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Synthesis and structure of new chlorine containing calix[4]resorcinols

Irina Rafaelevna Mironova (Knyazeva) 1
Irina Rafaelevna Mironova (Knyazeva)
, 
Victor Vasil'evich Syakaev 1
Victor Vasil'evich Syakaev
, 
Olga Aleksandrovna Lodochnikova 1
Olga Aleksandrovna Lodochnikova
, 
Alexander Romanovich Burilov 1
Alexander Romanovich Burilov
10.1016/j.mencom.2019.11.034
Published 2019-11-01
Communication , Volume 29, Issue 6, 700-701
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Mironova (Knyazeva) I. R. et al. Synthesis and structure of new chlorine containing calix[4]resorcinols // Mendeleev Communications. 2019. Vol. 29. No. 6. pp. 700-701.
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Mironova (Knyazeva) I. R., Syakaev V. V., Lodochnikova O. A., Burilov A. R. Synthesis and structure of new chlorine containing calix[4]resorcinols // Mendeleev Communications. 2019. Vol. 29. No. 6. pp. 700-701.
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TY - JOUR
DO - 10.1016/j.mencom.2019.11.034
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2019.11.034
TI - Synthesis and structure of new chlorine containing calix[4]resorcinols
T2 - Mendeleev Communications
AU - Mironova (Knyazeva), Irina Rafaelevna
AU - Syakaev, Victor Vasil'evich
AU - Lodochnikova, Olga Aleksandrovna
AU - Burilov, Alexander Romanovich
PY - 2019
DA - 2019/11/01
PB - Mendeleev Communications
SP - 700-701
IS - 6
VL - 29
ER -
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@article{2019_Mironova (Knyazeva),
author = {Irina Rafaelevna Mironova (Knyazeva) and Victor Vasil'evich Syakaev and Olga Aleksandrovna Lodochnikova and Alexander Romanovich Burilov},
title = {Synthesis and structure of new chlorine containing calix[4]resorcinols},
journal = {Mendeleev Communications},
year = {2019},
volume = {29},
publisher = {Mendeleev Communications},
month = {Nov},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2019.11.034},
number = {6},
pages = {700--701},
doi = {10.1016/j.mencom.2019.11.034}
}
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Mironova (Knyazeva), Irina Rafaelevna, et al. “Synthesis and structure of new chlorine containing calix[4]resorcinols.” Mendeleev Communications, vol. 29, no. 6, Nov. 2019, pp. 700-701. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2019.11.034.

Abstract

New calix[4]resorcinols containing four organochlorine moieties have been synthesized in high yields via one-step condensation of resorcinol, 2-methylresorcinol or pyrogallol with 4′-formylphenyl 4-(chloromethyl)benzoate. It has been found that the diastereomeric ratio of the products depends substantially on the starting polyphenol. The rctt- and/or rccc-diastereomers have been isolated and their structure and composition have been determined by 1H, 13C NMR and IR spectroscopy, MALDI mass spectrometry and elemental analysis, the crystal structure of one rctt-product has been established by single crystal X-ray diffraction.

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