthesis and challenges

Ikreedeegh Riyadh Ramadhan

Russian Chemical Reviews, 2022