Abstract
A new one-pot synthesis of e-spirocyclopropyl-e-caprolactones has been implemented via the reaction between vinylarenes, EtAlCl2 and dimethyl adipate catalyzed by Cp2ZrCl2 in 60% yield.
References
1.
Liu R.
Pure and Applied Chemistry,
2001
2.
Xavier N.M., Rauter A.P., Queneau Y.
Topics in Current Chemistry,
2010
3.
Takeda K., Imaoka I., Yoshii E.
Tetrahedron,
1994
4.
Shulishov E.V., Tomilov Y.V., Nefedov O.M.
Mendeleev Communications,
2013
5.
Elinson M.N., Ilovaisky A.I., Merkulova V.M., Zaimovskaya T.A., Nikishin G.I.
Mendeleev Communications,
2012
6.
Zheng J., Li Y.
Mendeleev Communications,
2012
7.
Ukhin L.Y., Belousova L.V., Shepelenko E.N., Morkovnik A.S.
Mendeleev Communications,
2013
8.
Stolyarenko V.Y., Evdokimov A.A., Shishkin V.I.
Mendeleev Communications,
2013
9.
Stolyarenko V.Y., Evdokimov A.A., Shishkin V.I.
Mendeleev Communications,
2013
10.
Sannigrahi M.
Tetrahedron,
1999
11.
M.D. Mashkovskii, Lekarstvennye sredstva (Drugs), 10th edn., Meditsina, Moscow, 1986, ch. 1, p. 491 (in Russian).
12.
Gella I.M., Sergienko L.Y., Cherevko A.N.
Pharmaceutical Chemistry Journal,
1990
13.
Dzhemilev U.M., Khafizova L.O., Gubaidullin R.R., Khalilov L.M., Ibragimov A.G.
Tetrahedron Letters,
2009
14.
Khafizova L.O., Gubaidullin R.R., Dzhemilev U.M.
Tetrahedron,
2011
15.
10.1016/j.mencom.2014.06.013_bib0075
Gordon
The Chemist's Companion,
1972
16.
Dolomanov O.V., Bourhis L.J., Gildea R.J., Howard J.A., Puschmann H.
Journal of Applied Crystallography,
2009
17.
Sheldrick G.M.
Acta Crystallographica Section A Foundations of Crystallography,
2007