Home / Publications / New simple synthesis of N-acylpyrazolidines and N-arylsulfonyl-2-pyrazolines

New simple synthesis of N-acylpyrazolidines and N-arylsulfonyl-2-pyrazolines

Alexander Vladimirovich Shevtsov 1
Alexander Vladimirovich Shevtsov
, 
Alexander Aleksandrovich Kislukhin 1
Alexander Aleksandrovich Kislukhin
, 
Vladimir Vladimirovich Kuznetsov 1
Vladimir Vladimirovich Kuznetsov
, 
Vera Yur'evna Petukhova 1
Vera Yur'evna Petukhova
, 
Vladimir A Maslennikov 1
Vladimir A Maslennikov
, 
Alexandra Olegovna Borissova 2
Alexandra Olegovna Borissova
, 
Konstantin Alexandrovich Lyssenko 2
Konstantin Alexandrovich Lyssenko
, 
Nina Nikolaevna Makhova 1
Nina Nikolaevna Makhova
10.1016/j.mencom.2007.03.023
Published 2007-03-15
Communication , Volume 17, Issue 2, 119-121
9
Share
Cite this
GOST
 | 
Cite this
GOST Copy
Shevtsov A. V. et al. New simple synthesis of N-acylpyrazolidines and N-arylsulfonyl-2-pyrazolines // Mendeleev Communications. 2007. Vol. 17. No. 2. pp. 119-121.
GOST all authors (up to 50) Copy
Shevtsov A. V., Kislukhin A. A., Kuznetsov V. V., Petukhova V. Y., Maslennikov V. A., Borissova A. O., Lyssenko K. A., Makhova N. N. New simple synthesis of N-acylpyrazolidines and N-arylsulfonyl-2-pyrazolines // Mendeleev Communications. 2007. Vol. 17. No. 2. pp. 119-121.
RIS
 | 
Cite this
RIS Copy
TY - JOUR
DO - 10.1016/j.mencom.2007.03.023
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2007.03.023
TI - New simple synthesis of N-acylpyrazolidines and N-arylsulfonyl-2-pyrazolines
T2 - Mendeleev Communications
AU - Shevtsov, Alexander Vladimirovich
AU - Kislukhin, Alexander Aleksandrovich
AU - Kuznetsov, Vladimir Vladimirovich
AU - Petukhova, Vera Yur'evna
AU - Maslennikov, Vladimir A
AU - Borissova, Alexandra Olegovna
AU - Lyssenko, Konstantin Alexandrovich
AU - Makhova, Nina Nikolaevna
PY - 2007
DA - 2007/03/15
PB - Mendeleev Communications
SP - 119-121
IS - 2
VL - 17
ER -
BibTex
 | 
Cite this
BibTex (up to 50 authors) Copy
@article{2007_Shevtsov,
author = {Alexander Vladimirovich Shevtsov and Alexander Aleksandrovich Kislukhin and Vladimir Vladimirovich Kuznetsov and Vera Yur'evna Petukhova and Vladimir A Maslennikov and Alexandra Olegovna Borissova and Konstantin Alexandrovich Lyssenko and Nina Nikolaevna Makhova},
title = {New simple synthesis of N-acylpyrazolidines and N-arylsulfonyl-2-pyrazolines},
journal = {Mendeleev Communications},
year = {2007},
volume = {17},
publisher = {Mendeleev Communications},
month = {Mar},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2007.03.023},
number = {2},
pages = {119--121},
doi = {10.1016/j.mencom.2007.03.023}
}
MLA
Cite this
MLA Copy
Shevtsov, Alexander Vladimirovich, et al. “New simple synthesis of N-acylpyrazolidines and N-arylsulfonyl-2-pyrazolines.” Mendeleev Communications, vol. 17, no. 2, Mar. 2007, pp. 119-121. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2007.03.023.

Abstract

New simple methods for the synthesis of 1-mono- and 1,2-diacylpyrazolidines as well as 1-arylsulfonyl-2-pyrazolines, based on the interaction of 1,5-diazabicylo[3.1.0]hexanes with acyl- or arylsulfonyl chlorides, have been proposed.

References

3.
The development of novel inhibitors of tumor necrosis factor-α (TNF-α) production based on substituted [5,5]-bicyclic pyrazolones
Laufersweiler M.J., Brugel T.A., Clark M.P., Golebiowski A., Bookland R.G., Laughlin S.K., Sabat M.P., Townes J.A., VanRens J.C., De B., Hsieh L.C., Heitmeyer S.A., Juergens K., Brown K.K., Mekel M.J., et. al.
Bioorganic and Medicinal Chemistry Letters, 2004
4.
Development of Orally Bioavailable Bicyclic Pyrazolones as Inhibitors of Tumor Necrosis Factor-α Production
Clark M.P., Laughlin S.K., Laufersweiler M.J., Bookland R.G., Brugel T.A., Golebiowski A., Sabat M.P., Townes J.A., VanRens J.C., Djung J.F., Natchus M.G., De B., Hsieh L.C., Xu S.C., Walter R.L., et. al.
Journal of Medicinal Chemistry, 2004
5.
D. T. Fosbenner, R. Liu and M. L. Moore, WO 2006/094003, 08.09.2006.
6.
J. Elguero, in Comprehensive Heterocyclic Chemistry, eds. A. R. Katritzky and C. W. Rees, Pergamon Press, Oxford, 1984. vol. 5, p. 169.
7.
The Synthesis and Physical Properties of Some 1- and 2-Pyrazolines1
Crawford R.J., Mishra A., Dummel R.J.
Journal of the American Chemical Society, 1966
8.
The reduction of functionalized pyrazolium salts as a stereoselective route to functionalized pyrazolidines
Bañuelos L.A., Cuadrado P., González-Nogal A.M., López-Solera I., Pulido F.J., Raithby P.R.
Tetrahedron, 1996
10.
Thermal Decomposition of cis- and trans-3,5-Dimethyl-1-pyrazoline
Crawford R.J., Mishra A.
Journal of the American Chemical Society, 1965
11.
Reactions of phenylhydrazones with electron-deficient alkenes
Snider B.B., Conn R.S., Sealfon S.
Journal of Organic Chemistry, 1979
12.
D. I. Sipkin, PhD Thesis, St. Petersburg University, 2002.
13.
10.1016/j.mencom.2007.03.023_bib13
Koptelov
Zh. Org. Khim., 2000
14.
Ring transformation of 1,5-diazabicyclo[3.1.0]hexanes under the action of arylketenes
Shevtsov A.V., Kuznetsov V.V., Kislukhin A.A., Petukhova V.Y., Strelenko Y.A., Makhova N.N., Lyssenko K.A.
Journal of Heterocyclic Chemistry, 2006
15.
Asymmetric nitrogen—41
Shustov G.V., Denisenko S.N., Chervin I.I., Asfandiarov N.L., Kostyanovsky R.G.
Tetrahedron, 1985
16.
Über Darstellung und Eigenschaften α-Halogenierter Amine
Böhme H., Mundlos E., Herboth O.
European Journal of Inorganic Chemistry, 1957
17.
Eine neue Synthese für 1,2,3-Triazole
Beck G., Giinther D.
European Journal of Inorganic Chemistry, 1973
18.
The Configuration of Tervalent Nitrogen. A Bicyclic Hydrazine Derivative1
Buhle E.L., Moore A.M., Wiselogle F.Y.
Journal of the American Chemical Society, 1943
20.
Testing aspherical atom refinements on small-molecule data sets
Hansen N.K., Coppens P.
Acta Crystallographica Section A, 1978
21.
T. S. Koritsansky, S. T. Howard, T. Richter, P. Macchi, A. Volkov, C. Gatti, P. R. Mallinson, L. J. Farrugia, Z. Su and N. K. Hansen, XD – A Computer Program Package for Multipole Refinement and Topological Analysis of Charge Densities from Diffraction Data, 2003.
23.
A. Stash and V. Tsirelson. WinXrpo, A Program for Calculation of the Crystal and Molecular Properties Using the Model Electron Density, 2001. further information available at http://xray.nifhi.ru/wxp/.