Home / Publications / Coupling of 1,2-bis(alkoxyamino)cyclohexanes with 1,3-dicarbonyl compounds: first synthesis of 1,4-dialkoxy-2,3-dihydro-1,4-diazepinium salts

Coupling of 1,2-bis(alkoxyamino)cyclohexanes with 1,3-dicarbonyl compounds: first synthesis of 1,4-dialkoxy-2,3-dihydro-1,4-diazepinium salts

Evgenii Alekseevich Mostovich 1, 2
Evgenii Alekseevich Mostovich
, 
Dmitrii Gennad'evich Mazhukin 1, 2
Dmitrii Gennad'evich Mazhukin
, 
Yuriy Vasil'evich Gatilov 1
Yuriy Vasil'evich Gatilov
, 
Tatyana Valeryevna Rybalova 1
Tatyana Valeryevna Rybalova
10.1016/j.mencom.2007.01.019
Published 2007-01-17
Communication , Volume 17, Issue 1, 48-50
3
Share
Cite this
GOST
 | 
Cite this
GOST Copy
Mostovich E. A. et al. Coupling of 1,2-bis(alkoxyamino)cyclohexanes with 1,3-dicarbonyl compounds: first synthesis of 1,4-dialkoxy-2,3-dihydro-1,4-diazepinium salts // Mendeleev Communications. 2007. Vol. 17. No. 1. pp. 48-50.
GOST all authors (up to 50) Copy
Mostovich E. A., Mazhukin D. G., Gatilov Y. V., Rybalova T. V. Coupling of 1,2-bis(alkoxyamino)cyclohexanes with 1,3-dicarbonyl compounds: first synthesis of 1,4-dialkoxy-2,3-dihydro-1,4-diazepinium salts // Mendeleev Communications. 2007. Vol. 17. No. 1. pp. 48-50.
RIS
 | 
Cite this
RIS Copy
TY - JOUR
DO - 10.1016/j.mencom.2007.01.019
UR - https://mendcomm.colab.ws/publications/10.1016/j.mencom.2007.01.019
TI - Coupling of 1,2-bis(alkoxyamino)cyclohexanes with 1,3-dicarbonyl compounds: first synthesis of 1,4-dialkoxy-2,3-dihydro-1,4-diazepinium salts
T2 - Mendeleev Communications
AU - Mostovich, Evgenii Alekseevich
AU - Mazhukin, Dmitrii Gennad'evich
AU - Gatilov, Yuriy Vasil'evich
AU - Rybalova, Tatyana Valeryevna
PY - 2007
DA - 2007/01/17
PB - Mendeleev Communications
SP - 48-50
IS - 1
VL - 17
ER -
BibTex
 | 
Cite this
BibTex (up to 50 authors) Copy
@article{2007_Mostovich,
author = {Evgenii Alekseevich Mostovich and Dmitrii Gennad'evich Mazhukin and Yuriy Vasil'evich Gatilov and Tatyana Valeryevna Rybalova},
title = {Coupling of 1,2-bis(alkoxyamino)cyclohexanes with 1,3-dicarbonyl compounds: first synthesis of 1,4-dialkoxy-2,3-dihydro-1,4-diazepinium salts},
journal = {Mendeleev Communications},
year = {2007},
volume = {17},
publisher = {Mendeleev Communications},
month = {Jan},
url = {https://mendcomm.colab.ws/publications/10.1016/j.mencom.2007.01.019},
number = {1},
pages = {48--50},
doi = {10.1016/j.mencom.2007.01.019}
}
MLA
Cite this
MLA Copy
Mostovich, Evgenii Alekseevich, et al. “Coupling of 1,2-bis(alkoxyamino)cyclohexanes with 1,3-dicarbonyl compounds: first synthesis of 1,4-dialkoxy-2,3-dihydro-1,4-diazepinium salts.” Mendeleev Communications, vol. 17, no. 1, Jan. 2007, pp. 48-50. https://mendcomm.colab.ws/publications/10.1016/j.mencom.2007.01.019.

Abstract

The reactions of two 1,2-bis(alkoxyamino)cyclohexanes with 2-substituted malonic aldehydes, acetylacetaldehyde and acetyl-acetone gave rise to imidazolidine derivatives, whereas 1,4-dialkoxy-2,3-dihydro-2,3-cyclohexano-1,4-diazepinium salts were the only products in acidic media.

References

1.
10.1016/j.mencom.2007.01.019_bib1_1
Mazhukin
Izv. Akad. Nauk, Ser. Khim., 1996
2.
Intramolecular Cyclization of 1,2-bis(N-alkoxy-N-nitrosoamino)alkanes: A Unique Route to 4,5-Dihydro-1,2,3-triazole 2-Oxides
Khlestkin V.K., Mazhukin D.G., Tikhonov A.Y., Rybalova T.V., Bagryanskaya I.Y., Gatilov Y.V.
Synthesis, 2000
3.
Unexpected transformation of 1,2-bis(N-methoxy-N-nitrosoamino)cycloalkanes: First synthesis of 4,5-dihydro-1,2,3-triazole 2-oxides
Khlestkin V.K., Mazhukin D.G., Tikhonov A.Y., Bagryanskaya I.Y., Gatilov Y.V., Utepbergenov D.I., Khramtsov V.V., Volodarsky L.B.
Tetrahedron Letters, 1996
5.
N-Methoxyindole-3-Carbinol Is a More Efficient Inducer of Cytochrome P-450 1A1 in Cultured Cells Than Indol-3-Carbinol
Stephensen P.U., Bonnesen C., Schaldach C., Andersen O., Bjeldanes L.F., Vang O.
Nutrition and Cancer, 2000
6.
Structure-activity relationships of anti-HIV-1 N-alkoxy- and N-allyloxy-benzimidazoles
Evans T.M., Gardiner J.M., Mahmood N., Smis M.
Bioorganic and Medicinal Chemistry Letters, 1997
7.
N-Alkoxy Analogues of 3,4,5-Trihydroxypiperidine
Sun L., Li P., Amankulor N., Tang W., Landry D.W., Zhao K.
Journal of Organic Chemistry, 1998
9.
Synthesis of 5-Substituted 1-Hydroxy-1,2,3-triazoles through Directed Lithiation of 1-(Benzyloxy)-1,2,3-triazole
Uhlmann P., Felding J., Vedsø P., Begtrup M.
Journal of Organic Chemistry, 1997
10.
A Novel Class of Zinc-Binding Inhibitors for the Phosphatidylcholine-Preferring Phospholipase C from Bacillus cereus
Martin S.F., Follows B.C., Hergenrother P.J., Franklin C.L.
Journal of Organic Chemistry, 2000
12.
New Polymer Synthesis by Nitroxide Mediated Living Radical Polymerizations
Hawker C.J., Bosman A.W., Harth E.
Chemical Reviews, 2001
13.
Alkoxyamine-Mediated Radical Cyclizations
Leroi C., Fenet B., Couturier J., Guerret O., Ciufolini M.A.
Organic Letters, 2003
14.
Alkoxyamine-Mediated Radical Synthesis of Indolinones and Indolines
Leroi C., Bertin D., Dufils P., Gigmes D., Marque S., Tordo P., Couturier J., Guerret O., Ciufolini M.A.
Organic Letters, 2003
17.
10.1016/j.mencom.2007.01.019_bib13
Klimko
Zh. Obshch. Khim., 1959
18.
Arnold Z., Žemlička J.
Collection of Czechoslovak Chemical Communications, 2013
19.
10.1016/j.mencom.2007.01.019_bib15
Barnett
J. Chem. Soc. (C), 1966
20.
10.1016/j.mencom.2007.01.019_bib16
Fanta
Chem. Rev., 1967