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New 4,4-bis(trifluoromethyl)-4H-1,3,2-benzodioxaphosphinine 2-oxides(sulfides)

Viktor Ivanovich Dyachenko 1
Viktor Ivanovich Dyachenko
, 
Alexander Aleksandrovich Korlyukov 1
Alexander Aleksandrovich Korlyukov
10.1016/j.mencom.2019.01.030
Published 2018-12-28
Communication , Volume 29, Issue 1, 89-90
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Dyachenko V. I., Korlyukov A. A. New 4,4-bis(trifluoromethyl)-4H-1,3,2-benzodioxaphosphinine 2-oxides(sulfides) // Mendeleev Communications. 2018. Vol. 29. No. 1. pp. 89-90.
GOST all authors (up to 50) Copy
Dyachenko V. I., Korlyukov A. A. New 4,4-bis(trifluoromethyl)-4H-1,3,2-benzodioxaphosphinine 2-oxides(sulfides) // Mendeleev Communications. 2018. Vol. 29. No. 1. pp. 89-90.
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TY - JOUR
DO - 10.1016/j.mencom.2019.01.030
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2019.01.030
TI - New 4,4-bis(trifluoromethyl)-4H-1,3,2-benzodioxaphosphinine 2-oxides(sulfides)
T2 - Mendeleev Communications
AU - Dyachenko, Viktor Ivanovich
AU - Korlyukov, Alexander Aleksandrovich
PY - 2018
DA - 2018/12/28
PB - Mendeleev Communications
SP - 89-90
IS - 1
VL - 29
ER -
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@article{2018_Dyachenko,
author = {Viktor Ivanovich Dyachenko and Alexander Aleksandrovich Korlyukov},
title = {New 4,4-bis(trifluoromethyl)-4H-1,3,2-benzodioxaphosphinine 2-oxides(sulfides)},
journal = {Mendeleev Communications},
year = {2018},
volume = {29},
publisher = {Mendeleev Communications},
month = {Dec},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2019.01.030},
number = {1},
pages = {89--90},
doi = {10.1016/j.mencom.2019.01.030}
}
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Dyachenko, Viktor Ivanovich, and Alexander Aleksandrovich Korlyukov. “New 4,4-bis(trifluoromethyl)-4H-1,3,2-benzodioxaphosphinine 2-oxides(sulfides).” Mendeleev Communications, vol. 29, no. 1, Dec. 2018, pp. 89-90. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2019.01.030.

Abstract

Substituted α,α-bis(trifluoromethyl)salicylic alcohols react with dichlorido(thio)phosphates in the presence of NEt3 to afford 2-alkoxy-4,4-bis(trifluoromethyl)-4H-1,3,2-benzodioxaphosphinine 2-oxide(sulfides) in high yields. The latter can be of interest as potential cholinesterase inhibitors.

References

2.
Antineurotic effect of the hydrazide of O-β-chlorethyl-para-N-dimethylaminophenyl-phosphinylacetic acid (amphasid)
Semina I.I., Baichurina A.Z., Garaev R.S.
Bulletin of Experimental Biology and Medicine, 1996
5.
Fluorine in Medicinal Chemistry
Böhm H., Banner D., Bendels S., Kansy M., Kuhn B., Müller K., Obst-Sander U., Stahl M.
ChemBioChem, 2004
6.
10.1016/j.mencom.2019.01.030_bib0030
Hiyama
Organofluorine Compounds: Chemistry and Applications, 2000
7.
10.1016/j.mencom.2019.01.030_sbref0035a
Nifant’ev
Russ. J. Gen. Chem., 1993
8.
EXAMPLES OF 1,3,2-DIOXABENZO-PHOSPHOR(III)INANES
Nifantyev E.E., Kukhareva T.S., Dyachenko V.I., Kolomietz A.O., Magomedova N.S., Belsky V.K., Vasyanina L.K.
Phosphorus, Sulfur and Silicon and the Related Elements, 1994
9.
10.1016/j.mencom.2019.01.030_bib0040
Nifant’ev
Russ. J. Gen. Chem., 1996
10.
Perhalo Ketones. VII. Phenolic Derivatives of the Perhaloacetones
Farah B.S., Gilbert E.E., Litt M., Otto J.A., Sibilia J.P.
Journal of Organic Chemistry, 1965
11.
Characteristic features of reactions of phenolate ions with polyfluorocarbonyl compounds
Dyachenko V.I., Kolomiets A.F., Fokin A.V.
Russian Chemical Bulletin, 1988
12.
Tables of bond lengths determined by X-ray and neutron diffraction. Part 1. Bond lengths in organic compounds
Allen F.H., Kennard O., Watson D.G., Brammer L., Orpen A.G., Taylor R.
Journal of the Chemical Society Perkin Transactions 2, 1987
13.
10.1016/j.mencom.2019.01.030_bib0060
Anticholinesterase Pesticides: Metabolism, Neurotoxicity and Epidemiology, 2011
14.
10.1016/j.mencom.2019.01.030_bib0065
Sheldrick
Acta Crystallogr., 2015
15.
10.1016/j.mencom.2019.01.030_bib0070
Sheldrick
Acta Crystallogr., 2015
16.
OLEX2: a complete structure solution, refinement and analysis program
Dolomanov O.V., Bourhis L.J., Gildea R.J., Howard J.A., Puschmann H.
Journal of Applied Crystallography, 2009