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A convenient synthesis of N,N',N''-trisubstituted diethylenetriamines

Milana Umud kyzy Agaeva 1, 2
Milana Umud kyzy Agaeva
, 
Badma Nikolaevich Mankaev 1, 2
Badma Nikolaevich Mankaev
, 
Vladislav Igorevich Filippenko 2
Vladislav Igorevich Filippenko
, 
Valeriia Andreevna Serova 1, 2
Valeriia Andreevna Serova
, 
Mikhail Petrovich Egorov 1
Mikhail Petrovich Egorov
, 
Sergey Sergeevich Karlov 1, 2
Sergey Sergeevich Karlov
2 Department of Chemistry, M.V. Lomonosov Moscow State University, Moscow, Russian Federation
10.1016/j.mencom.2023.02.003
Published 2023-02-13
Communication , Volume 33, Issue 2, 157-159
3
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Agaeva M. U. K. et al. A convenient synthesis of N,N',N''-trisubstituted diethylenetriamines // Mendeleev Communications. 2023. Vol. 33. No. 2. pp. 157-159.
GOST all authors (up to 50) Copy
Agaeva M. U. K., Mankaev B. N., Filippenko V. I., Serova V. A., Egorov M. P., Karlov S. S. A convenient synthesis of N,N',N''-trisubstituted diethylenetriamines // Mendeleev Communications. 2023. Vol. 33. No. 2. pp. 157-159.
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TY - JOUR
DO - 10.1016/j.mencom.2023.02.003
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2023.02.003
TI - A convenient synthesis of N,N',N''-trisubstituted diethylenetriamines
T2 - Mendeleev Communications
AU - Agaeva, Milana Umud kyzy
AU - Mankaev, Badma Nikolaevich
AU - Filippenko, Vladislav Igorevich
AU - Serova, Valeriia Andreevna
AU - Egorov, Mikhail Petrovich
AU - Karlov, Sergey Sergeevich
PY - 2023
DA - 2023/02/13
PB - Mendeleev Communications
SP - 157-159
IS - 2
VL - 33
ER -
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@article{2023_Agaeva,
author = {Milana Umud kyzy Agaeva and Badma Nikolaevich Mankaev and Vladislav Igorevich Filippenko and Valeriia Andreevna Serova and Mikhail Petrovich Egorov and Sergey Sergeevich Karlov},
title = {A convenient synthesis of N,N',N''-trisubstituted diethylenetriamines},
journal = {Mendeleev Communications},
year = {2023},
volume = {33},
publisher = {Mendeleev Communications},
month = {Feb},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2023.02.003},
number = {2},
pages = {157--159},
doi = {10.1016/j.mencom.2023.02.003}
}
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Agaeva, Milana Umud kyzy, et al. “A convenient synthesis of N,N',N''-trisubstituted diethylenetriamines.” Mendeleev Communications, vol. 33, no. 2, Feb. 2023, pp. 157-159. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2023.02.003.

Keywords

amidation.
carboxamides
diethylenetriamines
ligands
microwave-assisted synthesis
polyamines
reduction

Abstract

N,N',N''-Trisubstituted diethylenetriamines (1,4,7-triaza-heptanes) were synthesized by reduction of the relevantly substituted 2,2'-iminodiacetiamides which, in turn, were accessed from cheap reactants by the methods depending on their nature. The triamines thus obtained may be promising ligands for metal catalysts.

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