Home / Publications / High-resolution mass spectra of biotinylated, HEG-spacered molecular probes with oligosaccharide fragments of the capsular polysaccharides from Streptococcus pneumoniae

High-resolution mass spectra of biotinylated, HEG-spacered molecular probes with oligosaccharide fragments of the capsular polysaccharides from Streptococcus pneumoniae

Alexander Olegovich Chizhov 1
Alexander Olegovich Chizhov
, 
Elena Victorovna Sukhova 1
Elena Victorovna Sukhova
, 
Elena Aleksandrovna Khatuntseva 1
Elena Aleksandrovna Khatuntseva
, 
Yury Evgen'evich Tsvetkov 1
Yury Evgen'evich Tsvetkov
, 
Nikolay Eduardovich Nifantiev 1
Nikolay Eduardovich Nifantiev
10.1016/j.mencom.2015.11.020
Published 2015-11-09
Communication , Volume 25, Issue 6, 457-459
8
Share
Cite this
GOST
 | 
Cite this
GOST Copy
Chizhov A. O. et al. High-resolution mass spectra of biotinylated, HEG-spacered molecular probes with oligosaccharide fragments of the capsular polysaccharides from Streptococcus pneumoniae // Mendeleev Communications. 2015. Vol. 25. No. 6. pp. 457-459.
GOST all authors (up to 50) Copy
Chizhov A. O., Sukhova E. V., Khatuntseva E. A., Tsvetkov Y. E., Nifantiev N. E. High-resolution mass spectra of biotinylated, HEG-spacered molecular probes with oligosaccharide fragments of the capsular polysaccharides from Streptococcus pneumoniae // Mendeleev Communications. 2015. Vol. 25. No. 6. pp. 457-459.
RIS
 | 
Cite this
RIS Copy
TY - JOUR
DO - 10.1016/j.mencom.2015.11.020
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2015.11.020
TI - High-resolution mass spectra of biotinylated, HEG-spacered molecular probes with oligosaccharide fragments of the capsular polysaccharides from Streptococcus pneumoniae
T2 - Mendeleev Communications
AU - Chizhov, Alexander Olegovich
AU - Sukhova, Elena Victorovna
AU - Khatuntseva, Elena Aleksandrovna
AU - Tsvetkov, Yury Evgen'evich
AU - Nifantiev, Nikolay Eduardovich
PY - 2015
DA - 2015/11/09
PB - Mendeleev Communications
SP - 457-459
IS - 6
VL - 25
ER -
BibTex
 | 
Cite this
BibTex (up to 50 authors) Copy
@article{2015_Chizhov,
author = {Alexander Olegovich Chizhov and Elena Victorovna Sukhova and Elena Aleksandrovna Khatuntseva and Yury Evgen'evich Tsvetkov and Nikolay Eduardovich Nifantiev},
title = {High-resolution mass spectra of biotinylated, HEG-spacered molecular probes with oligosaccharide fragments of the capsular polysaccharides from Streptococcus pneumoniae},
journal = {Mendeleev Communications},
year = {2015},
volume = {25},
publisher = {Mendeleev Communications},
month = {Nov},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2015.11.020},
number = {6},
pages = {457--459},
doi = {10.1016/j.mencom.2015.11.020}
}
MLA
Cite this
MLA Copy
Chizhov, Alexander Olegovich, et al. “High-resolution mass spectra of biotinylated, HEG-spacered molecular probes with oligosaccharide fragments of the capsular polysaccharides from Streptococcus pneumoniae.” Mendeleev Communications, vol. 25, no. 6, Nov. 2015, pp. 457-459. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2015.11.020.

Abstract

High-resolution electrospray mass spectra (MS and MS/MS) of biotinylated, hexaethylene glycol (HEG) spacered molecular probes bearing immunogenic oligosaccharides, fragments of capsular polysaccharides of Streptococcus pneumoniae, were interpreted (four examples). Characteristic fragmentation of the aglycone at the end of the HEG chain distant from the biotin fragment has been revealed.

References

1.
Carbohydrates in Chemistry and Biology. Part I: Chemistry of Sac- charides, vols. 1 and 2, Part II: Biology of Saccharides, vols. 3 and 4, eds. B. Ernst, G.W. Hart and P. Sinay, Wiley-VCH, Weinheim, 2000.
3.
Synthesis and Molecular Recognition Studies of the HNK-1 Trisaccharide and Related Oligosaccharides. The Specificity of Monoclonal Anti-HNK-1 Antibodies as Assessed by Surface Plasmon Resonance and STD NMR
Tsvetkov Y.E., Burg-Roderfeld M., Loers G., Ardá A., Sukhova E.V., Khatuntseva E.A., Grachev A.A., Chizhov A.O., Siebert H., Schachner M., Jiménez-Barbero J., Nifantiev N.E.
Journal of the American Chemical Society, 2011
4.
Ananikov V.P., Khokhlova E.A., Egorov M.P., Sakharov A.M., Zlotin S.G., Kucherov A.V., Kustov L.M., Gening M.L., Nifantiev N.E.
Mendeleev Communications, 2015
5.
GlycoChip: multiarray for the study of carbohydrate-binding proteins
Galanina O.E., Mecklenburg M., Nifantiev N.E., Pazynina G.V., Bovin N.V.
Lab on a Chip, 2003
10.
Synthesis of the capsular polysaccharide of type 14
Kochetkov N.K., Nifant'ev N.E., Backinowsky L.V.
Tetrahedron, 1987
11.
Synthesis of derivatives of 2-amino-2-deoxy-4-O-(α- and β-d-galactopyranosyl)-d-glucose
Nifant'ev N.E., Backinowsky L.V., Kochetkov N.K.
Carbohydrate Research, 1988
12.
Belyakov P.A., Kadentsev V.I., Chizhov A.O., Kolotyrkina N.G., Shashkov A.S., Ananikov V.P.
Mendeleev Communications, 2010
13.
Przybył A.K., Nowakowska Z.
Mendeleev Communications, 2013
14.
10.1016/j.mencom.2015.11.020_bib0055
Kochetkov
Adv. Carbohydr. Chem., 1966
16.
Mass spectrometric analysis of carbohydrates labeled with a biotinylated tag
Kapková P.
Rapid Communications in Mass Spectrometry, 2009
17.
10.1016/j.mencom.2015.11.020_bib0070
Ardrey
Liquid Chromatography – Mass Spectrometry: An Introduction, 2003
19.
Mass spectrometry of oligosaccharides
Zaia J.
Mass Spectrometry Reviews, 2004