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Condensation of 5,7-dimethyl-4a,7a-diphenyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazin-6-one with halogenoacetic acids

Sergei Vitalyevich Vasilevskii 1
Sergei Vitalyevich Vasilevskii
, 
Pavel Alekseevich Belyakov 1
Pavel Alekseevich Belyakov
, 
Galina Anatol'evna Gazieva 1
Galina Anatol'evna Gazieva
,  , 
Natal'ya Georgievna Kolotyrkina 1
Natal'ya Georgievna Kolotyrkina
, 
Angelina Nikolaevna Kravchenko 1
Angelina Nikolaevna Kravchenko
10.1016/j.mencom.2010.01.018
Published 2009-12-30
Communication , Volume 20, Issue 1, 47-49
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Vasilevskii S. V. et al. Condensation of 5,7-dimethyl-4a,7a-diphenyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazin-6-one with halogenoacetic acids // Mendeleev Communications. 2009. Vol. 20. No. 1. pp. 47-49.
GOST all authors (up to 50) Copy
Vasilevskii S. V., Belyakov P. A., Gazieva G. A., Nelyubina Y. V., Kolotyrkina N. G., Kravchenko A. N. Condensation of 5,7-dimethyl-4a,7a-diphenyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazin-6-one with halogenoacetic acids // Mendeleev Communications. 2009. Vol. 20. No. 1. pp. 47-49.
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TY - JOUR
DO - 10.1016/j.mencom.2010.01.018
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2010.01.018
TI - Condensation of 5,7-dimethyl-4a,7a-diphenyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazin-6-one with halogenoacetic acids
T2 - Mendeleev Communications
AU - Vasilevskii, Sergei Vitalyevich
AU - Belyakov, Pavel Alekseevich
AU - Gazieva, Galina Anatol'evna
AU - Nelyubina, Yulia Vladimirovna
AU - Kolotyrkina, Natal'ya Georgievna
AU - Kravchenko, Angelina Nikolaevna
PY - 2009
DA - 2009/12/30
PB - Mendeleev Communications
SP - 47-49
IS - 1
VL - 20
ER -
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@article{2009_Vasilevskii,
author = {Sergei Vitalyevich Vasilevskii and Pavel Alekseevich Belyakov and Galina Anatol'evna Gazieva and Yulia Vladimirovna Nelyubina and Natal'ya Georgievna Kolotyrkina and Angelina Nikolaevna Kravchenko},
title = {Condensation of 5,7-dimethyl-4a,7a-diphenyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazin-6-one with halogenoacetic acids},
journal = {Mendeleev Communications},
year = {2009},
volume = {20},
publisher = {Mendeleev Communications},
month = {Dec},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2010.01.018},
number = {1},
pages = {47--49},
doi = {10.1016/j.mencom.2010.01.018}
}
MLA
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Vasilevskii, Sergei Vitalyevich, et al. “Condensation of 5,7-dimethyl-4a,7a-diphenyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazin-6-one with halogenoacetic acids.” Mendeleev Communications, vol. 20, no. 1, Dec. 2009, pp. 47-49. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2010.01.018.

Abstract

The reaction of 5,7-dimethyl-4a,7a-diphenyl-3-thioxoperhydroimidazo[4,5-e]-1,2,4-triazin-6-one with halogenoacetic acids was studied, and the directed synthesis of {(5,7-dimethyl-6-oxo-4a,7a-diphenyl-4,4a,5,6,7,7a-hexahydro-1H-imidazo[4,5-e]-1,2,4-triazin-3-yl)thio}acetic acid and 1,3-dimethyl-3a,9a-diphenyl-3,3a,9,9a-tetrahydroimidazo[4,5-e]-1,3-thiazolo[3,2-b]-1,2,4-triazine-2,7(1H,6H)-dione was perfomed for the first time; the structures of title compounds were confirmed by the 1H-{13C} HMBC, 1H-{15N} HSQC, TOCSY, NOESY, HMBC, HSQCED NMR spectroscopy methods and XRD analysis of the tricyclic product.

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