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Mechanochemical synthesis of PbS/Ni–Cr layered double hydroxide nanocomposite

Khazangul Adil Ibrahimova 1
Khazangul Adil Ibrahimova
, 
Abdulsaid A Azizov 1
Abdulsaid A Azizov
, 
Ofeliya Oqtay Balayeva 1
Ofeliya Oqtay Balayeva
, 
Rasim M Alosmanov 1
Rasim M Alosmanov
, 
Sevinj C Mammadyarova 2
Sevinj C Mammadyarova
10.1016/j.mencom.2021.01.031
Published 2020-12-30
Communication , Volume 31, Issue 1, 100-103
4
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Ibrahimova K. A. et al. Mechanochemical synthesis of PbS/Ni–Cr layered double hydroxide nanocomposite // Mendeleev Communications. 2020. Vol. 31. No. 1. pp. 100-103.
GOST all authors (up to 50) Copy
Ibrahimova K. A., Azizov A. A., Balayeva O. O., Alosmanov R. M., Mammadyarova S. C. Mechanochemical synthesis of PbS/Ni–Cr layered double hydroxide nanocomposite // Mendeleev Communications. 2020. Vol. 31. No. 1. pp. 100-103.
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TY - JOUR
DO - 10.1016/j.mencom.2021.01.031
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2021.01.031
TI - Mechanochemical synthesis of PbS/Ni–Cr layered double hydroxide nanocomposite
T2 - Mendeleev Communications
AU - Ibrahimova, Khazangul Adil
AU - Azizov, Abdulsaid A
AU - Balayeva, Ofeliya Oqtay
AU - Alosmanov, Rasim M
AU - Mammadyarova, Sevinj C
PY - 2020
DA - 2020/12/30
PB - Mendeleev Communications
SP - 100-103
IS - 1
VL - 31
ER -
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@article{2020_Ibrahimova,
author = {Khazangul Adil Ibrahimova and Abdulsaid A Azizov and Ofeliya Oqtay Balayeva and Rasim M Alosmanov and Sevinj C Mammadyarova},
title = {Mechanochemical synthesis of PbS/Ni–Cr layered double hydroxide nanocomposite},
journal = {Mendeleev Communications},
year = {2020},
volume = {31},
publisher = {Mendeleev Communications},
month = {Dec},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2021.01.031},
number = {1},
pages = {100--103},
doi = {10.1016/j.mencom.2021.01.031}
}
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MLA Copy
Ibrahimova, Khazangul Adil, et al. “Mechanochemical synthesis of PbS/Ni–Cr layered double hydroxide nanocomposite.” Mendeleev Communications, vol. 31, no. 1, Dec. 2020, pp. 100-103. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2021.01.031.

Keywords

layered double hydroxide
lead(II) sulfide nanoparticles
mechanochemical synthesis
Nanocomposite
optical properties
structural characteristics

Abstract

The synthesis of lead(II) sulfide nanocomposite based on nickel–chromium layered double hydroxide was accomplished by the mechanochemical method at room temperature. The obtained nanocomposites were characterized by powder X-ray diffraction, UV-VIS spectroscopy, scanning electron microscopy and energy-dispersive X-ray spectroscopy to estimate structural, optical and morphological properties. The PbS nanoparticles expanded the interlayer space of the layered double hydroxide, its crystal structure was destroyed, and the PbS nanoparticles attached to the surface affected the XRD result.

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