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Preparation of fine powders by clathrate-forming freeze-drying: a case study of ammonium nitrate

Andrey Gennadevich Ogienko 1, 2
Andrey Gennadevich Ogienko
, 
Ekaterina G Bogdanova 2
Ekaterina G Bogdanova
, 
Andrey Sergeevich Stoporev 1, 2, 3
Andrey Sergeevich Stoporev
, 
Anna Aleksandrovna Ogienko 4, 5
Anna Aleksandrovna Ogienko
, 
Marina Petrovna Shinkorenko 1
Marina Petrovna Shinkorenko
, 
Alexander Sergeyevich Yunoshev 2, 6
Alexander Sergeyevich Yunoshev
, 
Andrei Yur'evich Manakov 1, 2
Andrei Yur'evich Manakov
10.1016/j.mencom.2018.03.035
Published 2018-03-01
Communication , Volume 28, Issue 2, 211-213
6
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Ogienko A. G. et al. Preparation of fine powders by clathrate-forming freeze-drying: a case study of ammonium nitrate // Mendeleev Communications. 2018. Vol. 28. No. 2. pp. 211-213.
GOST all authors (up to 50) Copy
Ogienko A. G., Bogdanova E. G., Stoporev A. S., Ogienko A. A., Shinkorenko M. P., Yunoshev A. S., Manakov A. Y. Preparation of fine powders by clathrate-forming freeze-drying: a case study of ammonium nitrate // Mendeleev Communications. 2018. Vol. 28. No. 2. pp. 211-213.
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TY - JOUR
DO - 10.1016/j.mencom.2018.03.035
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2018.03.035
TI - Preparation of fine powders by clathrate-forming freeze-drying: a case study of ammonium nitrate
T2 - Mendeleev Communications
AU - Ogienko, Andrey Gennadevich
AU - Bogdanova, Ekaterina G
AU - Stoporev, Andrey Sergeevich
AU - Ogienko, Anna Aleksandrovna
AU - Shinkorenko, Marina Petrovna
AU - Yunoshev, Alexander Sergeyevich
AU - Manakov, Andrei Yur'evich
PY - 2018
DA - 2018/03/01
PB - Mendeleev Communications
SP - 211-213
IS - 2
VL - 28
ER -
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@article{2018_Ogienko,
author = {Andrey Gennadevich Ogienko and Ekaterina G Bogdanova and Andrey Sergeevich Stoporev and Anna Aleksandrovna Ogienko and Marina Petrovna Shinkorenko and Alexander Sergeyevich Yunoshev and Andrei Yur'evich Manakov},
title = {Preparation of fine powders by clathrate-forming freeze-drying: a case study of ammonium nitrate},
journal = {Mendeleev Communications},
year = {2018},
volume = {28},
publisher = {Mendeleev Communications},
month = {Mar},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2018.03.035},
number = {2},
pages = {211--213},
doi = {10.1016/j.mencom.2018.03.035}
}
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Ogienko, Andrey Gennadevich, et al. “Preparation of fine powders by clathrate-forming freeze-drying: a case study of ammonium nitrate.” Mendeleev Communications, vol. 28, no. 2, Mar. 2018, pp. 211-213. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2018.03.035.

Abstract

Fine powders of ammonium nitrate were prepared by the freeze-drying of a solution in a THF–water mixture. Freezing gives a THF hydrate and dispersed ammonium nitrate particles; the THF hydrate can be then removed by sublimation to leave fine ammonium nitrate powder. To optimize the process, the stability of cubic structure II THF clathrate hydrate in the presence of ammonium nitrate was studied by X-ray diffraction and thermal analysis.

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