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Synthesis of nanocrystalline magnesium oxide by thermolysis of magnesium citrate

Yulia Evgen'evna Sinelnikova 1, 2
Yulia Evgen'evna Sinelnikova
, 
Nikolai Favstovich Uvarov 1, 2
Nikolai Favstovich Uvarov
10.1016/j.mencom.2022.09.044
Published 2022-09-05
Communication , Volume 32, Issue 5, 697-699
3
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Sinelnikova Y. E., Uvarov N. F. Synthesis of nanocrystalline magnesium oxide by thermolysis of magnesium citrate // Mendeleev Communications. 2022. Vol. 32. No. 5. pp. 697-699.
GOST all authors (up to 50) Copy
Sinelnikova Y. E., Uvarov N. F. Synthesis of nanocrystalline magnesium oxide by thermolysis of magnesium citrate // Mendeleev Communications. 2022. Vol. 32. No. 5. pp. 697-699.
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TY - JOUR
DO - 10.1016/j.mencom.2022.09.044
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2022.09.044
TI - Synthesis of nanocrystalline magnesium oxide by thermolysis of magnesium citrate
T2 - Mendeleev Communications
AU - Sinelnikova, Yulia Evgen'evna
AU - Uvarov, Nikolai Favstovich
PY - 2022
DA - 2022/09/05
PB - Mendeleev Communications
SP - 697-699
IS - 5
VL - 32
ER -
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@article{2022_Sinelnikova,
author = {Yulia Evgen'evna Sinelnikova and Nikolai Favstovich Uvarov},
title = {Synthesis of nanocrystalline magnesium oxide by thermolysis of magnesium citrate},
journal = {Mendeleev Communications},
year = {2022},
volume = {32},
publisher = {Mendeleev Communications},
month = {Sep},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2022.09.044},
number = {5},
pages = {697--699},
doi = {10.1016/j.mencom.2022.09.044}
}
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Sinelnikova, Yulia Evgen'evna, and Nikolai Favstovich Uvarov. “Synthesis of nanocrystalline magnesium oxide by thermolysis of magnesium citrate.” Mendeleev Communications, vol. 32, no. 5, Sep. 2022, pp. 697-699. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2022.09.044.

Keywords

magnesium citrate
Mg3(C6H5O7)2·10H2O
nanocrystalline magnesium oxide
thermolysis mechanism
X-ray amorphous products

Abstract

Magnesium citrate, obtained by dissolving magnesium oxide in an aqueous solution of citric acid, turned out to be a decahydrate of the composition Mg3(C6H5O7)2·10H2O, which was established by the results of synchronous thermal analysis, X-ray diffraction and IR spectroscopy. It is shown that the thermal decomposition of this salt proceeds in three stages in the temperature ranges of 120–250, 250–370 and 370–550 °C to form nanocrystalline magnesium oxide with grain sizes from 7 to 23 nm.

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