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Synthesis, structure and thermal decomposition of cycloalkanone enamine peroxides

Evgenii Kuz'mich Starostin ¹

Evgenii Kuz'mich Starostin

Victor Nikolaevich Khrustalev ²

Victor Nikolaevich Khrustalev

0000-0001-8806-2975

Mikhail Yuvenal'evich Antipin ²

Mikhail Yuvenal'evich Antipin

Andrei Vitalievich Lalov ¹

Andrei Vitalievich Lalov

¹ N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, Russian Federation

² A.N. Nesmeyanov Institute of Organoelement Compounds of Russian Academy of Sciences, Moscow, Russian Federation

10.1016/j.mencom.2009.11.014

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Published 2009-11-02

Communication , Volume 19, Issue 6, 334-336

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Starostin E. K. et al. Synthesis, structure and thermal decomposition of cycloalkanone enamine peroxides // Mendeleev Communications. 2009. Vol. 19. No. 6. pp. 334-336.

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Starostin E. K., Khrustalev V. N., Antipin M. Y., Lalov A. V. Synthesis, structure and thermal decomposition of cycloalkanone enamine peroxides // Mendeleev Communications. 2009. Vol. 19. No. 6. pp. 334-336.

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TY - JOUR

DO - 10.1016/j.mencom.2009.11.014

UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2009.11.014

TI - Synthesis, structure and thermal decomposition of cycloalkanone enamine peroxides

T2 - Mendeleev Communications

AU - Starostin, Evgenii Kuz'mich

AU - Khrustalev, Victor Nikolaevich

AU - Antipin, Mikhail Yuvenal'evich

AU - Lalov, Andrei Vitalievich

PY - 2009

DA - 2009/11/02

PB - Mendeleev Communications

SP - 334-336

IS - 6

VL - 19

ER -

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@article{2009_Starostin,

author = {Evgenii Kuz'mich Starostin and Victor Nikolaevich Khrustalev and Mikhail Yuvenal'evich Antipin and Andrei Vitalievich Lalov},

title = {Synthesis, structure and thermal decomposition of cycloalkanone enamine peroxides},

journal = {Mendeleev Communications},

year = {2009},

volume = {19},

publisher = {Mendeleev Communications},

month = {Nov},

url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2009.11.014},

number = {6},

pages = {334--336},

doi = {10.1016/j.mencom.2009.11.014}

}

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Starostin, Evgenii Kuz'mich, et al. “Synthesis, structure and thermal decomposition of cycloalkanone enamine peroxides.” Mendeleev Communications, vol. 19, no. 6, Nov. 2009, pp. 334-336. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2009.11.014.

Abstract

Reactions of cycloalkanone enamines with H₂O₂ gave bis(1-morpholinocyclopent-1-yl)- and bis(1-morpholinocyclohex-1-yl)-peroxides, which were studied by NMR spectroscopy and X-ray diffraction. Thermolysis of bis(1-morpholinocyclohex-1-yl)-peroxide in n-hexane resulted in two major products, viz., cyclohexanone and morpholine.