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Synthesis of 17-(1,2,3-dithiazole) androstene derivatives

Stanislav Anatol'evich Amelichev 1
Stanislav Anatol'evich Amelichev
, 
Alexander Stepanovich Shashkov 1
Alexander Stepanovich Shashkov
, 
Igor Viktorovich Zavarzin 1
Igor Viktorovich Zavarzin
, 
Oleg Alexeevich Rakitin 1
Oleg Alexeevich Rakitin
10.1016/j.mencom.2011.07.003
Published 2011-07-01
Communication , Volume 21, Issue 4, 186-187
10
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Amelichev S. A. et al. Synthesis of 17-(1,2,3-dithiazole) androstene derivatives // Mendeleev Communications. 2011. Vol. 21. No. 4. pp. 186-187.
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Amelichev S. A., Shashkov A. S., Zavarzin I. V., Rakitin O. A. Synthesis of 17-(1,2,3-dithiazole) androstene derivatives // Mendeleev Communications. 2011. Vol. 21. No. 4. pp. 186-187.
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TY - JOUR
DO - 10.1016/j.mencom.2011.07.003
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2011.07.003
TI - Synthesis of 17-(1,2,3-dithiazole) androstene derivatives
T2 - Mendeleev Communications
AU - Amelichev, Stanislav Anatol'evich
AU - Shashkov, Alexander Stepanovich
AU - Zavarzin, Igor Viktorovich
AU - Rakitin, Oleg Alexeevich
PY - 2011
DA - 2011/07/01
PB - Mendeleev Communications
SP - 186-187
IS - 4
VL - 21
ER -
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@article{2011_Amelichev,
author = {Stanislav Anatol'evich Amelichev and Alexander Stepanovich Shashkov and Igor Viktorovich Zavarzin and Oleg Alexeevich Rakitin},
title = {Synthesis of 17-(1,2,3-dithiazole) androstene derivatives},
journal = {Mendeleev Communications},
year = {2011},
volume = {21},
publisher = {Mendeleev Communications},
month = {Jul},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2011.07.003},
number = {4},
pages = {186--187},
doi = {10.1016/j.mencom.2011.07.003}
}
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Amelichev, Stanislav Anatol'evich, et al. “Synthesis of 17-(1,2,3-dithiazole) androstene derivatives.” Mendeleev Communications, vol. 21, no. 4, Jul. 2011, pp. 186-187. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2011.07.003.

Keywords

1,2,3-dithiazoles
acetoximes
androstene derivatives
determination of configuration
synthesis

Abstract

17-(1,2,3-Dithiazole) androstene derivatives were synthesized from commercially available Pregnenolone acetate involving the reaction between 3b-acetoxy-20-hydroxyimino-5-pregnene with sulfur monochloride as the key step.

References

7.
Highly stereoselective synthesis of steroidal 2,5-diketopiperazines based on isocyanide chemistry
Bruttomesso A.C., Eiras J., Ramírez J.A., Galagovsky L.R.
Tetrahedron Letters, 2009
9.
O. A. Rakitin, in Comprehensive Heterocyclic Chemistry III, eds. A. R. Katritzky, C.A. Ramsden, E.F. V. Scriven and R. J. K. Taylor, Elsevier, Oxford, 2008, vol. 6, p. 1.
10.
One-pot synthesis of 5-phenylimino, 5-thieno or 5-oxo-1,2,3-dithiazoles and evaluation of their antimicrobial and antitumor activity
Konstantinova L.S., Bol’shakov O.I., Obruchnikova N.V., Laborie H., Tanga A., Sopéna V., Lanneluc I., Picot L., Sablé S., Thiéry V., Rakitin O.A.
Bioorganic and Medicinal Chemistry Letters, 2009
12.
10.1016/j.mencom.2011.07.003_bib0060
Emayan
Bull. Soc. Chim. Belg., 1997
14.
O. I. Bol'shakov, PhD Thesis, 2009, N.D. Zelinsky Institute of Organic Chemistry RAS, Moscow.
15.
D. M. McKinnon, in Comprehensive Heterocyclic Chemistry II, ed. I. Shinkai, Pergamon, Oxford, 1996, vol. 3, p. 571.