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Synthesis and crystal structure of triphenyltin and lead complexes with organic peroxides

Alexander G Medvedev 1
Alexander G Medvedev
,  , 
Dmitry Andreevich Grishanov 1, 2
Dmitry Andreevich Grishanov
, 
Artur V Eshtukov 3
Artur V Eshtukov
, 
Andrei Viktorovich Churakov 1
Andrei Viktorovich Churakov
, 
Ivan Andreevich Buldashov 1
Ivan Andreevich Buldashov
, 
Pavel A Egorov 1
Pavel A Egorov
, 
Ovadia Lev 2
Ovadia Lev
, 
Petr Valer'evich Prikhodchenko 1
Petr Valer'evich Prikhodchenko
10.1016/j.mencom.2022.01.018
Published 2022-01-03
Communication , Volume 32, Issue 1, 57-59
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Medvedev A. G. et al. Synthesis and crystal structure of triphenyltin and lead complexes with organic peroxides // Mendeleev Communications. 2022. Vol. 32. No. 1. pp. 57-59.
GOST all authors (up to 50) Copy
Medvedev A. G., Sharipov M. Y., Grishanov D. A., Eshtukov A. V., Churakov A. V., Buldashov I. A., Egorov P. A., Lev O., Prikhodchenko P. V. Synthesis and crystal structure of triphenyltin and lead complexes with organic peroxides // Mendeleev Communications. 2022. Vol. 32. No. 1. pp. 57-59.
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TY - JOUR
DO - 10.1016/j.mencom.2022.01.018
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2022.01.018
TI - Synthesis and crystal structure of triphenyltin and lead complexes with organic peroxides
T2 - Mendeleev Communications
AU - Medvedev, Alexander G
AU - Sharipov, Mikhail Yuryevich
AU - Grishanov, Dmitry Andreevich
AU - Eshtukov, Artur V
AU - Churakov, Andrei Viktorovich
AU - Buldashov, Ivan Andreevich
AU - Egorov, Pavel A
AU - Lev, Ovadia
AU - Prikhodchenko, Petr Valer'evich
PY - 2022
DA - 2022/01/03
PB - Mendeleev Communications
SP - 57-59
IS - 1
VL - 32
ER -
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@article{2022_Medvedev,
author = {Alexander G Medvedev and Mikhail Yuryevich Sharipov and Dmitry Andreevich Grishanov and Artur V Eshtukov and Andrei Viktorovich Churakov and Ivan Andreevich Buldashov and Pavel A Egorov and Ovadia Lev and Petr Valer'evich Prikhodchenko},
title = {Synthesis and crystal structure of triphenyltin and lead complexes with organic peroxides},
journal = {Mendeleev Communications},
year = {2022},
volume = {32},
publisher = {Mendeleev Communications},
month = {Jan},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2022.01.018},
number = {1},
pages = {57--59},
doi = {10.1016/j.mencom.2022.01.018}
}
MLA
Cite this
MLA Copy
Medvedev, Alexander G., et al. “Synthesis and crystal structure of triphenyltin and lead complexes with organic peroxides.” Mendeleev Communications, vol. 32, no. 1, Jan. 2022, pp. 57-59. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2022.01.018.

Keywords

Coordination peroxo compounds
hydrogen peroxide
lead
Organic hydroperoxides
Peroxo complexes
tin

Abstract

Crystalline triphenyltin cumyl and tert-butyl peroxides (Ph3SnOOCMe2Ph and Ph3SnOOBut, respectively) and triphenyllead cumyl peroxide (Ph3PbOOCMe2Ph) were synthesized and characterized by single crystal and powder X-ray diffraction, NMR, FTIR and Raman spectroscopies, TG and DSC analysis. The formation of triphenyltin tert-butyl peroxide in benzene in the presence of a base was proved by 119Sn, 13C and 1H NMR spectroscopy. To the best of our knowledge, the obtained complexes are the first structurally characterized coordination compounds of tin and lead with organic peroxides.

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