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4-Azidotetrahydroquinazoline derivatives in CuAAC reaction

Anna Andreevna Nazarova 1
Anna Andreevna Nazarova
Dmitry Alekseevich Vasilenko 1
Dmitry Alekseevich Vasilenko
Tamara Stepanovna Kuznetsova 1
Tamara Stepanovna Kuznetsova
Elena Borisovna Averina 1, 2
Elena Borisovna Averina
Published 2020-11-03
CommunicationVolume 30, Issue 6, 714-716
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Nazarova A. A. et al. 4-Azidotetrahydroquinazoline derivatives in CuAAC reaction // Mendeleev Communications. 2020. Vol. 30. No. 6. pp. 714-716.
GOST all authors (up to 50) Copy
Nazarova A. A., Sedenkova K. N., Vasilenko D. A., Grishin Y. K., Kuznetsova T. S., Averina E. B. 4-Azidotetrahydroquinazoline derivatives in CuAAC reaction // Mendeleev Communications. 2020. Vol. 30. No. 6. pp. 714-716.
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TY - JOUR
DO - 10.1016/j.mencom.2020.11.008
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2020.11.008
TI - 4-Azidotetrahydroquinazoline derivatives in CuAAC reaction
T2 - Mendeleev Communications
AU - Nazarova, Anna Andreevna
AU - Sedenkova, Kseniya N
AU - Vasilenko, Dmitry Alekseevich
AU - Grishin, Yuri Konstantinovich
AU - Kuznetsova, Tamara Stepanovna
AU - Averina, Elena Borisovna
PY - 2020
DA - 2020/11/03
PB - Mendeleev Communications
SP - 714-716
IS - 6
VL - 30
ER -
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@article{2020_Nazarova,
author = {Anna Andreevna Nazarova and Kseniya N Sedenkova and Dmitry Alekseevich Vasilenko and Yuri Konstantinovich Grishin and Tamara Stepanovna Kuznetsova and Elena Borisovna Averina},
title = {4-Azidotetrahydroquinazoline derivatives in CuAAC reaction},
journal = {Mendeleev Communications},
year = {2020},
volume = {30},
publisher = {Mendeleev Communications},
month = {Nov},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2020.11.008},
number = {6},
pages = {714--716},
doi = {10.1016/j.mencom.2020.11.008}
}
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Cite this
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Nazarova, Anna Andreevna, et al. “4-Azidotetrahydroquinazoline derivatives in CuAAC reaction.” Mendeleev Communications, vol. 30, no. 6, Nov. 2020, pp. 714-716. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2020.11.008.

Keywords

N-oxides
azidopyrimidine N-oxides
CuAAC
pyrimidines
quantum chemical calculations
tautomers
triazoles

Abstract

4-Azido-2-methyltetrahydroquinazoline N-oxide cleanly undergoes the copper(i)-catalyzed azide–alkyne cycloaddition (CuAAC) reaction with alkynes to give new conjugates with pyrimidine N-oxide and triazole moieties. Its deoxygenated analogue, 4-azido-2-methyltetrahydroquinazoline, is inert in CuACC process due to the shift of imidoyl azide–tetrazole equilibrium towards the tetrazole tautomer.

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