Home / Publications / Synthesis, crystal structures and solid state reactions of zinc(ii) cyclobutane-1,1′-dicarboxylates containing 1,2-bis(pyrid-4 yl)ethylene

Synthesis, crystal structures and solid state reactions of zinc(ii) cyclobutane-1,1′-dicarboxylates containing 1,2-bis(pyrid-4 yl)ethylene

Ivan Evgenievich Ushakov 1
Ivan Evgenievich Ushakov
, 
Alexander Sergeyevich Goloveshkin 1
Alexander Sergeyevich Goloveshkin
, 
Ekaterina Nikolaevna Zorina-Tikhonova 2
Ekaterina Nikolaevna Zorina-Tikhonova
, 
Aleksandr Sergeevich Chistyakov 2
Aleksandr Sergeevich Chistyakov
, 
Alexey Anatol'evich Sidorov 2
Alexey Anatol'evich Sidorov
, 
Igor Leonidovich Eremenko 1, 2
Igor Leonidovich Eremenko
, 
Alexander Dmitrievich Volodin 1
Alexander Dmitrievich Volodin
, 
Anna Vladimirovna Vologzhanina 1
Anna Vladimirovna Vologzhanina
10.1016/j.mencom.2019.11.012
Published 2019-11-01
Communication , Volume 29, Issue 6, 643-645
8
Share
Cite this
GOST
 | 
Cite this
GOST Copy
Ushakov I. E. et al. Synthesis, crystal structures and solid state reactions of zinc(ii) cyclobutane-1,1′-dicarboxylates containing 1,2-bis(pyrid-4 yl)ethylene // Mendeleev Communications. 2019. Vol. 29. No. 6. pp. 643-645.
GOST all authors (up to 50) Copy
Ushakov I. E., Goloveshkin A. S., Zorina-Tikhonova E. N., Chistyakov A. S., Sidorov A. A., Eremenko I. L., Volodin A. D., Vologzhanina A. V. Synthesis, crystal structures and solid state reactions of zinc(ii) cyclobutane-1,1′-dicarboxylates containing 1,2-bis(pyrid-4 yl)ethylene // Mendeleev Communications. 2019. Vol. 29. No. 6. pp. 643-645.
RIS
 | 
Cite this
RIS Copy
TY - JOUR
DO - 10.1016/j.mencom.2019.11.012
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2019.11.012
TI - Synthesis, crystal structures and solid state reactions of zinc(ii) cyclobutane-1,1′-dicarboxylates containing 1,2-bis(pyrid-4 yl)ethylene
T2 - Mendeleev Communications
AU - Ushakov, Ivan Evgenievich
AU - Goloveshkin, Alexander Sergeyevich
AU - Zorina-Tikhonova, Ekaterina Nikolaevna
AU - Chistyakov, Aleksandr Sergeevich
AU - Sidorov, Alexey Anatol'evich
AU - Eremenko, Igor Leonidovich
AU - Volodin, Alexander Dmitrievich
AU - Vologzhanina, Anna Vladimirovna
PY - 2019
DA - 2019/11/01
PB - Mendeleev Communications
SP - 643-645
IS - 6
VL - 29
ER -
BibTex
 | 
Cite this
BibTex (up to 50 authors) Copy
@article{2019_Ushakov,
author = {Ivan Evgenievich Ushakov and Alexander Sergeyevich Goloveshkin and Ekaterina Nikolaevna Zorina-Tikhonova and Aleksandr Sergeevich Chistyakov and Alexey Anatol'evich Sidorov and Igor Leonidovich Eremenko and Alexander Dmitrievich Volodin and Anna Vladimirovna Vologzhanina},
title = {Synthesis, crystal structures and solid state reactions of zinc(ii) cyclobutane-1,1′-dicarboxylates containing 1,2-bis(pyrid-4 yl)ethylene},
journal = {Mendeleev Communications},
year = {2019},
volume = {29},
publisher = {Mendeleev Communications},
month = {Nov},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2019.11.012},
number = {6},
pages = {643--645},
doi = {10.1016/j.mencom.2019.11.012}
}
MLA
Cite this
MLA Copy
Ushakov, Ivan Evgenievich, et al. “Synthesis, crystal structures and solid state reactions of zinc(ii) cyclobutane-1,1′-dicarboxylates containing 1,2-bis(pyrid-4 yl)ethylene.” Mendeleev Communications, vol. 29, no. 6, Nov. 2019, pp. 643-645. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2019.11.012.

Abstract

Synthesis and response towards heating and UV irradiation of two novel zinc(II) cyclobutane-1,1′-dicarboxylate complexes were examined using X-ray diffraction, FT-IR and 1H NMR spectroscopy. One of the complexes underwent a photoinitiated solid state transformation of 1,2-bis(pyrid-4-yl)ethylene into 1,2,3,4-tetrakis(pyrid-4-yl)cyclobutane. A preliminary dehydration of this solid decreases the conversion rate of photoreaction.

References

1.
Photodimerization in the solid state
Schmidt G.M.
Pure and Applied Chemistry, 1971
2.
Photodriven single-crystal-to-single-crystal transformation
Huang S., Hor T.S., Jin G.
Coordination Chemistry Reviews, 2017
4.
Photoinduced Linkage Isomers of Transition-Metal Nitrosyl Compounds and Related Complexes
Coppens P., Novozhilova I., Kovalevsky A.
Chemical Reviews, 2002
5.
Kiyani H., Mahmoodi N.O., Tabatabaeian K., Zanjanchi M.A.
Mendeleev Communications, 2009
6.
Supramolecular Dimerization and [2 + 2] Photocycloaddition Reactions of Crown Ether Styryl Dyes Containing a Tethered Ammonium Group: Structure-Property Relationships
Ushakov E.N., Vedernikov A.I., Lobova N.A., Dmitrieva S.N., Kuz’mina L.G., Moiseeva A.A., Howard J.A., Alfimov M.V., Gromov S.P.
Journal of Physical Chemistry A, 2015
7.
Stacking of double bonds for photochemical [2+2] cycloaddition reactions in the solid state
Nagarathinam M., Peedikakkal A.M., Vittal J.J.
Chemical Communications, 2008
8.
10.1016/j.mencom.2019.11.012_sbref0025c
Kuz7
Crystallogr. Rep., 2019
10.
Supramolecular organic photochemistry of crown-ether-containing styryl dyes
Gromov S.P., Alfimov M.V.
Russian Chemical Bulletin, 1997
12.
Photocontrolled molecular assembler based on cucurbit[8]uril: [2+2]autophotocycloaddition of styryl dyes in the solid state and in water
Gromov S.P., Vedernikov A.I., Kuz'mina L.G., Kondratuk D.V., Sazonov S.K., Strelenko Y.A., Alfimov M.V., Howard J.A.
European Journal of Organic Chemistry, 2010
13.
Exploitation of knowledge databases in the synthesis of zinc(II) malonates with photo-sensitive and photo-insensitive N,N′-containing linkers
Zorina-Tikhonova E.N., Chistyakov A.S., Kiskin M.A., Sidorov A.A., Dorovatovskii P.V., Zubavichus Y.V., Voronova E.D., Godovikov I.A., Korlyukov A.A., Eremenko I.L., Vologzhanina A.V.
IUCrJ, 2018
14.
Diastereoselective solid-state crossed photocycloaddition of olefins in a 3D Zn(ii) coordination polymer
Volodin A.D., Korlyukov A.A., Zorina-Tikhonova E.N., Chistyakov A.S., Sidorov A.A., Eremenko I.L., Vologzhanina A.V.
Chemical Communications, 2018
15.
The Reticular Chemistry Structure Resource (RCSR) Database of, and Symbols for, Crystal Nets
O’Keeffe M., Peskov M.A., Ramsden S.J., Yaghi O.M.
Accounts of Chemical Research, 2008
16.
A Step-by-Step Assembly of a 3D Coordination Polymer in the Solid-State by Desolvation and [2+2] Cycloaddition Reactions
Medishetty R., Tandiana R., Wu J., Bai Z., Du Y., Vittal J.J.
Chemistry - A European Journal, 2015
18.
Crystal structure refinement withSHELXL
Sheldrick G.M.
Acta crystallographica. Section C, Structural chemistry, 2015
19.
OLEX2: a complete structure solution, refinement and analysis program
Dolomanov O.V., Bourhis L.J., Gildea R.J., Howard J.A., Puschmann H.
Journal of Applied Crystallography, 2009