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Regiodirected synthesis of hydroazolic compounds with the use of thiosemicarbazide

Alexander Andreevich Anis'kov 1
Alexander Andreevich Anis'kov
, 
Anton Alekseevich Sazonov 2
Anton Alekseevich Sazonov
, 
Iraida Nikolaevna Klochkova 1
Iraida Nikolaevna Klochkova
10.1016/j.mencom.2009.01.021
Published 2009-01-19
Communication , Volume 19, Issue 1, 52-53
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Anis'kov A. A., Sazonov A. A., Klochkova I. N. Regiodirected synthesis of hydroazolic compounds with the use of thiosemicarbazide // Mendeleev Communications. 2009. Vol. 19. No. 1. pp. 52-53.
GOST all authors (up to 50) Copy
Anis'kov A. A., Sazonov A. A., Klochkova I. N. Regiodirected synthesis of hydroazolic compounds with the use of thiosemicarbazide // Mendeleev Communications. 2009. Vol. 19. No. 1. pp. 52-53.
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TY - JOUR
DO - 10.1016/j.mencom.2009.01.021
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2009.01.021
TI - Regiodirected synthesis of hydroazolic compounds with the use of thiosemicarbazide
T2 - Mendeleev Communications
AU - Anis'kov, Alexander Andreevich
AU - Sazonov, Anton Alekseevich
AU - Klochkova, Iraida Nikolaevna
PY - 2009
DA - 2009/01/19
PB - Mendeleev Communications
SP - 52-53
IS - 1
VL - 19
ER -
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@article{2009_Anis'kov,
author = {Alexander Andreevich Anis'kov and Anton Alekseevich Sazonov and Iraida Nikolaevna Klochkova},
title = {Regiodirected synthesis of hydroazolic compounds with the use of thiosemicarbazide},
journal = {Mendeleev Communications},
year = {2009},
volume = {19},
publisher = {Mendeleev Communications},
month = {Jan},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2009.01.021},
number = {1},
pages = {52--53},
doi = {10.1016/j.mencom.2009.01.021}
}
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Anis'kov, Alexander Andreevich, et al. “Regiodirected synthesis of hydroazolic compounds with the use of thiosemicarbazide.” Mendeleev Communications, vol. 19, no. 1, Jan. 2009, pp. 52-53. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2009.01.021.

Abstract

Interaction of α,β-unsaturated ketones of furan series with thiosemicarbazide under basic catalysis leads to 3-furyl-2-thiocarbamoylpyrazolines since nitrous nucleophilic centre of a reagent is activated, whereas the products of intermolecular cyclization of thiosemicarbazones under conditions of acid activation of sulfureous nucleophile are spirocyclic furylmethylene-1,3,4-thiadiazolines.

References

1.
10.1016/j.mencom.2009.01.021_bib1
Klochkova
Izv. Vuzov. Khim. Khim. Tekhnol., 2005
2.
10.1016/j.mencom.2009.01.021_bib2
Sazonov
Izv. Vuzov. Khim. Khim. Tekhnol., 2005