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Synthesis of spirophosphoranes containing a phosphorus–carbon bond using the reactions of substituted benzo[d]-1,3,2-dioxaphospholes with diethyl acetylenedicarboxylate

Liliya Misbakhovna Abdrakhmanova 1
Liliya Misbakhovna Abdrakhmanova
,  , 
Tamara Aleksandrovna Baronova 1
Tamara Aleksandrovna Baronova
, 
Mudaris Nurgaleevich Dimukhametov 1
Mudaris Nurgaleevich Dimukhametov
, 
Dmitry Borisovich Krivolapov 1
Dmitry Borisovich Krivolapov
, 
Igor Anatol'evich Litvinov 1
Igor Anatol'evich Litvinov
, 
Rashid Zagitovich Musin 1
Rashid Zagitovich Musin
, 
Aleksandr Ivanovich Konovalov 1
Aleksandr Ivanovich Konovalov
10.1016/j.mencom.2007.09.012
Published 2007-09-12
Communication , Volume 17, Issue 5, 284-286
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Abdrakhmanova L. M. et al. Synthesis of spirophosphoranes containing a phosphorus–carbon bond using the reactions of substituted benzo[d]-1,3,2-dioxaphospholes with diethyl acetylenedicarboxylate // Mendeleev Communications. 2007. Vol. 17. No. 5. pp. 284-286.
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Abdrakhmanova L. M., Mironov V. F., Baronova T. A., Dimukhametov M. N., Krivolapov D. B., Litvinov I. A., Musin R. Z., Konovalov A. I. Synthesis of spirophosphoranes containing a phosphorus–carbon bond using the reactions of substituted benzo[d]-1,3,2-dioxaphospholes with diethyl acetylenedicarboxylate // Mendeleev Communications. 2007. Vol. 17. No. 5. pp. 284-286.
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TY - JOUR
DO - 10.1016/j.mencom.2007.09.012
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2007.09.012
TI - Synthesis of spirophosphoranes containing a phosphorus–carbon bond using the reactions of substituted benzo[d]-1,3,2-dioxaphospholes with diethyl acetylenedicarboxylate
T2 - Mendeleev Communications
AU - Abdrakhmanova, Liliya Misbakhovna
AU - Mironov, Vladimir Fedorovich
AU - Baronova, Tamara Aleksandrovna
AU - Dimukhametov, Mudaris Nurgaleevich
AU - Krivolapov, Dmitry Borisovich
AU - Litvinov, Igor Anatol'evich
AU - Musin, Rashid Zagitovich
AU - Konovalov, Aleksandr Ivanovich
PY - 2007
DA - 2007/09/12
PB - Mendeleev Communications
SP - 284-286
IS - 5
VL - 17
ER -
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@article{2007_Abdrakhmanova,
author = {Liliya Misbakhovna Abdrakhmanova and Vladimir Fedorovich Mironov and Tamara Aleksandrovna Baronova and Mudaris Nurgaleevich Dimukhametov and Dmitry Borisovich Krivolapov and Igor Anatol'evich Litvinov and Rashid Zagitovich Musin and Aleksandr Ivanovich Konovalov},
title = {Synthesis of spirophosphoranes containing a phosphorus–carbon bond using the reactions of substituted benzo[d]-1,3,2-dioxaphospholes with diethyl acetylenedicarboxylate},
journal = {Mendeleev Communications},
year = {2007},
volume = {17},
publisher = {Mendeleev Communications},
month = {Sep},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2007.09.012},
number = {5},
pages = {284--286},
doi = {10.1016/j.mencom.2007.09.012}
}
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Abdrakhmanova, Liliya Misbakhovna, et al. “Synthesis of spirophosphoranes containing a phosphorus–carbon bond using the reactions of substituted benzo[d]-1,3,2-dioxaphospholes with diethyl acetylenedicarboxylate.” Mendeleev Communications, vol. 17, no. 5, Sep. 2007, pp. 284-286. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2007.09.012.

Abstract

The reaction of 2-(2-oxo-1,2-diphenyl)ethoxy- and 2-(2-methylcarbonyl)phenyloxybenzo[d]-1,3,2-dioxaphospholes with diethyl acetylenedicarboxylate was used to synthesise 5,6-bis(ethoxycarbonyl)-3,4-diphenyl-1,1-phenylenedioxy-1-phospha-2,7-dioxabicyclo[2.2.11,4]hept-5-ene and 5-methyl-6,7-bis(ethoxycarbonyl)-1,1-phenylenedioxy-3,4-benzo-1-phospha-2,8-dioxabicyclo-[3.2.11,5]oct-6-ene in high yields.

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