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A mechanistic insight into the chemoselectivity of the reaction between 3-phenyl-2-propynenitrile, secondary phosphine oxides and pyridinoids

Pavel Anatol'evich Volkov 1
Pavel Anatol'evich Volkov
Nina Kuzminichna Gusarova 1
Nina Kuzminichna Gusarova
Kseniya Olegovna Khrapova 1
Kseniya Olegovna Khrapova
Anton Alekseevich Telezhkin 1
Anton Alekseevich Telezhkin
Alexander Ivanovich Albanov 1
Alexander Ivanovich Albanov
Sergey Franzevich Vasilevskii 2
Sergey Franzevich Vasilevskii
Boris Aleksandrovich Trofimov 1
Boris Aleksandrovich Trofimov
Published 2021-09-08
CommunicationVolume 31, Issue 5, 670-672
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Volkov P. A. et al. A mechanistic insight into the chemoselectivity of the reaction between 3-phenyl-2-propynenitrile, secondary phosphine oxides and pyridinoids // Mendeleev Communications. 2021. Vol. 31. No. 5. pp. 670-672.
GOST all authors (up to 50) Copy
Volkov P. A., Gusarova N. K., Khrapova K. O., Telezhkin A. A., Albanov A. I., Vasilevskii S. F., Trofimov B. A. A mechanistic insight into the chemoselectivity of the reaction between 3-phenyl-2-propynenitrile, secondary phosphine oxides and pyridinoids // Mendeleev Communications. 2021. Vol. 31. No. 5. pp. 670-672.
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TY - JOUR
DO - 10.1016/j.mencom.2021.09.026
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2021.09.026
TI - A mechanistic insight into the chemoselectivity of the reaction between 3-phenyl-2-propynenitrile, secondary phosphine oxides and pyridinoids
T2 - Mendeleev Communications
AU - Volkov, Pavel Anatol'evich
AU - Gusarova, Nina Kuzminichna
AU - Khrapova, Kseniya Olegovna
AU - Telezhkin, Anton Alekseevich
AU - Albanov, Alexander Ivanovich
AU - Vasilevskii, Sergey Franzevich
AU - Trofimov, Boris Aleksandrovich
PY - 2021
DA - 2021/09/08
PB - Mendeleev Communications
SP - 670-672
IS - 5
VL - 31
ER -
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@article{2021_Volkov,
author = {Pavel Anatol'evich Volkov and Nina Kuzminichna Gusarova and Kseniya Olegovna Khrapova and Anton Alekseevich Telezhkin and Alexander Ivanovich Albanov and Sergey Franzevich Vasilevskii and Boris Aleksandrovich Trofimov},
title = {A mechanistic insight into the chemoselectivity of the reaction between 3-phenyl-2-propynenitrile, secondary phosphine oxides and pyridinoids},
journal = {Mendeleev Communications},
year = {2021},
volume = {31},
publisher = {Mendeleev Communications},
month = {Sep},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2021.09.026},
number = {5},
pages = {670--672},
doi = {10.1016/j.mencom.2021.09.026}
}
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Volkov, Pavel Anatol'evich, et al. “A mechanistic insight into the chemoselectivity of the reaction between 3-phenyl-2-propynenitrile, secondary phosphine oxides and pyridinoids.” Mendeleev Communications, vol. 31, no. 5, Sep. 2021, pp. 670-672. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2021.09.026.
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Keywords

$\mathrm{S_N^H{Ar}}$ reaction
3-phenyl-2-propynenitrile
isoquinoline
N-vinylation/C-phosphorylation
pyridinoids
secondary phosphine oxides

Abstract

Reactions between 3-phenyl-2-propynenitrile, secondary phosphine oxides and pyridinoids have been implemented and studied. Pyridine and isoquinoline react with propynenitrile and phosphine oxides at room temperature according to the N-vinylation/C-phosphorylation scheme to afford (Z)-N-(2-cyano-1-phenyl)ethenyl phosphoryl-1,4-dihydropyridines or -1,2-dihydroiso quinolines. In the case of pyridine on heating (80-85 °C), the reaction gives 4-phosphorylpyridines (\( \mathrm{S_N^H{Ar}} \) reaction) and 3-phenyl-acrylonitrile oligomers.

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