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Synthesis of tritium-labeled PAM-43

Igor Yulianovich Nagaev 1
Igor Yulianovich Nagaev
, 
Konstantin Valer'evich Shevchenko 1
Konstantin Valer'evich Shevchenko
, 
Valerii Pavlovich Shevchenko 1
Valerii Pavlovich Shevchenko
, 
Nikolai Fedorovich Myasoedov 1
Nikolai Fedorovich Myasoedov
, 
Vladimir Viktorovich Grigoriev 2
Vladimir Viktorovich Grigoriev
, 
Mstislav Igorevich Lavrov 3
Mstislav Igorevich Lavrov
, 
Ekaterina V Bondarenko 4
Ekaterina V Bondarenko
, 
Elena Evgen'evna Kalashnikova 4
Elena Evgen'evna Kalashnikova
10.1016/j.mencom.2018.01.021
Published 2017-12-22
Communication , Volume 28, Issue 1, 64-65
5
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Nagaev I. Y. et al. Synthesis of tritium-labeled PAM-43 // Mendeleev Communications. 2017. Vol. 28. No. 1. pp. 64-65.
GOST all authors (up to 50) Copy
Nagaev I. Y., Shevchenko K. V., Shevchenko V. P., Myasoedov N. F., Grigoriev V. V., Lavrov M. I., Bondarenko E. V., Kalashnikova E. E. Synthesis of tritium-labeled PAM-43 // Mendeleev Communications. 2017. Vol. 28. No. 1. pp. 64-65.
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TY - JOUR
DO - 10.1016/j.mencom.2018.01.021
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2018.01.021
TI - Synthesis of tritium-labeled PAM-43
T2 - Mendeleev Communications
AU - Nagaev, Igor Yulianovich
AU - Shevchenko, Konstantin Valer'evich
AU - Shevchenko, Valerii Pavlovich
AU - Myasoedov, Nikolai Fedorovich
AU - Grigoriev, Vladimir Viktorovich
AU - Lavrov, Mstislav Igorevich
AU - Bondarenko, Ekaterina V
AU - Kalashnikova, Elena Evgen'evna
PY - 2017
DA - 2017/12/22
PB - Mendeleev Communications
SP - 64-65
IS - 1
VL - 28
ER -
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@article{2017_Nagaev,
author = {Igor Yulianovich Nagaev and Konstantin Valer'evich Shevchenko and Valerii Pavlovich Shevchenko and Nikolai Fedorovich Myasoedov and Vladimir Viktorovich Grigoriev and Mstislav Igorevich Lavrov and Ekaterina V Bondarenko and Elena Evgen'evna Kalashnikova},
title = {Synthesis of tritium-labeled PAM-43},
journal = {Mendeleev Communications},
year = {2017},
volume = {28},
publisher = {Mendeleev Communications},
month = {Dec},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2018.01.021},
number = {1},
pages = {64--65},
doi = {10.1016/j.mencom.2018.01.021}
}
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Nagaev, Igor Yulianovich, et al. “Synthesis of tritium-labeled PAM-43.” Mendeleev Communications, vol. 28, no. 1, Dec. 2017, pp. 64-65. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2018.01.021.

Abstract

The deuterium- and tritium-labeled PAM-43 was obtained in 23% yield and with a specific radioactivity of 132 Ci mmol–1. As determined by mass spectrometry, a PAM-43 molecule contained 80% of deuterium in 2,3-dihydrobenzofuran fragments, while the central fragment contained 20% of deuterium.

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