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Efficient synthesis of new tricyclic pyrano[3,2-c]pyridine derivatives

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Mamedov I. G. et al. Efficient synthesis of new tricyclic pyrano[3,2-c]pyridine derivatives // Mendeleev Communications. 2019. Vol. 29. No. 2. pp. 232-233.
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Mamedov I. G., Khrustalev V. N., Dorovatovskii P. V., Naghiev F. N., Maharramov A. M. Efficient synthesis of new tricyclic pyrano[3,2-c]pyridine derivatives // Mendeleev Communications. 2019. Vol. 29. No. 2. pp. 232-233.
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TY - JOUR
DO - 10.1016/j.mencom.2019.03.040
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2019.03.040
TI - Efficient synthesis of new tricyclic pyrano[3,2-c]pyridine derivatives
T2 - Mendeleev Communications
AU - Mamedov, Ibrahim Garib
AU - Khrustalev, Victor Nikolaevich
AU - Dorovatovskii, Pavel Vladimirovich
AU - Naghiev, Farid N
AU - Maharramov, Abel M
PY - 2019
DA - 2019/03/01
PB - Mendeleev Communications
SP - 232-233
IS - 2
VL - 29
ER -
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@article{2019_Mamedov,
author = {Ibrahim Garib Mamedov and Victor Nikolaevich Khrustalev and Pavel Vladimirovich Dorovatovskii and Farid N Naghiev and Abel M Maharramov},
title = {Efficient synthesis of new tricyclic pyrano[3,2-c]pyridine derivatives},
journal = {Mendeleev Communications},
year = {2019},
volume = {29},
publisher = {Mendeleev Communications},
month = {Mar},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2019.03.040},
number = {2},
pages = {232--233},
doi = {10.1016/j.mencom.2019.03.040}
}
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Mamedov, Ibrahim Garib, et al. “Efficient synthesis of new tricyclic pyrano[3,2-c]pyridine derivatives.” Mendeleev Communications, vol. 29, no. 2, Mar. 2019, pp. 232-233. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2019.03.040.

Abstract

Reaction between arylidenemalononitriles and acetoacetanilide in the presence of piperazine hydrate in methanol at room temperature affords new tricyclic pyrano[3,2-c]pyridine derivatives of (rac-1S*,2R*,3R*,7R*,8R*,11R*)-2,11-diaryl-4,10-diimino-8-methyl-5-phenyl-6-oxo-9-oxa-5-azatricyclo-[5.3.1.03,8]undecane-1,3-dicarbonitrile family in yields of 55–84%. The molecular structures of the products were confirmed by X-ray crystallography and NMR spectroscopy.

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