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A simple method for quantification of nonstoichiometric magnetite nanoparticles using conventional X-ray diffraction technique

Lyubov Sergeevna Bondarenko 1
Lyubov Sergeevna Bondarenko
, 
Denis A Pankratov 2
Denis A Pankratov
,  , 
Gulzhian Iskakovna Dzhardimalieva 1, 3
Gulzhian Iskakovna Dzhardimalieva
, 
Alla Nikolaevna Streltsova 1
Alla Nikolaevna Streltsova
, 
Mauro Zarrelli 4
Mauro Zarrelli
, 
Kamila Asylbekovna Kydralieva 1
Kamila Asylbekovna Kydralieva
10.1016/j.mencom.2022.09.025
Published 2022-09-05
Communication , Volume 32, Issue 5, 642-644
12
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Bondarenko L. S. et al. A simple method for quantification of nonstoichiometric magnetite nanoparticles using conventional X-ray diffraction technique // Mendeleev Communications. 2022. Vol. 32. No. 5. pp. 642-644.
GOST all authors (up to 50) Copy
Bondarenko L. S., Pankratov D. A., Dzeranov A. A., Dzhardimalieva G. I., Streltsova A. N., Zarrelli M., Kydralieva K. A. A simple method for quantification of nonstoichiometric magnetite nanoparticles using conventional X-ray diffraction technique // Mendeleev Communications. 2022. Vol. 32. No. 5. pp. 642-644.
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TY - JOUR
DO - 10.1016/j.mencom.2022.09.025
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2022.09.025
TI - A simple method for quantification of nonstoichiometric magnetite nanoparticles using conventional X-ray diffraction technique
T2 - Mendeleev Communications
AU - Bondarenko, Lyubov Sergeevna
AU - Pankratov, Denis A
AU - Dzeranov, Artur Al'bertovich
AU - Dzhardimalieva, Gulzhian Iskakovna
AU - Streltsova, Alla Nikolaevna
AU - Zarrelli, Mauro
AU - Kydralieva, Kamila Asylbekovna
PY - 2022
DA - 2022/09/05
PB - Mendeleev Communications
SP - 642-644
IS - 5
VL - 32
ER -
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@article{2022_Bondarenko,
author = {Lyubov Sergeevna Bondarenko and Denis A Pankratov and Artur Al'bertovich Dzeranov and Gulzhian Iskakovna Dzhardimalieva and Alla Nikolaevna Streltsova and Mauro Zarrelli and Kamila Asylbekovna Kydralieva},
title = {A simple method for quantification of nonstoichiometric magnetite nanoparticles using conventional X-ray diffraction technique},
journal = {Mendeleev Communications},
year = {2022},
volume = {32},
publisher = {Mendeleev Communications},
month = {Sep},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2022.09.025},
number = {5},
pages = {642--644},
doi = {10.1016/j.mencom.2022.09.025}
}
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Bondarenko, Lyubov Sergeevna, et al. “A simple method for quantification of nonstoichiometric magnetite nanoparticles using conventional X-ray diffraction technique.” Mendeleev Communications, vol. 32, no. 5, Sep. 2022, pp. 642-644. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2022.09.025.

Abstract

A simple method was proposed for calculating the composition of nonstoichiometric or partially oxidized magnetite, based on a linear relationship between the position of the (440) peak in the X-ray diffraction pattern and the completeness of material oxidation. The results obtained were verified by the Rietveld refinement method and showed the possibility of a principal assessment of the magnetite/maghemite ratio.

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