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A new synthesis of a nitroimino-containing 1,2,4-triazin-5-one from 3-bromo-3-nitropropenoates

Valentina Mikhailovna Berestovitskaya 1
Valentina Mikhailovna Berestovitskaya
, 
Olga Yur'evna Ozerova 1
Olga Yur'evna Ozerova
, 
Tatiana Petrovna Efimova 1
Tatiana Petrovna Efimova
, 
Vladislav V Gurzhiy 2
Vladislav V Gurzhiy
, 
Tamara Aleksandrovna Novikova 1
Tamara Aleksandrovna Novikova
10.1016/j.mencom.2016.07.019
Published 2016-07-07
Communication , Volume 26, Issue 4, 323-325
13
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Berestovitskaya V. M. et al. A new synthesis of a nitroimino-containing 1,2,4-triazin-5-one from 3-bromo-3-nitropropenoates // Mendeleev Communications. 2016. Vol. 26. No. 4. pp. 323-325.
GOST all authors (up to 50) Copy
Berestovitskaya V. M., Ozerova O. Y., Efimova T. P., Gurzhiy V. V., Novikova T. A. A new synthesis of a nitroimino-containing 1,2,4-triazin-5-one from 3-bromo-3-nitropropenoates // Mendeleev Communications. 2016. Vol. 26. No. 4. pp. 323-325.
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TY - JOUR
DO - 10.1016/j.mencom.2016.07.019
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2016.07.019
TI - A new synthesis of a nitroimino-containing 1,2,4-triazin-5-one from 3-bromo-3-nitropropenoates
T2 - Mendeleev Communications
AU - Berestovitskaya, Valentina Mikhailovna
AU - Ozerova, Olga Yur'evna
AU - Efimova, Tatiana Petrovna
AU - Gurzhiy, Vladislav V
AU - Novikova, Tamara Aleksandrovna
PY - 2016
DA - 2016/07/07
PB - Mendeleev Communications
SP - 323-325
IS - 4
VL - 26
ER -
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@article{2016_Berestovitskaya,
author = {Valentina Mikhailovna Berestovitskaya and Olga Yur'evna Ozerova and Tatiana Petrovna Efimova and Vladislav V Gurzhiy and Tamara Aleksandrovna Novikova},
title = {A new synthesis of a nitroimino-containing 1,2,4-triazin-5-one from 3-bromo-3-nitropropenoates},
journal = {Mendeleev Communications},
year = {2016},
volume = {26},
publisher = {Mendeleev Communications},
month = {Jul},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2016.07.019},
number = {4},
pages = {323--325},
doi = {10.1016/j.mencom.2016.07.019}
}
MLA
Cite this
MLA Copy
Berestovitskaya, Valentina Mikhailovna, et al. “A new synthesis of a nitroimino-containing 1,2,4-triazin-5-one from 3-bromo-3-nitropropenoates.” Mendeleev Communications, vol. 26, no. 4, Jul. 2016, pp. 323-325. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2016.07.019.

Abstract

Reaction of 1-amino-2-nitroguanidine with alkyl 3-bromo-3-nitropropenoates affords 3-nitroimino-6-nitromethyl-4,5-dihydro-(2H)-1,2,4-triazin-5-one, whose structure was characterized by IR, UV, NMR spectroscopy and X-ray single crystal analysis.

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