Keywords
aliphatic primary amine; ansa-bis(amidinate); multinuclear lithium
Abstract
A practical synthetic pathway to alkyl-ended ansa-bis(amidinate) ligands was developed via linking the freshly prepared aliphatic group substituted lithium amidinate and the subsequent deprotonation. The lithium complexes prepared by this method were characterized by NMR spectroscopy, elemental analysis and single-crystal X-ray diffraction analysis.
References
1.
Barker J., Kilner M.
Coordination Chemistry Reviews,
1994
2.
Edelmann F.T.
Coordination Chemistry Reviews,
1994
3.
Mohamed A.A.
Coordination Chemistry Reviews,
2010
4.
Chernega A.N., Gómez R., Green M.L.
Journal of the Chemical Society Chemical Communications,
1993
5.
Dick D.G., Edema J.J., Duchateau R., Gambarotta S.
Inorganic Chemistry,
1993
6.
Ward B.D., Risler H., Weitershaus K., Bellemin-Laponnaz S., Wadepohl H., Gade L.H.
Inorganic Chemistry,
2006
7.
Aharonovich S., Botoshansky M., Waymouth R.M., Eisen M.S.
Inorganic Chemistry,
2010
8.
Aharonovich S., Kapon M., Botoshanski M., Eisen M.S.
Organometallics,
2008
9.
Whitener G.D., Hagadorn J.R., Arnold J.
Journal of the Chemical Society Dalton Transactions,
1999
10.
Hagadorn J.R., Arnold J.
Angewandte Chemie - International Edition,
1998
11.
Bambirra S., Meetsma A., Hessen B., Teuben J.H.
Organometallics,
2001
12.
Ge S., Meetsma A., Hessen B.
Organometallics,
2008
13.
14.
Epshteyn A., Trunkely E.F., Kissounko D.A., Fettinger J.C., Sita L.R.
Organometallics,
2009
15.
Schnutenhaus H., Brintzinger H.H.
1979
16.
Wang J., Xu F., Cai T., Shen Q.
Organic Letters,
2008
17.
Li W., Xue M., Xu F., Tu J., Zhang Y., Shen Q.
Dalton Transactions,
2012
18.
Li J., Huang S., Weng L., Liu D.
European Journal of Inorganic Chemistry,
2003
19.
Li J., Huang S., Weng L., Liu D.
Journal of Organometallic Chemistry,
2006
20.
Kawaguchi H., Matsuo T.
Chemical Communications,
2002
21.
Yakovenko M.V., Trifonov A.A., Kirillov E., Roisnel T., Carpentier J.
Inorganica Chimica Acta,
2012
22.
Tolpygin A.O., Shavyrin A.S., Cherkasov A.V., Fukin G.K., Trifonov A.A.
Organometallics,
2012
23.
Bai S., Guo J., Liu D.
Dalton Transactions,
2006
24.
Bai S., Guo J., Liu D., Wong W.
European Journal of Inorganic Chemistry,
2006
25.
Bai S., Tong H., Guo J., Zhou M., Liu D.
Inorganica Chimica Acta,
2009
26.
Bai S., Tong H., Guo J., Zhou M., Liu D., Yuan S.
Polyhedron,
2010
27.
Bai S., Guan F., Hu M., Yuan S., Guo J., Liu D.
Dalton Transactions,
2011
28.
Mao J., Wang T., Liu R., Bai S., Guo J., Liu D.
Mendeleev Communications,
2013
29.
Segmüller T., Schlüter P.A., Drees M., Schier A., Nogai S., Mitzel N.W., Straßner T., Karsch H.H.
Journal of Organometallic Chemistry,
2007
30.
Zhou M., Song Y., Gong T., Tong H., Guo J., Weng L., Liu D.
Inorganic Chemistry,
2008
31.
Zhou M., Gong T., Qiao X., Tong H., Guo J., Liu D.
Inorganic Chemistry,
2011