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Synthesis, characterisation and crystal structure of 3,5-dimethylpyrazole-1-carbothioic acid amide

Sukhvinder Kaur Chawla 1
Sukhvinder Kaur Chawla
, 
Simrat Kaur 1
Simrat Kaur
, 
Nidhi Gupta 1
Nidhi Gupta
, 
Geeta Hundal 1
Geeta Hundal
10.1016/j.mencom.2007.11.012
Published 2007-11-09
Communication , Volume 17, Issue 6, 335-336
3
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Chawla S. K. et al. Synthesis, characterisation and crystal structure of 3,5-dimethylpyrazole-1-carbothioic acid amide // Mendeleev Communications. 2007. Vol. 17. No. 6. pp. 335-336.
GOST all authors (up to 50) Copy
Chawla S. K., Kaur S., Gupta N., Hundal G. Synthesis, characterisation and crystal structure of 3,5-dimethylpyrazole-1-carbothioic acid amide // Mendeleev Communications. 2007. Vol. 17. No. 6. pp. 335-336.
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TY - JOUR
DO - 10.1016/j.mencom.2007.11.012
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2007.11.012
TI - Synthesis, characterisation and crystal structure of 3,5-dimethylpyrazole-1-carbothioic acid amide
T2 - Mendeleev Communications
AU - Chawla, Sukhvinder Kaur
AU - Kaur, Simrat
AU - Gupta, Nidhi
AU - Hundal, Geeta
PY - 2007
DA - 2007/11/09
PB - Mendeleev Communications
SP - 335-336
IS - 6
VL - 17
ER -
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@article{2007_Chawla,
author = {Sukhvinder Kaur Chawla and Simrat Kaur and Nidhi Gupta and Geeta Hundal},
title = {Synthesis, characterisation and crystal structure of 3,5-dimethylpyrazole-1-carbothioic acid amide},
journal = {Mendeleev Communications},
year = {2007},
volume = {17},
publisher = {Mendeleev Communications},
month = {Nov},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2007.11.012},
number = {6},
pages = {335--336},
doi = {10.1016/j.mencom.2007.11.012}
}
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Chawla, Sukhvinder Kaur, et al. “Synthesis, characterisation and crystal structure of 3,5-dimethylpyrazole-1-carbothioic acid amide.” Mendeleev Communications, vol. 17, no. 6, Nov. 2007, pp. 335-336. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2007.11.012.

Abstract

3,5-Dimethylpyrazole-1-carbothioic acid amide was obtained (along with acetyl thiosemicarbazide) by the condensation of acetylacetone with thiosemicarbazide and characterised through X-ray diffraction and spectral studies.

References

2.
Copper(II) and Cobalt(III) Pyridoxal Thiosemicarbazone Complexes with Nitroprusside as Counterion:  Syntheses, Electronic Properties, and Antileukemic Activity
Belicchi-Ferrari M., Bisceglie F., Casoli C., Durot S., Morgenstern-Badarau I., Pelosi G., Pilotti E., Pinelli S., Tarasconi P.
Journal of Medicinal Chemistry, 2005
3.
Fluorescence studies of the intra-cellular distribution of zinc bis(thiosemicarbazone) complexes in human cancer cells.
Cowley A.R., Davis J., Dilworth J.R., Donnelly P.S., Dobson R., Nightingale A., Peach J.M., Shore B., Kerr D., Seymour L.
Chemical Communications, 2005
4.
Acetylacetonate bis(thiosemicarbazone) complexes of copper and nickel: towards new copper radiopharmaceuticals
Cowley A.R., Dilworth J.R., Donnelly P.S., Gee A.D., Heslop J.M.
Dalton Transactions, 2004
5.
10.1016/j.mencom.2007.11.012_bib1_5
Thomas
J. Chem. Soc, Dalton Trans., 2003
6.
Studies on the Mechanism of Hypoxic Selectivity in Copper Bis(Thiosemicarbazone) Radiopharmaceuticals
Maurer R.I., Blower P.J., Dilworth J.R., Reynolds C.A., Zheng Y., Mullen G.E.
Journal of Medicinal Chemistry, 2002
8.
THE PREPARATION OF SOME THIOSEMICARBAZONES AND THEIR COPPER COMPLEXES: PART III
Gingras B.A., Suprunchuk T., Bayley C.H.
Canadian Journal of Chemistry, 1962
10.
Chemistry of Carbon Compounds, ed. E. H. Rodd, Elsevier, Amsterdam, 1957, p. 246.
12.
G. M. Sheldrick, SHELXLTL. Program for Crystal Structure Refinement, Release 5.03, Siemens Analytical X-ray Instruments Inc., WI, USA, 1995.
13.
10.1016/j.mencom.2007.11.012_bib8
Parsi
Comput. Chem., 1983