Keywords
calcium
crystal morphology
crystallography
EDTA
electron microscopy
hydrothermal synthesis
hydroxyapatite
X-ray diffraction
Abstract
The morphology of hydroxyapatite crystals formed in hydrothermal reaction of calcium EDTA complex with KH2PO4 at 120°C depends on the pH value of the reaction medium. Bone-like platy microcrystals were prepared at pH 6, while at higher pH values rod-like species were obtained.
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